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1. 发明授权

US5214286A Horizontal multiple internal reflection accessory for internal reflection spectroscopy 失效
标题翻译：用于内部反射光谱的水平多重内反射附件
公开(公告)号：US5214286A
公开(公告)日：1993-05-25
申请号：US895019
申请日：1992-06-08
申请人： Milan Milosevic , Nicolas J. Harrick
发明人： Milan Milosevic , Nicolas J. Harrick
IPC分类号： G01N21/55
CPC分类号： G01J3/02 , G01J3/0286 , G01J3/0291 , G01N21/552
摘要： The multiple internal reflection accessories for internal reflection spectrometry described here utilizes a novel approach to match the round beam size and shape from a conventional FT-IR spectrometer to the typical rectangular IRE aperture. Its transfer optics distort the beam entering and exiting the IRE so that the cross-section of the beam is matched to that of the standard rectangular aperture of the IRE. This configuration reduces energy losses, eliminates the need to aluminize the edges of the crystal, and reduces spurious peaks from the adhesive or O-rings used to conventionally mount the crystal.
摘要翻译：这里描述的用于内部反射光谱的多个内部反射附件利用了将常规FT-IR光谱仪的圆形光束尺寸和形状与典型的矩形IRE孔径相匹配的新颖方法。其传输光学器件使入射和离开IRE的光束变形，使得光束的横截面与IRE的标准矩形孔的横截面相匹配。该配置减少了能量损失，消除了对晶体边缘进行镀铝的需要，并且减少了用于常规安装晶体的粘合剂或O形环的杂散峰。

2. 发明授权

US4853542A Collecting hemispherical attachment for spectrophotometry 失效
标题翻译：收集半球形附件用于分光光度法
公开(公告)号：US4853542A
公开(公告)日：1989-08-01
申请号：US59323
申请日：1987-06-08
申请人： Milan Milosevic , Nicolas J. Harrick
发明人： Milan Milosevic , Nicolas J. Harrick
IPC分类号： G01N21/47 , G01N21/51
CPC分类号： G01N21/474 , G01N2021/516 , G01N2021/6469
摘要： An attachment or accessory for performing diffuse reflectance spectroscopy on a conventional UV-VIS-IR spectrophotometer. The attachment includes a removable body having a hemispherical mirrored interior surface positioned over the sample, and containing windows for entrance and exit of radiation. Multiple sampling of the same sample area enhances the quality of the spectrophotometer output.
摘要翻译：用于在常规UV-VIS-IR分光光度计上进行漫反射光谱的附件或附件。附件包括具有位于样品上方的半球形镜面内表面的可移除体，并且包含用于进入和离开辐射的窗口。相同样品区域的多次采样提高了分光光度计输出的质量。

3. 发明授权

US5262845A Optical accessory for variable angle reflection spectroscopy 失效
标题翻译：用于可变角度反射光谱的光学附件
公开(公告)号：US5262845A
公开(公告)日：1993-11-16
申请号：US894991
申请日：1992-06-08
申请人： Milan Milosevic , Nicolas J. Harrick
发明人： Milan Milosevic , Nicolas J. Harrick
IPC分类号： G01J3/02 , G01J3/42 , G01N21/47 , G01N21/01
CPC分类号： G01N21/474 , G01J3/02 , G01J3/0216 , G01J3/0237 , G01J3/0291 , G01J3/42
摘要： A variable angle reflection accessory for use in reflection spectrometry characterized by a pair of fixed ellipsoidal reflectors positioned inside an enclosure adjacent a sample surface on the outside of the enclosure and a pair of rotatable plane mirrors positioned at opposite sides of the sample surface. The spectrometer beam is brought to a focus at the first plane mirror, from which it is reflected off the first ellipsoidal reflector to a focus at the sample surface. The reflected beam follows a corresponding path back to the spectrometer. Rotating the mirrors in unison causes the beam angle of incidence on the sample surface to vary over a wide range while maintaining optical alignments and continuing to center the radiation on the same sample area. The outside positioning of the sample surface allows the accessory to be easily coupled to a purge port of the spectrometer and allows rapid sample exchanges without breaking the purge atmosphere.
摘要翻译：一种用于反射光谱测定的可变角度反射附件，其特征在于，一对固定的椭圆体反射器位于外壳附近的外壳附近的外壳上的样品表面和位于样品表面的相对侧的一对可旋转的平面镜。光谱仪光束在第一平面镜处被聚焦，从第一平面反射镜将其从第一椭圆反射器反射到样品表面处的焦点。反射光束跟随相应的路径回到光谱仪。一致地转动反射镜导致样品表面上的光束入射角在宽范围内变化，同时保持光学对准并且继续将辐射对准在相同的样品区域上。样品表面的外部定位允许附件容易地耦合到光谱仪的吹扫端口，并允许快速的样品交换而不破坏吹扫气氛。

