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1. 发明授权

US4294940A Resin composition for electrocoating 失效
标题翻译：用于电涂的树脂组合物
公开(公告)号：US4294940A
公开(公告)日：1981-10-13
申请号：US110688
申请日：1980-01-09
申请人： Minoru Hino , Takao Oshima , Kazuo Hayatsu , Michio Yamamoto , Seimei Yasui
发明人： Minoru Hino , Takao Oshima , Kazuo Hayatsu , Michio Yamamoto , Seimei Yasui
IPC分类号： C08G18/08 , C08G18/69 , C08G18/80 , C09D5/44 , C08G18/62 , C25D13/06
CPC分类号： C09D5/4403 , C08G18/0814 , C08G18/694 , C08G18/696 , C08G18/8061 , C09D5/4434 , Y10S524/901
摘要： A resin composition for electrocoating which comprises(I) a reaction product (G) of an epoxy compound (E), optionally an epoxy group-modifying agent (F) and a partially esterified and/or partially amidated product (D) which is obtained by partially esterifying and/or partially amidating an adduct (A) of a conjugated diene polymer with an .alpha.,.beta.-unsaturated dicarboxylic acid or its anhydride with an alcoholic hydroxy group-containing compound (B) and/or a primary or secondary monoamine (C), respectively, and(II) a completely blocked organic polyisocyanate,said mixture of the reaction product (G) and the completely blocked organic polyisocyanate being neutralized, ora neutralized product of an adduct (H) of the reaction product (G) with a partially blocked organic polyisocyanate.The resin composition is applicable to electrocoating, particularly cathodic electrocoating, and hence, is useful for electrocoating of steel products, particularly for electrocoating of automobiles.
摘要翻译：一种用于电泳的树脂组合物，其包含（I）环氧化合物（E）的反应产物（G），任选的环氧基改性剂（F）和部分酯化和/或部分酰胺化的产物（D），其获得通过用α，β-不饱和二羧酸或其酸酐与含醇羟基的化合物（B）和/或伯或仲单胺部分酯化和/或部分酰化共轭二烯聚合物的加合物（A）（C），和（II）完全封闭的有机多异氰酸酯，反应产物（G）和完全封闭的有机多异氰酸酯的混合物被中和，或反应产物（G）的加合物（H）的中和产物，与部分封闭的有机多异氰酸酯。该树脂组合物可用于电泳，特别是阴极电泳涂覆，因此可用于钢制品的电涂，特别是用于汽车电涂层。

2. 发明授权

US4463134A Modified epoxy resin composition 失效
标题翻译：改性环氧树脂组合物
公开(公告)号：US4463134A
公开(公告)日：1984-07-31
申请号：US333453
申请日：1981-12-22
申请人： Minoru Hino , Takao Oshima , Akihiro Tachibana
发明人： Minoru Hino , Takao Oshima , Akihiro Tachibana
IPC分类号： C08G59/00 , C08C19/36 , C08F8/14 , C08F8/30 , C08F8/32 , C08F8/46 , C08G59/10 , C08G59/14 , C08G59/40 , C08G59/50 , C08L63/00 , C08F36/06 , C08F279/02 , C08L63/02
CPC分类号： C08G59/50 , C08C19/36 , C08G59/10 , C08L63/00 , Y10S525/911
摘要： Modified epoxy resin compositions having excellent flexibility and excellent compatibility with conventional epoxy resins as well as exhibiting the original properties of the epoxy resin before being modified such as mechanical strength, adhesion, heat resistance are disclosed and chemical resistance, which are obtained by treating an epoxy resin with at least one modified adduct [D] of a conjugated diene polymer or copolymer which has an imido bond and/or amido bond and a semi-ester structure and has an acid value owing to a free carboxyl group of 5 to 100. The modified adduct is obtained by reacting an adduct [A] of a polymer of a conjugated diene having a number average molecular weight of 300 to 20,000 or a copolymer of the conjugated diene and a vinyl monomer with an .alpha.,.beta.-unsaturated dicarboxylic acid or its anhydride, with a compound [B] containing one primary amino group in the molecule and a compound [C] containing a hydroxy group in the molecule.
摘要翻译：公开了具有优异的柔性和与常规环氧树脂的良好相容性的改性环氧树脂组合物，以及在改性之前表现出环氧树脂的原始性能，例如机械强度，粘合性，耐热性，并且通过处理环氧树脂具有至少一种具有酰亚胺键和/或酰胺键和半酯结构并且由于游离羧基为5至100具有酸值的共轭二烯聚合物或共聚物的至少一种改性加合物[D]的树脂。通过使数均分子量为300〜20,000的共轭二烯的聚合物的加合物[A]或共轭二烯与乙烯基单体的共聚物与α，β-不饱和二羧酸或其酸酐与分子中含有一个伯氨基的化合物[B]和分子中含有羟基的化合物[C]反应。

