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    • 2. 发明申请
    • METHOD FOR PRODUCING DISPERSION LIQUID CONTAINING SILVER NANOPARTICLES, AND DISPERSION LIQUID CONTAINING SILVER NANOPARTICLES
    • 用于生产含有银纳米颗粒的分散液的方法和含有银纳米颗粒的分散液
    • US20160264810A1
    • 2016-09-15
    • US15030816
    • 2014-10-01
    • DAICEL CORPORATION
    • Kazuki OKAMOTOYuki IGUCHI
    • C09D11/52H01L21/28H01L29/49H01L21/288C09D11/322C09D11/36
    • The present invention provides a dispersion liquid containing silver nano-particles that develops excellent conductivity by low-temperature calcining and has silver nano-particles stably and well dispersed in a dispersion solvent, and a method for producing the dispersion liquid containing silver nano-particles. [solution] A method for producing a dispersion liquid containing silver nano-particles, comprising: mixing a silver compound with amines comprising an aliphatic monoamine (A) comprising an aliphatic hydrocarbon group and one amino group, said hydrocarbon group having 6 or more carbon atoms in total; and further comprising at least one of: an aliphatic monoamine (B) comprising an aliphatic hydrocarbon group and one amino group, said hydrocarbon group having 5 or less carbon atoms in total; and an aliphatic diamine (C) comprising an aliphatic hydrocarbon group and two amino groups, said hydrocarbon group having 8 or less carbon atoms in total; to form a complex compound comprising the silver compound and the amines; thermally decomposing the complex compound by heating to form silver nano-particles; and dispersing the silver nano-particles in a dispersion solvent containing an alcohol-based solvent and an aliphatic hydrocarbon-based solvent in a specific ratio.
    • 本发明提供一种含有银纳米颗粒的分散液,其通过低温煅烧而产生优异的导电性,并且将银纳米颗粒稳定且良好地分散在分散溶剂中,以及含有银纳米颗粒的分散液的制备方法。 [溶液]含有银纳米粒子的分散液的制造方法,其特征在于,将银化合物与包含脂肪族烃基和一个氨基的脂肪族单胺(A)的胺混合,所述烃基的碳原子数为6以上 总共; 并且还包含以下至少一种:脂肪族单胺(B),其包含脂族烃基和一个氨基,所述烃基总共具有5个或更少的碳原子; 和包含脂族烃基和两个氨基的脂族二胺(C),所述烃基总共具有8个或更少的碳原子; 以形成包含银化合物和胺的络合物; 通过加热热分解复合化合物以形成银纳米颗粒; 并以特定的比例将银纳米颗粒分散在含有醇系溶剂和脂族烃类溶剂的分散溶剂中。