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1. 发明申请

US20120061615A1 Rare Earth Ion Doped Silicate Luminescence Glass and Preparation Method Thereof 有权
标题翻译：稀土离子掺杂硅酸盐发光玻璃及其制备方法
公开(公告)号：US20120061615A1
公开(公告)日：2012-03-15
申请号：US13320753
申请日：2009-05-19
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qiao , Qingtao Li
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qiao , Qingtao Li
IPC分类号： C09K11/79
CPC分类号： C03C4/12 , C03C3/062 , C03C3/095
摘要： A rare earth ion doped silicate luminescence glass and preparation method thereof are provided. The luminescence glass is the material with the following formula: aM2O.bM′2O3.cSiO2.dRE2O3, wherein M is at least one of Na, K and Li, M′ is at least one of Y, Gd, La, Sc and Lu, RE is at least one of Ce, Tm, Tb, Ho, Dy, Er, Nd, Sm, Eu and Pr. The preparation method is: grinding the raw material until mixed uniformly, calcining the raw material at 1200-1500° C. for 1-5 h, cooling to room temperature, annealing at 600-1100° C. for 0.5-24 h, cooling to room temperature again, molding then getting the product. The performance of the product is stable. The product is homogenous, and the luminescence performance is good. The light transmittance is high. The process of the preparation method is simple and with low cost.
摘要翻译：提供了一种稀土离子掺杂硅酸盐发光玻璃及其制备方法。发光玻璃是具有下式的材料：aM2O.bM'2O3.cSiO2.dRE2O3，其中M是Na，K和Li中的至少一种，M'是Y，Gd，La，Sc和Lu中的至少一种，RE为Ce，Tm，Tb，Ho，Dy，Er，Nd，Sm，Eu和Pr中的至少一种。制备方法为：研磨原料直至混合均匀，在1200-1500℃下煅烧原料1-5小时，冷却至室温，在600-1100℃退火0.5-24小时，冷却再到室温，成型然后得到产品。产品性能稳定。产品均匀，发光性能好。透光率高。制备方法简单，成本低。

2. 发明授权

US08925349B2 Rare earth ion doped silicate luminescence glass and preparation method thereof 有权
标题翻译：稀土离子掺杂硅酸盐发光玻璃及其制备方法
公开(公告)号：US08925349B2
公开(公告)日：2015-01-06
申请号：US13320753
申请日：2009-05-19
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qiao , Qingtao Li
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qiao , Qingtao Li
IPC分类号： C03C3/095 , C03C6/04 , C03B32/00 , C03C4/12 , C03C3/062
CPC分类号： C03C4/12 , C03C3/062 , C03C3/095
摘要： A rare earth ion doped silicate luminescence glass and preparation method thereof are provided. The luminescence glass is the material with the following formula: aM2O.bM′2O3.cSiO2.dRE2O3, wherein M is at least one of Na, K and Li, M′ is at least one of Y, Gd, La, Sc and Lu, RE is at least one of Ce, Tm, Tb, Ho, Dy, Er, Nd, Sm, Eu and Pr. The preparation method is: grinding the raw material until mixed uniformly, calcining the raw material at 1200-1500° C. for 1-5 h, cooling to room temperature, annealing at 600-1100° C. for 0.5-24 h, cooling to room temperature again, molding then getting the product. The performance of the product is stable. The product is homogenous, and the luminescence performance is good. The light transmittance is high. The process of the preparation method is simple and with low cost.
摘要翻译：提供了一种稀土离子掺杂硅酸盐发光玻璃及其制备方法。发光玻璃是具有下式的材料：aM2O.bM'2O3.cSiO2.dRE2O3，其中M是Na，K和Li中的至少一种，M'是Y，Gd，La，Sc和Lu中的至少一种，RE为Ce，Tm，Tb，Ho，Dy，Er，Nd，Sm，Eu和Pr中的至少一种。制备方法为：研磨原料直至混合均匀，在1200-1500℃下煅烧原料1-5小时，冷却至室温，在600-1100℃退火0.5-24小时，冷却再到室温，成型然后得到产品。产品性能稳定。产品均匀，发光性能好。透光率高。制备方法简单，成本低廉。