4. 发明授权

US5220401A Multiple internal reflectance liquid sampling 失效
标题翻译：多重内反射液体采样
公开(公告)号：US5220401A
公开(公告)日：1993-06-15
申请号：US888841
申请日：1992-05-27
申请人： Milan Milosevic , Nicolas J. Harrick
发明人： Milan Milosevic , Nicolas J. Harrick
IPC分类号： G01N21/05 , G01N21/55 , G01N21/85 , G02B1/02 , G02B6/00
CPC分类号： G02B6/00 , G01N21/552 , G02B1/02 , G01N21/05 , G01N21/8507
摘要： A liquid cell for IRS comprising a rod-shaped crystal having a cylindrical sampling surface and integral conical end portions forming end entrance and exit faces for a radiation beam. The center of the end faces are masked. All radiation entering the entrance face internally reflects from the conical surface and propagates down the IRE by multiple internal reflections from the cylindrical sampling surface. The IRE can be sealed into a trough or flow-through housing for the liquid sample. The seals are at insensitive regions of the IRE.
摘要翻译：一种用于IRS的液体池，包括具有圆柱形取样表面的棒状晶体和形成用于辐射束的端部入射和出射面的整体锥形端部。端面的中心被遮蔽。进入入口面的所有辐射在内部从锥形表面反射，并通过多个内部反射从圆柱形采样表面向下传播到IRE。 IRE可以被密封到用于液体样品的槽或流通壳体中。密封件在IRE的不敏感区域。

5. 发明授权

US5177561A Purging of optical spectrometer accessories 失效
标题翻译：清洗光谱仪配件
公开(公告)号：US5177561A
公开(公告)日：1993-01-05
申请号：US831529
申请日：1992-02-05
申请人： Milan Milosevic , Nicolas J. Harrick
发明人： Milan Milosevic , Nicolas J. Harrick
IPC分类号： G01J3/02 , G01N21/25 , G01N21/35
CPC分类号： G01J3/02 , G01J3/0205 , G01J3/0286 , G01J3/0291 , G01N21/255 , G01N2021/174 , G01N2021/1793 , G01N2021/3595 , G01N2021/6469 , G01N21/474 , G01N2201/084
摘要： Optical spectroscopy in a purging atmosphere wherein an optical accessory is gas-tight coupled in the spectrometer sample compartment to the open beam port of the spectrometer, whereby the same purging gas used by the spectrometer can be employed to purge the accessory. Where the accessory allows external sample placement or external adjustments, rapid sample changing or adjustment is possible without breaking the purge seal. In another embodiment, the accessory has its own purge inlet and sealed windows for receiving the spectrometer beam.
摘要翻译：在清洗气氛中的光谱学，其中光学附件在光谱仪样品室中气密耦合到光谱仪的开口光束端口，由此可以使用由光谱仪使用的相同的净化气体来清洗附件。如果附件允许外部样品放置或外部调整，可以快速进行样品更换或调整，而不会破坏吹扫密封。在另一个实施例中，附件具有其自己的吹扫入口和用于接收光谱仪束的密封窗口。

