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    • 4. 发明授权
    • Apparatus for measuring a silver or halogen ion concentration
    • 用于测量银或卤素离子浓度的装置
    • US06372105B1
    • 2002-04-16
    • US08657903
    • 1996-06-07
    • Hirokazu SaitoSugihiko Tada
    • Hirokazu SaitoSugihiko Tada
    • G01N2726
    • G03C1/015
    • A method of producing a silver halide photographic emulsion in which a silver ion concentration in precipitation of a silver halide emulsion in a precipitation bath is controlled, wherein a precipitation bath in which stirring is conducted rapidly and uniformly, and crystal formation and crystal growth are uniformly performed is used, the method comprises the steps of: in a start period of precipitation, quantitavely adding a silver nitrate solution and a halogen salt solution at a constant ratio flow rate; when an EAg value reaches a designated EAg value region in the vicinity of a preset target EAg value, starting a control of an adding rate of the halogen salt solution by using a controller which has an operation period equal to or shorter than 1 sec.; and after holding a tuning parameter of a proportional, integral and differential (PID) action controller to a minimum response level, conducting a control in which the tuning parameter is switched to an optimum control tuning parameter which corresponds to the preset target value and a solute rate of silver/halogen ions to be added.
    • 一种卤化银照相乳剂的制备方法,其中控制沉淀浴中的卤化银乳剂沉淀中的银离子浓度,其中快速且均匀地进行搅拌的沉淀浴以及晶体生成和晶体生长均匀 所述方法包括以下步骤:在起始沉淀期间,以恒定比例流量定量加入硝酸银溶液和卤素盐溶液; 当EAg值达到预设目标EAg值附近的指定EAg值区域时,通过使用具有等于或小于1sec的操作周期的控制器开始控制卤盐溶液的添加率; 并且在将比例积分微分(PID)动作控制器的调谐参数保持在最小响应水平之后,进行将调谐参数切换到对应于预设目标值的最佳控制调谐参数的控制和溶质 银/卤离子的添加​​速率。
    • 5. 发明授权
    • Process for producing a magnetic recording medium
    • 磁记录介质的制造方法
    • US4664734A
    • 1987-05-12
    • US823871
    • 1986-01-29
    • Tsutomu OkitaSugihiko Tada
    • Tsutomu OkitaSugihiko Tada
    • G11B5/84G11B5/842H01F10/02
    • G11B5/842G11B5/84
    • A process for producing a magnetic recording medium is disclosed. The process comprises coating a magnetic coating composition comprising a ferromagnetic powder, a binder, and an organic solvent on either a non-magnetic support or a roller or band having a mirror surface to form a magnetic layer on the non-magnetic support or the roller or band, respectively, drying the magnetic layer so as to have a solvent content of from 0.05 to 10% by weight, contacting the magnetic layer on the support or the roller or band with a roller or band having a mirror surface or a non-magnetic support, respectively, and separating the magnetic layer from the roller or band. The resulting magnetic recording medium has smooth surface, high electromagnetic properties, and good durability.
    • 公开了一种制造磁记录介质的方法。 该方法包括在非磁性载体或具有镜面的辊或带上涂覆包含铁磁性粉末,粘合剂和有机溶剂的磁性涂料组合物,以在非磁性载体或辊上形成磁性层 或带,分别干燥磁性层以使溶剂含量为0.05至10重量%,使支撑体或辊或带上的磁性层与具有镜面或非磁性层的辊或带接触, 分别将磁性层与辊或带分离。 所得磁记录介质具有光滑的表面,高的电磁特性和良好的耐久性。
    • 7. 发明授权
    • Method of producing a silver halide photographic emulsion, apparatus for
the same, method of measuring a silver or halogen ion concentration and
an apparatus for the same
    • 制备卤化银照相乳剂的方法,其设备,银或卤素离子浓度测定方法及其装置
    • US5702851A
    • 1997-12-30
    • US549543
    • 1995-10-27
    • Hirokazu SaitoSugihiko Tada
    • Hirokazu SaitoSugihiko Tada
    • G03C1/015G03K1/015
    • G03C1/015
    • A method of producing a silver halide photographic emulsion in which a silver ion concentration in precipitation of a silver halide emulsion in a precipitation bath is controlled, wherein a precipitation bath in which stirring is conducted rapidly and uniformly, and crystal formation and crystal growth are uniformly performed is used, the method comprises the steps of: in a start period of precipitation, quantitavely adding a silver nitrate solution and a halogen salt solution at a constant ratio flow rate; when an E.sub.Ag value reaches a designated E.sub.Ag value region in the vicinity of a preset target E.sub.Ag value, starting a control of an adding rate of the halogen salt solution by using a controller which has an operation period equal to or shorter than 1 sec.; and after holding a tuning parameter of a proportional, integral and differential (PID) action controller to a minimum response level, conducting a control in which the tuning parameter is switched to an optimum control tuning parameter which corresponds to the preset target value and a solute rate of silver/halogen ions to be added.
    • 一种卤化银照相乳剂的制备方法,其中控制沉淀浴中的卤化银乳剂沉淀中的银离子浓度,其中快速且均匀地进行搅拌的沉淀浴以及晶体生成和晶体生长均匀 所述方法包括以下步骤:在起始沉淀期间,以恒定比例流量定量加入硝酸银溶液和卤素盐溶液; 当EAg值达到预设目标EAg值附近的指定EAg值区域时,通过使用具有等于或小于1sec的操作周期的控制器开始控制卤盐溶液的添加率; 并且在将比例积分微分(PID)动作控制器的调谐参数保持在最小响应水平之后,进行将调谐参数切换到对应于预设目标值的最佳控制调谐参数的控制和溶质 银/卤离子的添加​​速率。