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1. 发明申请

US20140194637A1 A-OLEFIN OLIGOMER AND PRODUCTION METHOD THEREOF 审中-公开
标题翻译： A-OLEFIN低聚物及其生产方法
公开(公告)号：US20140194637A1
公开(公告)日：2014-07-10
申请号：US14238165
申请日：2012-07-31
申请人： Minako Tsuji , Takuji Okamoto , Takenori Fujimura , Yutaka Minami
发明人： Minako Tsuji , Takuji Okamoto , Takenori Fujimura , Yutaka Minami
IPC分类号： C07C2/34 , C07F7/08 , C08F110/14 , C07C11/21
CPC分类号： C07C2/34 , B01J31/143 , B01J31/146 , B01J31/2295 , B01J2231/20 , B01J2531/48 , C07C2/24 , C07C2/32 , C07C11/02 , C07C11/21 , C07C2531/14 , C07C2531/38 , C07F7/0803 , C08F4/65908 , C08F4/65912 , C08F110/14 , C08F4/65927
摘要： An α-olefin oligomer having the following features (1) to (6), and a method for producing the α-olefin oligomer using a particular double-crosslinked meso complex provide an α-olefin oligomer that contains a smaller amount of a dimer component while having a low viscosity, not in accordance with the Schulz-Flory distribution, and a method for producing the same: (1) a trimer component proportion C3 (% by mass) that is larger than a theoretical value obtained from the S—F distribution, (2) a hexamer component proportion C6 (% by mass) that is smaller than a theoretical value obtained from the S—F distribution, (3) a kinematic viscosity at 100° C. of 20 mm2/s or less, (4) a meso triad fraction [mm] measured by 13C-NMR of 40% by mol of less, (5) from 0.2 to 1.0 of a vinylidene group per one molecule, and (6) an average carbon number of a monomer unit of from 6 to 30, wherein the S—F distribution is calculated based on a chain propagation probability α calculated from a dimer component proportion C2 (% by mass).
摘要翻译：具有以下特征（1）至（6）的α-烯烃低聚物和使用特定双交联的内消旋复合物的α-烯烃低聚物的制备方法提供了含有较少量二聚体组分的α-烯烃低聚物同时具有不符合舒尔茨 - 弗洛尔分布的低粘度及其制造方法：（1）比从S-F获得的理论值大的三聚体组分比例C3（质量％）分布，（2）比从S-F分布得到的理论值小的六聚体成分比例C6（质量％），（3）100℃下的运动粘度为20mm 2 / s以下，（ 4）通过13C-NMR测定的每摩尔亚乙烯基的摩尔数小于（5）0.2〜1.0的中和三单元组分[mm]，（6）单体单元的平均碳数从6到30，其中基于从二聚体co计算的链传播概率α计算S-F分布组分比例C2（质量％）。

2. 发明申请

US20130310527A1 HIGHLY VISCOUS HIGHER ALPHAOLEFIN POLYMER AND METHOD FOR PRODUCING SAME 审中-公开
标题翻译：高粘度聚乙烯高分子聚合物及其生产方法
公开(公告)号：US20130310527A1
公开(公告)日：2013-11-21
申请号：US13824073
申请日：2011-09-01
申请人： Takenori Fujimura , Minako Tsuji , Takuji Okamoto , Yutaka Minami
发明人： Takenori Fujimura , Minako Tsuji , Takuji Okamoto , Yutaka Minami
IPC分类号： C08F110/14
CPC分类号： C08F110/14 , C07F17/00 , C08F4/65908 , C08F4/65912 , C08F2500/17 , C08F2500/20 , C08F2500/15 , C08F4/65927
摘要： An α-olefin polymer has (A) a tacticity index(meso triad fraction)[mm] of 10 to 50 mol %, (B) a kinematic viscosity at 100° C. of 200 to 10,000 mm2/s, (C) a content of a dimer and a trimer is less than 2 mass %, and (D) an average number of carbon atoms of 4 to 30.
摘要翻译：（A）立构规整度指数（meso triad fraction）[mm]为10〜50摩尔％，（B）100℃下的运动粘度为200〜10,000mm 2 / s，（C）a 二聚体和三聚体的含量小于2质量％，（D）平均碳原子数为4〜30。