3. 发明授权

US4371665A Modified epoxy resin composition 失效
标题翻译：改性环氧树脂组合物
公开(公告)号：US4371665A
公开(公告)日：1983-02-01
申请号：US333454
申请日：1981-12-22
申请人： Minoru Hino , Takao Oshima
发明人： Minoru Hino , Takao Oshima
IPC分类号： C08G59/00 , C08C19/36 , C08F8/14 , C08F8/30 , C08F8/32 , C08F8/46 , C08G59/10 , C08G59/14 , C08G59/40 , C08G59/50 , C08L63/00
CPC分类号： C08G59/50 , C08C19/36 , C08G59/10 , C08L63/00
摘要： Modified epoxy resin composition having excellent flexibility and excellent compatibility with conventional epoxy resins as well as the original properties of the epoxy resin before modified such as mechanical strength, adhesion, heat resistance and chemical resistance, which is obtained by treating an epoxy resin with at least one modified adduct [D] of a conjugated diene polymer or copolymer which has an imido bond and/or amido bond and a semi-ester structure and has an acid value owing to a free carboxyl group of 5 to 100, said modified adduct being obtained by reacting an adduct [A] of a polymer of a conjugated diene having a number average molecular weight of 300 to 20,000 or a copolymer of the conjugated diene and a vinyl monomer with an .alpha.,.beta.-unsaturated dicarboxylic acid or its anhydride, with a compound [B] of the formula: ##STR1## and a compound [C] of the formula:R.sub.3 --CH.sub.2).sub.m OH [II].
摘要翻译：改性环氧树脂组合物具有优异的柔韧性和与常规环氧树脂的优异相容性以及环氧树脂在改性之前的原始性能，如机械强度，粘合性，耐热性和耐化学性，其通过至少处理环氧树脂具有酰亚胺键和/或酰胺键和半酯结构并且由于游离羧基的酸值为5〜100的共轭二烯聚合物或共聚物的一种改性加合物[D]，所述改性加合物得到通过使数均分子量为300〜20,000的共轭二烯的聚合物的加合物[A]或共轭二烯与乙烯基单体的共聚物与α，β-不饱和二羧酸或其酸酐反应，具有下式的化合物[B]：[I]和式：R 3 -CH 2）m OH [II]的化合物[C]。

4. 发明授权

US4178186A Resin for coatings 失效
标题翻译：涂料用树脂
公开(公告)号：US4178186A
公开(公告)日：1979-12-11
申请号：US655530
申请日：1976-02-05
申请人： Seimei Yasui , Minoru Hino
发明人： Seimei Yasui , Minoru Hino
IPC分类号： C08F8/00 , C08C19/28 , C08C19/36 , C08F8/32 , C08F8/46 , C09D11/00 , C09D11/10 , C09D11/106 , C09D11/108 , C09D121/00 , C09D11/02
CPC分类号： C08C19/36 , C08C19/28
摘要： A resin for coatings, particularly useful as a medium for printing inks and paints, comprising a modified polymer produced by adding at least one .alpha.,.beta.-unsaturated dicarboxylic acid or anhydride thereof to at least one liquid conjugated diolefinic polymer having a number average molecular weight of 150 to 3,000, a viscosity of 2 to 5,000 cps at 30.degree. C. and at least 50% of cis-1,4 structure and subjecting the resulting adduct to imidation or diamidation with at least one amine having 1 to 27 carbon atoms and whereby the total amine value of the resulting modified polymer being made not more than 3.
摘要翻译：用于涂料的树脂，特别用作印刷油墨和油漆的介质，其包含通过将至少一种α，β-不饱和二羧酸或其酸酐加成至少一种具有数均分子量的液体共轭二烯烃聚合物而制备的改性聚合物在30℃下粘度为2至5,000cps，并且至少50％为顺式-1,4结构，并将所得加合物用至少一种具有1至27个碳原子的胺进行酰亚胺化或二酰亚胺化，以及由此得到的改性聚合物的总胺值不大于3。

