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1. 发明申请

US20080269455A1 Process for Production of Polybenzazole Polymer and the Polymer 审中-公开
标题翻译：聚吲哚聚合物和聚合物的生产工艺
公开(公告)号：US20080269455A1
公开(公告)日：2008-10-30
申请号：US12066819
申请日：2006-09-11
申请人： Naoki Watanabe , Go Mastuoka , Fuyuhiko Kubota , Yukihiro Abe , Yasuko Mitooka
发明人： Naoki Watanabe , Go Mastuoka , Fuyuhiko Kubota , Yukihiro Abe , Yasuko Mitooka
IPC分类号： C08G73/22
CPC分类号： C08G73/22 , C08G73/18 , C08G75/32
摘要： PROBLEMS The present invention relates to a process for producing a polybenzoxazole polymer and provides a process for producing the polybenzoxazole polymer within a short reaction time. MEANS FOR SOLVING PROBLEMS A process for producing a polybenzazole polymer comprises producing the polybenzazole polymer in a non-oxidizing dehydrating solvent while employing a compound represented by the following general formula (1) as a raw material including a first polymerization step in which polymerization is performed at a temperature of 150° C. or less and a latter polymerization step in which polymerization is performed at a temperature of 200° C. or more, wherein at least the latter polymerization step is performed in a kneading-type reaction apparatus to complete the polymerization reaction: wherein X represents an O atom, an S atom or an NH group; Ar1 represents a tetravalent organic group having two or less of benzene rings, naphthalene rings or pyridine rings; Ar2 represents a bivalent organic group having two or less of benzene rings, naphthalene rings or pyridine rings; both of Ar1 and Ar2 may have one or more functional groups such as a methyl group and a hydroxyl group; and R represents H or a univalent organic group with a carbon number of 1 to 6.
摘要翻译：聚苯并恶唑聚合物的制造方法技术领域本发明涉及聚苯并恶唑聚合物的制造方法，其提供在短的反应时间内生产聚苯并恶唑聚合物的方法。解决问题的手段聚吲哚聚合物的制造方法包括在使用由以下通式（1）表示的化合物作为原料的非氧化性脱水溶剂中制造聚吲哚聚合物，其包括进行聚合的第一聚合步骤在150℃以下的温度下进行聚合，后一聚合步骤在200℃或更高温度下进行聚合，其中至少在后一聚合步骤在捏合型反应设备中进行以完成聚合反应：其中X表示O原子，S原子或NH基团; Ar 1表示具有2个以下苯环，萘环或吡啶环的四价有机基团; Ar 2表示具有两个或更少个苯环，萘环或吡啶环的二价有机基团; Ar 1和Ar 2 2都可以具有一个或多个官能团，例如甲基和羟基; 且R表示H或碳数为1至6的一价有机基团。

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