3. 发明授权

US08445618B2 Highly crystalline higher α-olefin polymer and process for production thereof 有权
标题翻译：高结晶高级α-烯烃聚合物及其制备方法
公开(公告)号：US08445618B2
公开(公告)日：2013-05-21
申请号：US12094692
申请日：2006-11-29
申请人： Takenori Fujimura , Masami Kanamaru , Takuji Okamoto , Yutaka Minami
发明人： Takenori Fujimura , Masami Kanamaru , Takuji Okamoto , Yutaka Minami
IPC分类号： C08F210/00 , C08F10/14
CPC分类号： C08F110/14 , C08F2500/01 , C08F2500/20 , C08F2500/03
摘要： A highly crystalline higher α-olefin polymer that is excellent in compatibility with a thermoplastic resin, particularly a polyolefin, compatibility with a lubricant oil, a fuel oil and wax, mixing property with an inorganic filler, and secondary working property, and a process for production thereof are provided. The highly crystalline higher α-olefin polymer is obtained by polymerizing a monomer containing 80% by mol or more of a higher α-olefin having from 22 to 40 carbon atoms, and satisfies the following items (1) and (2). (1) The melting point (Tm), which is observed, by using a differential scanning calorimeter (DSC), from a melting endothermic curve obtained by maintaining a specimen at 190° C. for 5 minutes under a nitrogen atmosphere, cooling the specimen to −10° C. at a rate of 5° C./min, maintaining at −10° C. for 5 minutes, and then elevating a temperature thereof to 190° C. at a rate of 10° C./min, is from 55 to 100° C. (2) Standards weight average molecular weight (Mw) measured by a gel permeation chromatography (GPC) based on polystyrene is from 1,000 to 5,000,000, and the molecular weight distribution (Mw/Mn) measured thereby is 5.0 or less.
摘要翻译：与热塑性树脂，特别是聚烯烃的相容性优异的高结晶性高级α-烯烃聚合物，与润滑油，燃料油和蜡的相容性，与无机填料的混合性能和二次加工性能的方法提供其生产。通过聚合含有80摩尔％以上的具有22〜40个碳原子的较高级α-烯烃的单体，可以得到高结晶性的高级α-烯烃聚合物，并且满足下述（1）和（2）。（1）通过使用差示扫描量热计（DSC）从在氮气氛下将试样在190℃下保持5分钟而获得的熔融吸热曲线观察到的熔点（Tm），冷却试样至-10℃，以5℃/ min的速率，在-10℃保持5分钟，然后以10℃/ min的速率升温至190℃，（2）通过基于聚苯乙烯的凝胶渗透色谱法（GPC）测定的标准重均分子量（Mw）为1,000〜5,000,000，由此测定的分子量分布（Mw / Mn）为 5.0以下

4. 发明申请

US20090240016A1 HIGHLY CRYSTALLINE HIGHER ALPHA-OLEFIN POLYMER AND PROCESS FOR PRODUCTION THEREOF 有权
标题翻译：高结晶高ALPHA-OLEFIN聚合物及其生产方法
公开(公告)号：US20090240016A1
公开(公告)日：2009-09-24
申请号：US12094692
申请日：2006-11-29
申请人： Takenori Fujimura , Masami Kanamaru , Takuji Okamoto , Yutaka Minami
发明人： Takenori Fujimura , Masami Kanamaru , Takuji Okamoto , Yutaka Minami
IPC分类号： C08F210/14
CPC分类号： C08F110/14 , C08F2500/01 , C08F2500/20 , C08F2500/03
摘要： A highly crystalline higher α-olefin polymer that is excellent in compatibility with a thermoplastic resin, particularly a polyolefin, compatibility with a lubricant oil, a fuel oil and wax, mixing property with an inorganic filler, and secondary working property, and a process for production thereof are provided. The highly crystalline higher α-olefin polymer is obtained by polymerizing a monomer containing 80% by mol or more of a higher α-olefin having from 22 to 40 carbon atoms, and satisfies the following items (1) and (2). (1) The melting point (Tm), which is observed, by using a differential scanning calorimeter (DSC), from a melting endothermic curve obtained by maintaining a specimen at 190° C. for 5 minutes under a nitrogen atmosphere, cooling the specimen to −10° C. at a rate of 5° C./min, maintaining at −10° C. for 5 minutes, and then elevating a temperature thereof to 190° C. at a rate of 10° C./min, is from 55 to 100° C. (2) Standards weight average molecular weight (Mw) measured by a gel permeation chromatography (GPC) based on polystyrene is from 1,000 to 5,000,000, and the molecular weight distribution (Mw/Mn) measured thereby is 5.0 or less.
摘要翻译：与热塑性树脂，特别是聚烯烃的相容性优异的高结晶性高级α-烯烃聚合物，与润滑油，燃料油和蜡的相容性，与无机填料的混合性能和二次加工性能的方法提供其生产。通过聚合含有80摩尔％以上的具有22〜40个碳原子的较高级α-烯烃的单体，可以得到高结晶性的高级α-烯烃聚合物，并且满足下述（1）和（2）。（1）通过使用差示扫描量热计（DSC）从在氮气氛下将试样在190℃下保持5分钟而获得的熔融吸热曲线观察到的熔点（Tm），冷却试样至-10℃，以5℃/ min的速率，在-10℃保持5分钟，然后以10℃/ min的速率升温至190℃，（2）通过基于聚苯乙烯的凝胶渗透色谱法（GPC）测定的标准重均分子量（Mw）为1,000〜5,000,000，由此测定的分子量分布（Mw / Mn）为 5.0以下