5. 发明授权

US4162240A Process for production of novel polymer emulsion 失效
标题翻译：生产新型聚合物乳液的方法
公开(公告)号：US4162240A
公开(公告)日：1979-07-24
申请号：US815263
申请日：1977-07-13
申请人： Minoru Hino , Seimei Yasui , Akira Shintani
发明人： Minoru Hino , Seimei Yasui , Akira Shintani
IPC分类号： C08C19/36 , C08F2/24 , C08F279/02 , C08F299/04 , C08G63/553 , C09D167/06
CPC分类号： C08G63/553 , C08C19/36 , C08F279/02 , C08F299/0414 , C09D167/06
摘要： A process for production of a polymer emulsion comprising polymerizing at least one partially esterified, imidated or amidated product of an adduct with a compound having a polymerizable unsaturated group and a hydroxy group, epoxy group or amino group, in an aqueous system in the presence or absence of a vinyl monomer, said adduct being produced by adding an .alpha.,.beta.-unsaturated dicarboxylic acid or anhydride thereof to at least one compound selected from the group consisting of a synthetic unsaturated polymer having a number average molecular weight of 150 to 30,000 and an iodine value of 50 to 500, a natural drying oil, a natural semidrying oil and an unsaturated fatty acid which composes the natural drying or semidrying oils. The polymer emulsion shows excellent coating film properties when used for paints.
摘要翻译：一种制备聚合物乳液的方法，其包括在水性体系中在存在或不存在下在水性体系中聚合至少一种部分酯化，酰亚胺化或酰胺化的加合物与具有可聚合不饱和基团和羟基，环氧基或氨基的化合物，或不存在乙烯基单体，所述加合物是通过向选自数均分子量为150至30,000的合成不饱和聚合物和至少一种数均分子量为150至30,000的化合物中的至少一种化合物加入α，β-不饱和二羧酸或其酸酐而制备的，碘值为50〜500，天然干性油，天然半干油和不饱和脂肪酸组成天然干燥或半干油。当用于涂料时，聚合物乳液显示出优异的涂膜性能。

6. 发明授权

US4094836A Aqueous alkyd resins 失效
标题翻译：水性醇酸树脂
公开(公告)号：US4094836A
公开(公告)日：1978-06-13
申请号：US785699
申请日：1977-04-07
申请人： Seimei Yasui , Minoru Hino , Kazuya Hayashi
发明人： Seimei Yasui , Minoru Hino , Kazuya Hayashi
IPC分类号： C08G63/553 , C09D11/10 , C09D167/08 , C09D3/52 , C09D3/66 , C09D5/02
CPC分类号： C09D11/105 , C08G63/553 , C09D167/08
摘要： An aqueous alkyd resin obtained by the neutralization of a polycondensation resin with a base, the polycondensation resin being prepared by reacting a reaction mixture obtained by the transesterification or esterification of (a) a natural fat and oil or a fatty acid with a polyhydric alcohol with an adduct of (b) a liquid polybutadiene having a number average molecular weight of 150 to 900, a viscosity of 2 to 80 cps. at 30.degree. C and at least 50% of the cis-1,4 structure with an .alpha.,.beta.-unsaturated dicarboxylic acid or the anhydride thereof, and/or the half-ester of said adduct, and with (c) an aromatic polycarboxylic acid or the anhydride thereof, and the polycondensation resin having free carboxyl groups in the amount corresponding to an acid value of 30 to 70 and containing 5 to 50% by weight of the component (b). This alkyd shows excellent coating film properties when used for water-base paints, printing inks and the like.
摘要翻译：通过用碱中和缩聚树脂获得的醇酸树脂水溶液，所述缩聚树脂通过使（a）天然油脂或脂肪酸与多元醇的酯交换或酯化得到的反应混合物与（b）数均分子量为150〜900，粘度为2〜80cps的液体聚丁二烯的加合物。在30℃和至少50％的具有α，β-不饱和二羧酸或其酸酐的顺式-1,4结构和/或所述加合物的半酯，和（c）芳族多元羧酸酸或其酸酐，和具有对应于酸值为30〜70的量且含有5〜50重量％的组分（b）的游离羧基的缩聚树脂。当用于水性涂料，印刷油墨等时，该醇酸树脂具有优异的涂膜性能。