3. 发明授权

US08592333B2 Green light-emitting glass and method of preparing the same 有权
标题翻译：绿色发光玻璃及其制备方法
公开(公告)号：US08592333B2
公开(公告)日：2013-11-26
申请号：US13257314
申请日：2009-03-25
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qiao , Qingtao Li
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qiao , Qingtao Li
IPC分类号： C03C3/095 , C03C4/12 , C03B25/00 , C09K11/78 , C09K11/79
CPC分类号： C09K11/7774 , C03C3/095 , C03C4/12
摘要： A green light-emitting glass and the method of preparing the same are provided. The components with parts by mole of the green light-emitting glass are alkali oxide 25-40, Y2O3 0.01-15, SiO2 40-70, Tb2O3 0.01-15. The method of preparing the glass includes mixing alkali salt with Y2O3, SiO2 and Tb4O7, firing the mixture at 1200° C.-1500° C. for 1-5 hours, cooling the precursor to the room temperature and annealing the precursor in a reducing atmosphere at 600° C.-1200° C. for 1-20 hours. A green light-emitting glass with good transparence, high uniformity, easily being made into big bulk and high stability is provided. The process of capsulation of parts by using the glass is simple. And a method of preparing the glass with simple process and low cost is provided.
摘要翻译：提供绿色发光玻璃及其制备方法。具有摩尔比的绿色发光玻璃的组分是碱金属氧化物25-40，Y2O3 0.01-15，SiO2 40-70，Tb2O3 0.01-15。制备玻璃的方法包括将碱金属盐与Y 2 O 3，SiO 2和Tb 4 O 7混合，将混合物在1200℃-1500℃下烧制1-5小时，将前体冷却至室温，并在还原气氛在600℃-1200℃下保持1-20小时。提供透明性好，均匀性好，容易制成大体积，高稳定性的绿色发光玻璃。通过使用玻璃来封装部件的过程很简单。并提供了一种以简单的工艺和低成本制备玻璃的方法。

4. 发明申请

US20130001444A1 WHITE LIGHT LUMINESCENT DEVICE BASED ON PURPLE LIGHT LEDS 审中-公开
标题翻译：基于紫外光LED的白光发光装置
公开(公告)号：US20130001444A1
公开(公告)日：2013-01-03
申请号：US13514959
申请日：2009-12-31
申请人： Mingjie Zhou , Wenbo Ma , Yanbo Qiao , Zhaopu Shi , Qingtao Li
发明人： Mingjie Zhou , Wenbo Ma , Yanbo Qiao , Zhaopu Shi , Qingtao Li
IPC分类号： F21V9/16 , G21K5/00
CPC分类号： C09K11/7734 , C03C14/006 , C03C17/22 , C03C2214/16 , F21V3/061 , F21V3/12 , F21V9/30 , F21Y2115/10 , H01L25/0753 , H01L33/507 , H01L2924/0002 , Y02B20/181 , H01L2924/00
摘要： The present invention relates to a white light luminescent device based on purple light LED. The white light luminescent device includes a housing, a support plate, at least one purple light LED semiconductor light source, and a piece of high silica luminescent glass. The support plate is received in the housing. The at least one purple light LED semiconductor light source is positioned on the support plate. The piece of high silica luminescent glass doped with Eu ions is opposite to the purple light LED semiconductor light source. One surface of the high silica luminescent glass away from the purple light LED semiconductor light source is coated with a phosphor layer formed with a selection from a mixture of yellow phosphor and red phosphor, a mixture of green phosphor and red phosphor, and yellow phosphor.
摘要翻译：本发明涉及一种基于紫光LED的白光发光装置。白光发光装置包括壳体，支撑板，至少一个紫色LED半导体光源和高二氧化硅发光玻璃片。支撑板被容纳在壳体中。至少一个紫光LED半导体光源位于支撑板上。掺有Eu离子的高二氧化硅发光玻璃与紫光LED半导体光源相反。远离紫色LED半导体光源的高二氧化硅发光玻璃的一个表面涂覆有由黄色荧光体和红色荧光体的混合物，绿色荧光体和红色荧光体的混合物以及黄色荧光体形成的荧光体层。

