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    • 2. 发明授权
    • Transmission electron microscope having electron spectroscope
    • 透射电子显微镜具有电子分光镜
    • US08263936B2
    • 2012-09-11
    • US12414883
    • 2009-03-31
    • Shohei TeradaYoshifumi Taniguchi
    • Shohei TeradaYoshifumi Taniguchi
    • G01N23/00G21K7/00
    • G01N23/04G01N2223/102G01N2223/3037
    • A transmission electron microscope is capable of correcting, with high efficiency and high accuracy, an electron energy loss spectrum extracted from each of measured portions included in an electron energy loss spectral image with two axes representing the amount of an energy loss and positional information on a measured portion. The transmission electron microscope has an electron spectroscope and a spectrum correction system. The spectrum correction system corrects a spectrum extracted from each measured portion included in an electron energy loss spectral image acquired from a sample based on a difference between a spectrum extracted from a standard portion of a standard spectral image and a spectrum extracted from a portion different from the standard portion.
    • 透射电子显微镜能够以高效率和高精度校正从包含在电子能量损失光谱图像中的每个测量部分提取的电子能量损失谱,其中两个轴表示能量损失量和位置信息 测量部分。 透射电子显微镜具有电子分光镜和光谱校正系统。 频谱校正系统基于从标准光谱图像的标准部分提取的光谱与从不同于标准光谱图像的部分提取的光谱之间的差异,从包含在从样本获取的电子能量损失光谱图像中的每个测量部分中提取的光谱 标准部分。
    • 8. 发明授权
    • Transmission electron microscope and method of observing element
distribution
    • 透射电子显微镜及观察元素分布的方法
    • US5981948A
    • 1999-11-09
    • US30477
    • 1998-02-25
    • Yoshifumi TaniguchiShigeto Isakozawa
    • Yoshifumi TaniguchiShigeto Isakozawa
    • G01N23/04H01J37/22H01J37/26H01J37/153
    • H01J37/26H01J2237/05
    • Letting core-loss energy of an objective element be E.sub.c, and width of the energy selection slit be .DELTA.E. Initially, a pre-edge image obtained by increasing an acceleration voltage of an electron gun by E.sub.c -.DELTA.E and a pre-pre-edge image obtained by increasing an acceleration voltage by E.sub.c -.DELTA.E are taken with the same exposure time, and an intensity ratio R of the pre-edge image to the pre-pre-edge image is calculated. Next, a post-edge image obtained by increasing an acceleration voltage by E.sub.c is taken with an exposure time t.sub.pre, and a pre-edge image is taken with an exposure time R.times.t.sub.pre. An element distribution image of the objective element can be obtained by simply performing image subtraction of the pre-edge image from the post-edge image in a computer.
    • 使目标元素的核心损耗能量为Ec,能量选择狭缝的宽度为DELTA E.首先,通过用Ec-DELTA E增加电子枪的加速电压而获得的前缘图像和预先 以相同的曝光时间拍摄通过用Ec-DELTA E增加加速电压而获得的-edge图像,并且计算前缘图像与前前缘图像的强度比R. 接下来,利用曝光时间tpre拍摄通过用Ec增加加速电压而获得的后边缘图像,并且以曝光时间Rxtpre拍摄前边缘图像。 可以通过简单地从计算机中的后边缘图像执行预边缘图像的图像相减来获得目标元素的元素分布图像。
    • 10. 发明申请
    • TRANSMISSION ELECTRON MICROSCOPE HAVING ELECTRON SPECTROMETER
    • 具有电子光谱仪的传输电子显微镜
    • US20110240854A1
    • 2011-10-06
    • US13133653
    • 2009-11-11
    • Shohei TeradaYoshifumi TaniguchiTatsumi Hirano
    • Shohei TeradaYoshifumi TaniguchiTatsumi Hirano
    • G01N23/00H01J37/153
    • H01J37/05H01J37/153H01J37/244H01J2237/2446
    • In a spectral image formed by two orthogonal axes, one of which is an axis of the amount of energy loss and the other of which is an axis of positional information, by the use of an electron spectrometer and a transmission electron microscope, distortion in the spectral image of a sample to be analyzed is corrected with high efficiency and high accuracy by comparing electron beam positions calculated from a two-dimensional electron beam position image formed by the two orthogonal axes (the axis of the amount of energy loss and the axis of positional information) with reference electron beam positions, and calculating amounts of the distortion based on the differences of the electron beam positions. Method and apparatus are offered which correct distortion in a spectral image with high efficiency and high accuracy, the image being formed by the two orthogonal axes (the axis of the amount of energy loss and the axis of positional information).
    • 在由两个正交轴形成的光谱图像中,其中一个是能量损失量的轴,另一个是位置信息的轴,通过使用电子光谱仪和透射电子显微镜,在 通过比较从由两个正交轴形成的二维电子束位置图像计算的电子束位置(能量损失量的轴和能量损失的轴线),以高效率和高精度来校正要分析的样本的光谱图像 位置信息),以及基于电子束位置的差异计算失真量。 提供了以高效率和高精度校正光谱图像失真的方法和装置,该图像由两个正交轴(能量损失量的轴和位置信息的轴)形成。