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1. 发明授权

US06218465B1 Crosslinked elastomer and producing process thereof 失效
标题翻译：交联弹性体及其制备方法
公开(公告)号：US06218465B1
公开(公告)日：2001-04-17
申请号：US09031702
申请日：1998-02-27
申请人： Minoru Kobayashi , Minoru Aoki , Yoshinobu Asako , Akihiko Fukada , Hayato Ikeda
发明人： Minoru Kobayashi , Minoru Aoki , Yoshinobu Asako , Akihiko Fukada , Hayato Ikeda
IPC分类号： C08J510
CPC分类号： C08F290/126 , C08F290/12 , C08F290/14
摘要： For example, a blended composition is produced first by letting a monomer composition, mainly composed of alkyl (meth)acrylate and including a compound having a plurality of polymeric groups within a molecule, contain microscopic particles, such as carbon black, having an average primary particle size in a range between 1 nm and 200 nm, and then the blended composition is polymerized. Consequently, it has become possible to produce inexpensive crosslinked elastomer having excellent physical properties, such as small creep (low creep) in compression set, tensile elongation set, etc., and excellent mechanical strength, such as tensile break strength and tensile break elongation, in a simple procedure omitting the post-crosslinking step at a high-level productivity while saving energy and time spent in the kneading step.
摘要翻译：例如，首先通过使主要由（甲基）丙烯酸烷基酯组成的单体组合物，并且在分子内包含具有多个聚合基团的化合物包含具有平均初级的微观颗粒（例如炭黑）来制备共混组合物粒度在1nm和200nm之间的范围内，然后共混组合物聚合。因此，可以生产出具有优异的物理性能的低价交联弹性体，如压缩永久变形中的蠕变（蠕变低），拉伸伸长率设定等，以及拉伸断裂强度和拉伸断裂伸长率等优异的机械强度，以简单的方法省略了高级生产率的后交联步骤，同时节省了在捏合步骤中消耗的能量和时间。

2. 发明申请

US20070049655A1 Radiation-curable composition and cured product thereof 审中-公开
标题翻译：可辐射固化组合物及其固化产物
公开(公告)号：US20070049655A1
公开(公告)日：2007-03-01
申请号：US11509029
申请日：2006-08-24
申请人： Masanori Yoshimune , Yuichi Kawata , Akihiko Fukada
发明人： Masanori Yoshimune , Yuichi Kawata , Akihiko Fukada
IPC分类号： B29D11/00
CPC分类号： C08F222/1006
摘要： To provide a radiation-curable composition which can provide a cured product capable of sufficiently satisfying all of light resistance, transparency and curability and therefore can be useful in much more applications in addition to optical members, lighting members, and automobile members. A radiation-curable composition used after cured by radiation energy, wherein a cured product produced by curing the curable composition by radiation energy of 2 J/cm2 satisfies: an initial light transmittance of 80% or more at a wavelength of 380 nm, and a light transmittance retention of 90% or more after 200 hours of accelerated light resistance test.
摘要翻译：本发明提供能够提供能够充分满足耐光性，透明性，固化性的固化物的放射线固化性组合物，因此除了光学部件，照明部件以及汽车部件以外，还可以使用更多的应用。通过辐射能固化后使用的可辐射固化组合物，其中通过2J / cm 2的辐射能固化可固化组合物制备的固化产物满足：初始透光率为80％以上波长380nm，加速耐光试验200小时后的透光率保持率为90％以上。