5. 发明申请

US20120010067A1 Green Light-Emitting Glass and Method of Preparing the Same 有权
标题翻译：绿色发光玻璃及其制备方法
公开(公告)号：US20120010067A1
公开(公告)日：2012-01-12
申请号：US13257314
申请日：2009-03-25
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qia , Qingtao Li
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi , Yanbo Qia , Qingtao Li
IPC分类号： C03C3/095 , C03B37/00
CPC分类号： C09K11/7774 , C03C3/095 , C03C4/12
摘要： A green light-emitting glass and the method of preparing the same are provided. The components with parts by mole of the green light-emitting glass are alkali oxide 25-40, Y2O3 0.01-15, SiO2 40-70, Tb2O3 0.01-15. The method of preparing the glass includes mixing alkali salt with Y2O3, SiO2 and Tb4O7, firing the mixture at 1200° C-1500° C. for 1-5 hours, cooling the precursor to the room temperature and annealing the precursor in a reducing atmosphere at 600° C-1200° C. for 1-20 hours. A green light-emitting glass with good transparence, high uniformity, easily being made into big bulk and high stability is provided. The process of capsulation of parts by using the glass is simple. And a method of preparing the glass with simple process and low cost is provided.
摘要翻译：提供绿色发光玻璃及其制备方法。具有摩尔比的绿色发光玻璃的组分是碱金属氧化物25-40，Y2O3 0.01-15，SiO2 40-70，Tb2O3 0.01-15。制备玻璃的方法包括将碱金属盐与Y 2 O 3，SiO 2和Tb 4 O 7混合，将混合物在1200℃-1500℃下烧制1-5小时，将前体冷却至室温并在还原气氛中退火前体在600℃-1200℃下保持1-20小时。提供透明性好，均匀性好，容易制成大体积，高稳定性的绿色发光玻璃。通过使用玻璃来封装部件的过程很简单。并提供了一种以简单的工艺和低成本制备玻璃的方法。

6. 发明申请

US20120091394A1 BLUE LIGHT EMITTING GLASS AND PREPARATION METHOD THEREOF 有权
标题翻译：蓝光发光玻璃及其制备方法
公开(公告)号：US20120091394A1
公开(公告)日：2012-04-19
申请号：US13377569
申请日：2009-06-25
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
IPC分类号： C09K11/79 , C03B32/00
CPC分类号： C03C3/095 , C03B32/00 , C03C3/062 , C03C4/12 , C09K11/7721
摘要： Blue light emitting glass and the preparation method thereof are provided. The blue light emitting glass has the following composition: aCaO.bAl2O3.cSiO2.xCeO2, wherein a, b, c and x are, by mol part, 15-55, 15-35, 20-60 and 0.01-5 respectively. The preparation method comprises: weighing the raw materials according to the composition of the blue light emitting glass; mixing the raw materials uniformly and melting the raw materials to obtain glass melt; moulding the glass melt to obtain transparent glass; thermally treating the transparent glass under reducing atmosphere, and thereafter obtaining the finished product. The blue light emitting glass obtained has intense broadband excitation spectrum in ultraviolet region and emits intense blue light under the excitation of ultraviolet light. It is suitable for using as luminescent medium material.
摘要翻译：提供蓝色发光玻璃及其制备方法。蓝色发光玻璃具有以下组成：aCaO.bAl2O3.cSiO2.xCeO2，其中a，b，c和x分别为15-55,15-35,20-60和0.01-5。制备方法包括：根据蓝色发光玻璃的成分称量原料; 均匀混合原料，熔化原料，得到玻璃熔体; 将玻璃熔体成型得到透明玻璃; 在还原气氛下对透明玻璃进行热处理，然后得到成品。获得的蓝色发光玻璃在紫外线区域具有强烈的宽带激发光谱，并在紫外光的激发下发出强烈的蓝光。适合用作发光介质材料。

7. 发明申请

US20120199791A1 BISMUTH ION SENSITIZED RARE EARTH GERMANATE LUMINESCENCE MATERIALS AND PREPARATION METHODS THEREOF 有权
标题翻译： BISMUTH离子敏感稀土地球化学发光材料及其制备方法
公开(公告)号：US20120199791A1
公开(公告)日：2012-08-09
申请号：US13501596
申请日：2009-10-12
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
IPC分类号： C09K11/78
CPC分类号： C09K11/7775 , C09K11/7793
摘要： Bismuth ion sensitized rare earth germanate luminescence materials and preparation methods are disclosed. The luminescence materials are the compounds of the following general formula (Y1-x-y-zAxBiyLnz)2GeO5. The preparation methods comprise: using oxides, carbonates, oxalates, acetates, nitrates or halides of Y, A, Bi, Ln and Ge as raw materials, wherein A is one of Gd, Lu, Sc and La, and Ln is at least one of Tm, Ho, Sm, Tb, Eu and Dy, homogeneously grinding the raw materials, sintering at 1300-1500° C. for 6-24 h, and then cooling them to room temperature to obtain the bismuth ion sensitized rare earth germanate luminescence materials.
摘要翻译：公开了铋离子敏化稀土锗酸盐发光材料及制备方法。发光材料是以下通式（Y1-x-y-zAxBiyLnz）2GeO5的化合物。制备方法包括：以Y，A，Bi，Ln和Ge为原料的氧化物，碳酸盐，草酸盐，乙酸盐，硝酸盐或卤化物为原料，其中A为Gd，Lu，Sc和La之一，Ln为至少一种的Tm，Ho，Sm，Tb，Eu和Dy，对原材料进行均匀研磨，在1300-1500℃下烧结6〜24h，然后冷却至室温，得到铋离子增感稀土锗酸盐发光材料