5. 发明授权

US08178635B2 α-Olefin polymer and process for production thereof 有权
标题翻译： α-烯烃聚合物及其生产方法
公开(公告)号：US08178635B2
公开(公告)日：2012-05-15
申请号：US12526978
申请日：2008-02-18
申请人： Takenori Fujimura , Masami Kanamaru , Yutaka Minami , Takuji Okamoto
发明人： Takenori Fujimura , Masami Kanamaru , Yutaka Minami , Takuji Okamoto
IPC分类号： C08F4/64 , C08F4/76 , C08F10/14 , C08F10/00
CPC分类号： C08F10/14 , C08F4/65908 , C08F4/65912 , C08F110/14 , C08F210/14 , Y10S526/904 , Y10S526/941 , Y10S526/943 , C08F4/65927 , C08F4/6492 , C08F2500/20 , C08F2500/03 , C08F2500/02 , C08F2500/17
摘要： Provided is an α-olefin polymer having an excellent balance between a molecular weight and a melting point, which is a polymer of one or more kinds of α-olefins having 20 to 40 carbon atoms, and which meets the following requirements (1) to (4): (1) the α-olefin polymer has a molecular weight distribution (Mw/Mn) determined from its weight average molecular weight (Mw) and number average molecular weight (Mn) in terms of polystyrene measured by a GPC method of 2 or less, and has an Mw of 5,000 or less; (2) measurement of a melting point (Tm) of the α-olefin polymer with DSC shows one melting peak, a melting heat absorption (AH) calculated from an area of the melting peak is 20 J/g or more, and the melting peak has a half value width of 10° C. or less; (3) when the Mw falls within a range of 1,000 to 5,000 and an average number of carbon atoms (Cn) of the α-olefins falls within a range of 20 to 40, the Mw, the Cn, and the Tm measured with the DSC satisfy the relationship, 0.0025×Mw+(Cn×3.3812−29.5)≦Tm≦0.0025×Mw+((Cn+1)×3.3812−29.5); and (4) a stereoregularity index [M2] derived from a chain of the α-olefins each having 20 to 40 carbon atoms is 20% by mol or more.
摘要翻译：本发明提供一种具有20〜40个碳原子的一种以上的α-烯烃的分子量和熔点之间的平衡优异的α-烯烃聚合物，其满足以下要求（1）〜（4）：（1）α-烯烃聚合物的重均分子量（Mw）和数均分子量（Mn）的聚苯乙烯的分子量分布（Mw / Mn） 2以下，Mw为5000以下; （2）通过DSC测定α-烯烃聚合物的熔点（Tm），显示出一个熔融峰，由熔融峰面积计算出的熔融热吸收（AH）为20J / g以上，熔融峰值的半值宽度为10℃以下; （3）当Mw落在1,000〜5000的范围内时，α-烯烃的平均碳原子数（Cn）在20〜40的范围内，使用以下方法测定的Mw，Cn和Tm DSC满足关系：0.0025×Mw +（Cn×3.3812-29.5）＆nlE; Tm＆nlE; 0.0025×Mw +（（Cn + 1）×3.3812-29.5）; 和（4）来自各自具有20〜40个碳原子的α-烯烃的链的立构规整性指数[M2]为20摩尔％以上。