7. 发明授权

US4725338A Purification process of polymerization solvent 失效
标题翻译：聚合溶剂的纯化过程
公开(公告)号：US4725338A
公开(公告)日：1988-02-16
申请号：US832412
申请日：1986-02-24
申请人： Tadashi Asanuma , Tatuo Ohoka , Minoru Hino , Nobutaka Uchikawa
发明人： Tadashi Asanuma , Tatuo Ohoka , Minoru Hino , Nobutaka Uchikawa
IPC分类号： C08F2/00 , B01D3/40 , C08F6/00 , C08F6/06 , C08F10/00 , B01D3/34
CPC分类号： B01D3/40 , Y10S203/06 , Y10S203/09 , Y10S203/20 , Y10S526/912
摘要： A process for purifying a solvent suitable for use in the polymerization of an olefin in the presence of a Ziegler-Natta catalyst, which comprises feeding the polymerization solvent to a stage lower than a chimney tray of a multi-stage distillation column, said chimney tray being provided at a height between the top and bottom of the column, feeding an organoaluminum compound to a stage higher than the chimney tray, drawing out a condensate from the chimney tray, heating the condensate to produce heated vapor, introducing the heated vapor to the chimney tray or to a stage higher than the chimney tray but lower than the stage to which the organoaluminum compound has been fed, and drawing the solvent in a purified state from the top.
摘要翻译：一种在齐格勒 - 纳塔催化剂存在下纯化适用于烯烃聚合的溶剂的方法，该方法包括将聚合溶剂进料到比多级蒸馏塔的烟囱式塔板低的阶段，所述烟囱式塔板提供在塔的顶部和底部之间的高度，将有机铝化合物供给到高于烟囱托盘的台阶上，从烟囱托盘抽出冷凝物，加热冷凝物以产生加热的蒸汽，将加热的蒸气引入到烟囱式塔板或高于烟囱式塔架但比有机铝化合物进料的阶段低的阶段，并从顶部抽出处于纯化状态的溶剂。

8. 发明授权

US4252727A Esters of an adduct of diolefinic polymer and unsaturated dicarboxylic compound 失效
标题翻译：二烯烃聚合物和不饱和二羧酸化合物的加成物的酯
公开(公告)号：US4252727A
公开(公告)日：1981-02-24
申请号：US655531
申请日：1976-02-05
申请人： Seimei Yasui , Minoru Hino , Kunio Izumi , Otsugu Hayashi
发明人： Seimei Yasui , Minoru Hino , Kunio Izumi , Otsugu Hayashi
IPC分类号： C08F8/00 , C08C19/28 , C08C19/36 , C08F8/14 , C08F8/46 , C09D11/00 , C09D11/10 , C09D11/106 , C09D11/108 , C09D121/00 , C07C69/34 , C07C69/347
CPC分类号： C08C19/28 , C08C19/36
摘要： A resin for coatings, particularly useful as a medium for printing inks and paints, comprising a modified polymer produced by adding at least one .alpha.,.beta.-unsaturated dicarboxylic acid or anhydride thereof to at least one liquid conjugated diolefinic polymer having a number average molecular weight of 150 to 3,000, a viscosity of 2 to 5,000 cps at 30.degree. C. and at least 50% of cis-1,4 structure and subjecting the resulting adduct to diesterification with at least one alcohol having 1 to 27 carbon atoms and whereby the acid value owing to the carboxyl group or the carboxylic anhydride group of the resulting modified polymer being made not more than 10.
摘要翻译：用于涂料的树脂，特别用作印刷油墨和油漆的介质，其包含通过将至少一种α，β-不饱和二羧酸或其酸酐加成至少一种具有数均分子量的液体共轭二烯烃聚合物而制备的改性聚合物在30℃下的粘度为2至5,000cps，并且至少50％为顺式-1,4结构，并将所得加合物用至少一种具有1至27个碳原子的醇进行二酯化，由于所得改性聚合物的羧基或羧酸酐基产生的酸值不大于10。

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