3. 发明授权

US06887946B2 (Meth) acryloyl group-containing compound and method for producing the same 失效
标题翻译：（甲基）丙烯酰基化合物及其制造方法
公开(公告)号：US06887946B2
公开(公告)日：2005-05-03
申请号：US10284249
申请日：2002-10-31
申请人： Akihiko Fukada , Keiji Yurugi , Toshio Awaji , Nobuaki Otsuki
发明人： Akihiko Fukada , Keiji Yurugi , Toshio Awaji , Nobuaki Otsuki
IPC分类号： C07C67/29 , C07C67/04 , C07C69/54 , C08F2/46 , C08F8/02 , C08F220/18 , C08F299/02 , C08G59/14 , C08G63/91 , C08G65/332 , C08G85/00 , C09D4/02 , C08F220/02
CPC分类号： C07C67/04 , C07C67/29 , C07C69/60 , C07C69/54
摘要： It is an object of the present invention to provide a compound having a (meth)acryloyl group that is suitably used in various applications, a process for producing such compound simply and under mild conditions, and an useful photo-curable composition and aqueous photo-curable composition comprising such compound.The present invention is related to a process for producing a compound having a (meth)acryloyl group which comprises reacting a compound having both a (meth)acryloyl group and a vinyl ether group with a compound having at least two functional groups capable of an addition reaction with said vinyl ether group, and to a compound having a (meth)acryloyl group which is obtained by an addition reaction of a functional group of a compound (A) having at least two functional groups and the vinyl ether group of a compound (B) having both a (meth)acryloyl group and a vinyl ether group, said functional groups of said compound (A) being selected from the group consisting of a hydroxyl group, a carboxyl group and a thiol group.
摘要翻译：本发明的目的是提供一种适用于各种用途的具有（甲基）丙烯酰基的化合物，简单且温和的条件下制备该化合物的方法，以及有用的光固化性组合物和水性光固化性组合物，包含这种化合物的可固化组合物。本发明涉及一种具有（甲基）丙烯酰基的化合物的制备方法，该方法包括使具有（甲基）丙烯酰基和乙烯基醚基的化合物与具有至少两个能够加成的官能团的化合物反应与具有至少两个官能团的化合物（A）的官能团和化合物的乙烯基醚基的官能团（A）的加成反应获得的（甲基）丙烯酰基的化合物与所述乙烯基醚基反应， B）具有（甲基）丙烯酰基和乙烯基醚基的化合物，所述化合物（A）的所述官能团选自羟基，羧基和硫醇基。

4. 发明申请

US20050192373A1 Curable composition for optical parts 审中-公开
标题翻译：光学部件的固化组合物
公开(公告)号：US20050192373A1
公开(公告)日：2005-09-01
申请号：US11065329
申请日：2005-02-25
申请人： Toshio Awaji , Kaoru Mori , Akihiko Fukada , Masanori Yoshimune
发明人： Toshio Awaji , Kaoru Mori , Akihiko Fukada , Masanori Yoshimune
IPC分类号： C08F290/06 , C08F20/28 , C08F299/02 , G02B1/04 , C08G2/00 , C08F2/46
CPC分类号： G02B1/04 , C08L33/10 , C08L33/08 , C08L33/14
摘要： A curable composition for optical parts, including a (meth)acrylic acid ester (A) of a compound having two or more hydroxy groups in one molecule and containing no aromatic hydrocarbon structure, wherein a content of an ether structure represented by the following general formula (1): —(O—CH2—CHR1)n— (1) wherein n is in the range of 1 to 100 and R1 is at least one selected from the group consisting of hydrogen, methyl, and ethyl, in the composition is 5% by weight or higher, and a content of sulfonic acid and/or a sulfonic acid ester in the composition is 100 ppm or lower in terms of sulfur atom content. This curable composition makes it possible to obtain optical parts by curing, which are transparent and hardly cause coloration, denaturation, and deterioration to light from a light source having an emission wavelength distribution extending from a short wavelength region of visible light to an ultraviolet region.
摘要翻译：一种用于光学部件的可固化组合物，包括一分子中具有两个或多个羟基的化合物的（甲基）丙烯酸酯（A），其不含芳族烃结构，其中由以下通式表示的醚结构的含量（1）：<？in-line-formula description =“In-line Formulas”end =“lead”？> - （O-CH 2 - 其中n在1到100的范围内，而R 1 在组成中，选自氢，甲基和乙基的至少一种为5重量％以上，组合物中磺酸和/或磺酸酯的含量为100 ppm或更低的硫原子含量。该固化性组合物可以通过固化获得透明的光学部件，并且几乎不引起来自具有从可见光的短波长范围向紫外线区域延伸的发光波长分布的光源的光的着色，变性和劣化。