6. 发明申请

US20100036066A1 ALPHA-OLEFIN POLYMER AND PROCESS FOR PRODUCTION THEREOF 有权
标题翻译： ALPHA-OLEFIN聚合物及其生产方法
公开(公告)号：US20100036066A1
公开(公告)日：2010-02-11
申请号：US12526978
申请日：2008-02-18
申请人： Takenori Fujimura , Masami Kanamaru , Yutaka Minami , Takuji Okamoto
发明人： Takenori Fujimura , Masami Kanamaru , Yutaka Minami , Takuji Okamoto
IPC分类号： C08F4/42 , C08F10/14
CPC分类号： C08F10/14 , C08F4/65908 , C08F4/65912 , C08F110/14 , C08F210/14 , Y10S526/904 , Y10S526/941 , Y10S526/943 , C08F4/65927 , C08F4/6492 , C08F2500/20 , C08F2500/03 , C08F2500/02 , C08F2500/17
摘要： Provided is an α-olefin polymer having an excellent balance between a molecular weight and a melting point, which is a polymer of one or more kinds of α-olefins having 20 to 40 carbon atoms, and which meets the following requirements (1) to (4): (1) the α-olefin polymer has a molecular weight distribution (Mw/Mn) determined from its weight average molecular weight (Mw) and number average molecular weight (Mn) in terms of polystyrene measured by a GPC method of 2 or less, and has an Mw of 5,000 or less; (2) measurement of a melting point (Tm) of the α-olefin polymer with DSC shows one melting peak, a melting heat absorption (AH) calculated from an area of the melting peak is 20 J/g or more, and the melting peak has a half value width of 10° C. or less; (3) when the Mw falls within a range of 1,000 to 5,000 and an average number of carbon atoms (Cn) of the α-olefins falls within a range of 20 to 40, the Mw, the Cn, and the Tm measured with the DSC satisfy the relationship, 0.0025×Mw+(Cn×3.3812−29.5)≦Tm≦0.0025×Mw+((Cn+1)×3.3812−29.5); and (4) a stereoregularity index [M2] derived from a chain of the α-olefins each having 20 to 40 carbon atoms is 20% by mol or more.
摘要翻译：本发明提供一种具有20〜40个碳原子的一种以上的α-烯烃的分子量和熔点之间的平衡优异的α-烯烃聚合物，其满足以下要求（1）〜（4）：（1）α-烯烃聚合物的分子量分布（Mw / Mn）由其重均分子量（Mw）和数均分子量（Mn）的聚苯乙烯换算而成 2以下，Mw为5000以下; （2）用DSC测定α-烯烃聚合物的熔点（Tm），显示出一个熔融峰，由熔融峰面积计算出的熔融热吸收（AH）为20J / g以上，熔融峰值的半值宽度为10℃以下; （3）当Mw落在1,000〜5000的范围内时，α-烯烃的平均碳原子数（Cn）在20〜40的范围内，Mw，Cn和Tm DSC满足关系，0.0025xMw +（Cnx3.3812-29.5）<= Tm <= 0.0025xMw +（（Cn + 1）×3.3812-29.5）; 和（4）衍生自各自具有20〜40个碳原子的α-烯烃链的立构规整性指数[M2]为20摩尔％以上。

7. 发明授权

US07459503B2 Process for production of modified propylene polymers and modified propylene polymers produced by the process 失效
标题翻译：通过该方法生产改性丙烯聚合物和改性丙烯聚合物的方法
公开(公告)号：US07459503B2
公开(公告)日：2008-12-02
申请号：US10509329
申请日：2003-04-11
申请人： Masami Kanamaru , Yutaka Minami , Ryo Aburatani , Tomio Tatsumi , Takenori Fujimura
发明人： Masami Kanamaru , Yutaka Minami , Ryo Aburatani , Tomio Tatsumi , Takenori Fujimura
IPC分类号： C08F8/06 , C08F8/46
CPC分类号： C09J123/12 , C08L2023/42 , C08L2666/02 , C09J123/10
摘要： The present invention relates to a method for producing a modified propylene-based polymer containing modifying a propylene-based polymer by a radical initiator and an organic acid, a modified propylene-based polymer obtained by the method, and an adhesive composition containing the modified propylene-based polymer. The propylene-based polymer is a propylene homopolymer satisfying the conditions of (a) mmmm=20 to 60 mol %, (b) [rrrr/(1-mmmm)]≦0.1, (c) rmrm>2.5 mol %, (d) mmxrr/(mr)2≦2.0, and (e) the weight ratio (W25) of components eluted at 25° C. or lower in a temperature programmed chromatography is 20 to 100% by weight, or a propylene copolymer satisfying the condition of (h) the stereoregularity index (P) obtained by 13C-NMR measurement is 55 to 90 mol %.The modified propylene-based polymer of the invention can make a polyolefin, etc. more adhesive, stronger, or flexible, to be useful for a high-adhesive sealant or an polyolefin with increased compatibility to an inorganic filler, etc., particularly as a resin for a hot-melt adhesive.
摘要翻译：本发明涉及通过自由基引发剂和有机酸改性丙烯类聚合物的改性丙烯类聚合物的制造方法，该方法得到的改性丙烯类聚合物和含有改性丙烯的粘合剂组合物基聚合物。丙烯类聚合物是满足（a）mmmm = 20〜60mol％，（b）[rrrr /（1-mmmm）] <= 0.1，（c）rmrm> 2.5mol％的条件的丙烯均聚物， d）mmxrr /（mr）2 <= 2.0，（e）在温度程序化色谱法中在25℃以下洗脱的组分的重量比（W25）为20〜100重量％，或者满足（h）由13 C-NMR测定得到的立构规整度指数（P）的条件为55〜90摩尔％。本发明的改性丙烯类聚合物可以使聚烯烃等具有更好的粘合性，更强或柔性，可用于具有增加与无机填料等的相容性的高粘合密封剂或聚烯烃，特别是作为用于热熔胶的树脂。