8. 发明申请

US20120132856A1 OXIDE LUMINESCENT MATERIALS ACTIVATED BY TRIVALENT THULIUM AND THEIR PREPARATIONS 有权
标题翻译：由多晶硅及其制备物质活化的氧化物发光材料
公开(公告)号：US20120132856A1
公开(公告)日：2012-05-31
申请号：US13254860
申请日：2009-03-06
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
IPC分类号： C09K11/78
CPC分类号： C09K11/7767
摘要： The present invention relates to oxide luminescent materials activated by trivalent thulium and their preparations. The luminescent materials are the compounds with the following general formula: (RE1-xTmx)2O3, wherein a range of x is 0
摘要翻译：本发明涉及三价铯活化的氧化物发光材料及其制备方法。发光材料是具有以下通式的化合物：（RE1-xTmx）2O3，其中x的范围为0

9. 发明申请

US20120056130A1 FULL-COLOR LIGHT-EMITTING MATERIAL AND PREPARATION METHOD THEREOF 有权
标题翻译：全彩色发光材料及其制备方法
公开(公告)号：US20120056130A1
公开(公告)日：2012-03-08
申请号：US13319336
申请日：2009-05-11
申请人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
发明人： Mingjie Zhou , Wenbo Ma , Zhaopu Shi
IPC分类号： C09K11/66
CPC分类号： C09K11/7793 , C09K11/7775
摘要： A full-color light-emitting material and preparation method thereof are provided. A light-emitting material is following general formula compound (Y1-x-y-zAxByCz)2GeO5, wherein 0
摘要翻译：提供了全色发光材料及其制备方法。发光材料是以下通式化合物（Y1-xy-zAxByCz）2GeO5，其中0

10. 发明申请

US20130119313A1 SILICATE FLUORESCENT MATERIAL AND PREPARATION METHOD THEREOF 审中-公开
标题翻译：硅酸盐荧光材料及其制备方法
公开(公告)号：US20130119313A1
公开(公告)日：2013-05-16
申请号：US13811859
申请日：2010-07-28
申请人： Mingjie Zhou , Wenbo Ma , Yanbo Qiao
发明人： Mingjie Zhou , Wenbo Ma , Yanbo Qiao
IPC分类号： C09K11/77
CPC分类号： C09K11/7774 , C09K11/873
摘要： A silicate fluorescent material is provided. The general chemical formula of the luminescent material is Ln2SiO5:Tb, M, wherein Ln represents at least one of the elements selected from Y, Gd, La or Lu, M represents at least one of the nanoparticles selected from Ag, Au, Os, Ir, Pt, Ru, Rh or Pd, the mole ratio of Tb to Ln is greater than 0 but not greater than 0.25. The porous glass containing metal nanoparticles is prepared by introducing metal nano ions into the porous glass and extracting the uniformly dispersed metal nanoparticles from the porous glass via a chemical reduction method. A silicate fluorescent material with enhanced luminescence is obtained by substituting SiO2 which is the raw material in the process for preparing the silicate fluorescent material via the conventional high temperature solid phase sintering with the porous glass containing metal nanoparticles. The performance of the silicate fluorescent material is better and the light emitting efficiency of the silicate fluorescent material is higher compared with the conventional silicate fluorescent material.
摘要翻译：提供硅酸盐荧光材料。发光材料的一般化学式为Ln2SiO5：Tb，M，其中Ln表示选自Y，Gd，La或Lu中的至少一种元素，M表示选自Ag，Au，Os， Ir，Pt，Ru，Rh或Pd，Tb与Ln的摩尔比大于0但不大于0.25。通过将金属纳米离子引入多孔玻璃中并通过化学还原法从多孔玻璃中提取均匀分散的金属纳米粒子来制备含金属纳米颗粒的多孔玻璃。通过用含有金属纳米颗粒的多孔玻璃的常规高温固相烧结来代替通过常规高温固相烧结制备硅酸盐荧光材料的方法中的原料SiO 2来获得具有增强发光的硅酸盐荧光材料。与传统的硅酸盐荧光材料相比，硅酸盐荧光材料的性能更好，硅酸盐荧光材料的发光效率更高。

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