5. 发明授权

US06767980B2 Reactive diluent and curable resin composition 有权
标题翻译：活性稀释剂和可固化树脂组合物
公开(公告)号：US06767980B2
公开(公告)日：2004-07-27
申请号：US10125604
申请日：2002-04-19
申请人： Keiji Yurugi , Akihiko Fukada , Kenji Matsukawa
发明人： Keiji Yurugi , Akihiko Fukada , Kenji Matsukawa
IPC分类号： C08F22068
CPC分类号： C08F290/064 , C08F220/40 , C08F222/06 , C08F290/061 , C09D4/06 , C09D11/101 , C09D11/30 , C09D133/00
摘要： The present invention provides a reactive diluent composition which overcomes drawbacks of both the radical-cure and the cationic-cure reactive diluents and can be applied in a broad variety of uses such as paints, inks, adhesives, pressure sensitive adhesives, surface-modifiers, and molding materials; a curable resin composition containing the same; an activated energy ray-curable resin composition; and an activated energy ray-curable ink composition for ink-jet printing. A reactive diluent composition comprising a vinyl ether group-containing (meth)acrylic ester represented by the following general formula (1): CH2═CR1—COO—R2—O—CH═CH—R3 (1) wherein R1 represents a hydrogen atom or a methyl group; R2 represents an organic residue of 2 to 20 carbon atoms; R3 represents a hydrogen atom or an organic residue of 1 to 11 carbon atoms and a hydroxyl group-containing polymerizable compound and/or divinyl ether.
摘要翻译：本发明提供一种反应性稀释剂组合物，其克服了自由基固化和阳离子固化反应性稀释剂的缺点，并且可以应用于各种用途，例如油漆，油墨，粘合剂，压敏粘合剂，表面改性剂，和成型材料; 含有该固化性树脂组合物的固化性树脂组合物; 活性能量射线固化树脂组合物; 以及用于喷墨印刷的活性能量射线固化型油墨组合物。1.一种反应性稀释剂组合物，其包含由以下通式（1）表示的含乙烯基醚基的（甲基）丙烯酸酯：其中R 1表示氢原子或甲基; R 2表示2〜20个碳原子的有机残基; R 3表示氢原子或1〜11个碳原子的有机残基和含有羟基的聚合性化合物和/或二乙烯基醚。

6. 发明授权

US06191229B1 (Meth)acryl syrup, method of manufacturing the same, and method of manufacturing molding material including the same 失效
标题翻译：（甲基）丙烯酸树脂浆，其制造方法，以及包含该组合物的成型材料的制造方法
公开(公告)号：US06191229B1
公开(公告)日：2001-02-20
申请号：US08849612
申请日：1997-06-04
申请人： Masazumi Sasabe , Akihiko Fukada , Keiichiro Mizuta
发明人： Masazumi Sasabe , Akihiko Fukada , Keiichiro Mizuta
IPC分类号： C08F26504
CPC分类号： C08F8/46 , C08F2800/20 , C08F220/14
摘要： The present invention provides (meth)acryl syrup which shows excellent storage stability as a molding material, and also provides a method of manufacturing the (meth)acryl syrup in a shorter period of time compared with the conventional method, and a molding material which permits a molded article having excellent heat-resistance, solvent-resistance, weathering resistance, and water-resistance, etc., to be manufactured. The (meth)acryl syrup is manufactured, for example, by polymerizing a monomer component including (meth)acrylic ester and a vinyl monomer having a carboxyl group in a presence of a thiol compound, and subsequently processing the reaction mixture with maleic anhydride and a basic compound. The molding material includes the (meth)acryl syrup, and may also include a thickening agent, derivatives of succinic acid, a reinforcing material, etc.
摘要翻译：本发明提供作为成型材料具有优异的储存稳定性的（甲基）丙烯酸树脂浆料，并且还提供了与常规方法相比在较短时间内制备（甲基）丙烯酸树脂浆料的方法，以及允许具有优异的耐热性，耐溶剂性，耐候性，耐水性等的成型品。（甲基）丙烯酸树脂浆是通过在硫醇化合物的存在下聚合包含（甲基）丙烯酸酯和具有羧基的乙烯基单体的单体组分，然后将马来酸酐和基本化合物。成型材料包括（甲基）丙烯酸树脂浆，还可以包括增稠剂，琥珀酸衍生物，增强材料等。

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