8. 发明授权

US07714081B2 Heat-storage material composition 失效
标题翻译：储热材料组成
公开(公告)号：US07714081B2
公开(公告)日：2010-05-11
申请号：US10577496
申请日：2004-10-27
申请人： Masanori Sera , Yutaka Minami , Takenori Fujimura
发明人： Masanori Sera , Yutaka Minami , Takenori Fujimura
IPC分类号： C08L23/00 , C08L23/02
CPC分类号： C09K5/063
摘要： The present invention relates to a heat storage material composition comprising 20 to 100% by weight of a heat storage material, 80 to 0% by weight of crystalline polyolefin (B) and 50 to 0% by weight of an elastomer (C), and the heat storage material described above contains a side chain-crystalline polymer (A), wherein the heat storage material described above comprises preferably a higher α-olefin polymer (a) containing 50 mole % or more of higher α-olefin having 10 or more carbon atoms and a petroleum wax (b) in which a melting point (Tm) is higher by 10° C. or more than that of the polymer (a). Provided is a heat storage material composition which has less bleeding and stickiness and is excellent in stability at high temperature and which can meet a change in temperature such as a difference in room temperature when applied to a material for floor heating and can avoid a heating state deviated to high temperature or low temperature.
摘要翻译：本发明涉及一种储热材料组合物，其包含20至100重量％的蓄热材料，80至0重量％的结晶聚烯烃（B）和50至0重量％的弹性体（C），以及上述储热材料含有侧链状聚合物（A），其中上述储热材料优选包含含有50摩尔％以上的具有10个以上的高级α-烯烃的高级α-烯烃聚合物（a）碳原子和熔点（Tm）高于聚合物（a）的10℃以上的石油蜡（b）。本发明提供一种蓄热材料组合物，其具有较少的渗透性和粘性，并且在高温下的稳定性优异，并且当施加到用于地板加热的材料时可以满足诸如室温差的温度变化并且可以避免加热状态偏向高温或低温。

9. 发明授权

US07109283B2 Higher α-olefin copolymers and process for preparation thereof 有权
标题翻译：高级α-烯烃共聚物及其制备方法
公开(公告)号：US07109283B2
公开(公告)日：2006-09-19
申请号：US11324304
申请日：2006-01-04
申请人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
发明人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
IPC分类号： C08F10/14
CPC分类号： C08F210/14 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F2500/20 , C08F2500/03
摘要： The present invention provides a crystalline higher α-olefin copolymer obtained by copolymerizing at least two higher α-olefins having 10 or more carbon atoms or at least one higher α-olefin having 10 or more carbon atoms with at least one other olefin, wherein it satisfies certain conditions.
摘要翻译：本发明提供通过使至少两种具有10个或更多个碳原子的高级α-烯烃或至少一个具有10个或更多个碳原子的高级α-烯烃与至少一种其它烯烃共聚得到的结晶高级α-烯烃共聚物，其中满足一定条件。

10. 发明授权

US07019091B2 Higher α-olefin copolymers and process for preparation thereof 失效
公开(公告)号：US07019091B2
公开(公告)日：2006-03-28
申请号：US10925037
申请日：2004-08-25
申请人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
发明人： Yutaka Minami , Takenori Fujimura , Masanori Sera , Tomoaki Takebe
IPC分类号： C08F4/642 , C08F210/14
CPC分类号： C08F210/14 , C08F4/65908 , C08F4/65912 , C08F4/65927 , C08F2500/20 , C08F2500/03
摘要： The present invention provides a crystalline higher α-olefin copolymer obtained by copolymerizing at least two higher α-olefins having 10 or more carbon atoms or at least one higher α-olefin having 10 or more carbon atoms with at least one other olefin, wherein it satisfies certain conditions.

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