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1. 发明授权

US3741921A Flame retardant polyurethane foams based on polyethers from 4,4,4 - trichloro-1,2-epoxybutane 失效
标题翻译：基于4,4,4-三氯-1,2-环氧丁烷的聚醚的阻燃聚氨酯泡沫塑料
公开(公告)号：US3741921A
公开(公告)日：1973-06-26
申请号：US3741921D
申请日：1972-05-01
申请人： OLIN CORP
发明人： LAPKIN M
IPC分类号： C08G18/50 , C08G65/22 , C08G22/46 , C08G22/16
CPC分类号： C08G65/223 , C08G18/5009 , Y10S260/24 , Y10S521/914
摘要： FLAME RETARDANT POLYURETHANE FOAMS AND A PROCESS FOR PREPARING THEM ARE DISCLOSED. THE PROCESS COMPRISES REACTING, IN THE PRESENCE OF A CATALYST, AND A FOAMING AGENT, AN ORGANIC ISOCYANATE WITH A CHLORINATED POLYHYDROXY POLYETHER PREPARED BY REACTING A DEXTROSE- OR SUCROSE-BASED MATERIAL WITH 4,4,4-TRICHLORO-1,2-EPOXYBUTANE.

2. 发明授权

US3719636A Method for the preparation of biodegradable glycidol surfactants 失效
标题翻译：生物可降解甘露糖醇表面活性剂的制备方法
公开(公告)号：US3719636A
公开(公告)日：1973-03-06
申请号：US3719636D
申请日：1970-04-09
申请人： OLIN CORP
发明人： WOJTOWICZ J , LAPKIN M
IPC分类号： C11D1/72 , C07C41/02 , C07C41/10
CPC分类号： C11D1/72 , Y10S516/01 , Y10S516/02 , Y10S516/917
摘要： This invention relates to a novel method of preparing biodegradable glycidol surfactants by reacting selected aliphatic alcohols with glycidol in the presence of a polar, non-reactive, miscible solvent and to the surfactants produced by such method.
摘要翻译：本发明涉及一种通过选择的脂肪醇与缩水甘油在极性，非反应性混溶性溶剂的存在下反应制备可生物降解的缩水甘油表面活性剂的方法，以及通过这种方法制备的表面活性剂。

3. 发明授权

US3847844A Process for making fire-retardant polyurethane foam using crude 4,4,4-trichloro-1,2-epoxybutane 失效
标题翻译：使用原料4,4,4-三氯-1,2-环氧丁烷制备阻燃聚氨酯泡沫的方法
公开(公告)号：US3847844A
公开(公告)日：1974-11-12
申请号：US40863773
申请日：1973-10-23
申请人： OLIN CORP
发明人： POLAK R , FUZESI S , LAPKIN M
IPC分类号： C07D303/08 , C08G18/50 , C08G65/22 , C08G22/46 , C08G22/16
CPC分类号： C07D303/08 , C08G18/5009 , C08G65/223
摘要： 1. IN PROCESS FOR PREPARING A POLYURETHANE FOAM BY REACTING A POLYETHER POLYOL WITH AN ORGANIC POLYISOCYANATE IN THE PRESENCE OF A REACTION CATALYST AND A FOAMING AGENT, SAID POLYETHER POLYOL COMPRISING THE PRODUCT OF REACTING 4,4,4, - TRICHLORO -1,2- EPOSYBUTANE WITH A MIXTURE OF (1) DEXTROSE AND (2) WATER, A POLYHYDRIC ALIPHATIC ALCOHOL OR A MIXTURE OF WATER AND A POLYHYDRIC ALIPHATIC ALCOHOL, THE IMPROVEMENT WHICH COMPRISES USING SAID EPOXYBUTANE AS A CRUDE MATERIAL HAVING NO MORE THAN ABOUT 5% BY WEIGHT OF VOLATILE COMPONENTS AND CONTAINING FROM ABOUT 15 TO ABOUT ABOUR 42% BY WEIGHT OF IMPURITIES AND CORRESPONDINGLY FROM ABOUT 85 TO ABOUT 58% OF SAID EPOXYBUTANE, SAID CRUDE EPOXYBUTANE BEING PREPARED BY A PROXESS CONSISTING ESSENTIALLY OF (A) REACTING, AT A TEMPERATURE FROM ABOUT 35 TO ABOUT 62* C., 4,4,4-TRICHLORO-2-HALOBUTANOL WITH AN AQUEOUS SOLUTION AF AN ALKALI METAL HYDROXIDE OR AN ALKALINE EARTH METAL HYDROXIDE, SAID AQUEOUS SOLUTION BEING EMPLOYED IN A SUFFICIENT PROPORTION TO PROVIDE AT LEAST A STOICIOMETRIC AMOUNT OF HYDROXIDE WHICH IS REQUIRED TO REACT WITH SAID 4,4,4, - TRICHLORO -2HALOGUTANOL, THEREBY FORMING A TWO-PHASE REACTION PRODUCT MIXTURE, NAMELY, AN AQUEOUS PHASE AND A NON-AQUEOUS PHASE CONTAINING SAID CRUDE EPOXYBUTANE, AND (B) SEPARATING SAID TWO PHASES AND RECOVERING SAID CRUDE EPOXYBUTANE.

4. 发明授权

US3726855A Chlorinated polyhydroxy polyethers 失效
标题翻译：氯化聚羟基聚醚
公开(公告)号：US3726855A
公开(公告)日：1973-04-10
申请号：US3726855D
申请日：1970-07-06
申请人： OLIN CORP
发明人： LAPKIN M
IPC分类号： C08G18/50 , C07C47/18
CPC分类号： C08G18/5009
摘要： CHLORINATED POLYHYDROXY POLYETHERS ARE PREPARED BY REACTING A SUCROSE- OR DEXTROSE-BASED MATERIAL, WITH OVER 15% BY WEIGHT OF THE TOTAL REACTANTS EMPLOYED IN PREPARING THE CHLORINATED POLYHYDROXY POLYETHER OF 4,4,4-TRICHLORO-1,2-EPOXYBUTANE IN THE PRESENCE OF AN ACID CATALYST AT 30-200*C. THESE CHLORINATED POLYHYDROXY POLYETHERS ARE USEFUL IN THE PREPARATION OF FLAME-RETARDANT POLYURETHANE FOAMS.

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