6. 发明授权

US5308983A Spectroscopic accessory with microscope illuminator 失效
标题翻译：光学附件与显微照明器
公开(公告)号：US5308983A
公开(公告)日：1994-05-03
申请号：US907629
申请日：1992-07-02
申请人： Milan Milosevic , Nicolas J. Harrick , Craig R. Wisch
发明人： Milan Milosevic , Nicolas J. Harrick , Craig R. Wisch
IPC分类号： G01J3/42 , G01N21/55 , G02B21/00 , G02B21/06 , G01N21/17 , G01N21/01
CPC分类号： G01N21/552 , G02B21/00 , G02B21/06 , G01J3/42
摘要： An optical accessory for reflection spectroscopy having a very small sampling area and provided with a microscope for aiding the user to locate a sample to be analyzed on the active sampling area where it can interact with a radiation beam. The microscope is characterized by fiber optic bundles to supply sample illumination via a cone-shaped light-funnelling tip terminated in a thin hard optically transparent wear tip, e.g., of sapphire. The microscope is also used to apply pressure via the wear tip to the sample while it is being illuminated and while it can be viewed to maximize interaction with the radiation.
摘要翻译：用于具有非常小的采样区域的反射光谱的光学附件，并且具有显微镜，用于帮助用户定位要在其上可以与辐射束相互作用的有源采样区域上要分析的样本。显微镜的特征在于光纤束，其通过终止于诸如蓝宝石的薄硬光学透明耐磨尖端的锥形光漏斗末端提供样品照明。显微镜还被用于在被照亮时通过磨损尖端向样品施加压力，并且当它被看到以最大化与辐射的相互作用时。

7. 发明授权

US5210418A Ultra-small sample analyzer for internal reflection spectroscopy 失效
标题翻译：用于内反射光谱的超小样品分析仪
公开(公告)号：US5210418A
公开(公告)日：1993-05-11
申请号：US762577
申请日：1991-09-19
申请人： Nicolas J. Harrick , Milan Milosevic
发明人： Nicolas J. Harrick , Milan Milosevic
IPC分类号： G01N21/47 , G01N21/55
CPC分类号： G01N21/552 , G01J3/0286 , G01J3/0291 , G01N21/474
摘要： An ultra-small sample analyzer for internal reflection spectrometry comprises a small hemispherical crystal of an infrared-transparent hard material whose flat surface receives the sample to be analyzed. The analyzing beam is contracted to a very small size when incident on the hemispherical surface. Pressure-applying means of a size substantially matching that of the beam at the sampling surface enables interaction of substantially the entire beam with the sample producing spectra of high contrast from microgram or nanogram quantities of the sample.
摘要翻译：用于内部反射光谱的超小样本分析仪包括红外透明硬质材料的小半球形晶体，其平坦表面接收要分析的样品。当入射在半球形表面上时，分析束收缩到非常小的尺寸。与采样表面上的光束大小匹配的压力施加装置使得基本上整个光束与样品的相互作用能够从微克或纳克量的样品产生高对比度的光谱。

8. 发明授权

US5048970A Optical attachment for variable angle reflection spectroscopy 失效
标题翻译：用于可变角度反射光谱的光学附件
公开(公告)号：US5048970A
公开(公告)日：1991-09-17
申请号：US546081
申请日：1990-06-29
申请人： Milan Milosevic , Nicolas J. Harrick
发明人： Milan Milosevic , Nicolas J. Harrick
IPC分类号： G01J3/02 , G01J3/42 , G01N21/47 , G01N21/55
CPC分类号： G01N21/55 , G01J3/02 , G01J3/0216 , G01J3/0237 , G01J3/0291 , G01N21/474 , G01J2003/425 , G01N2021/4723
摘要： A vaariable angle reflection accessory for use in reflection spectrometry characterized by a pair of fixed ellipsoidal reflectors positioned over the sample surface and a pair of rotatable plane mirrors positions at opposite sides of the sample surface. The spectrometer beam is brought to a focus at the first plane mirror, from which it is reflected off the first ellipsoidal reflector to a focus at the sample surface. The reflected beam follows a corresponding path back to the spectrometer. Rotating the mirrors in unison causes the beam angle of incidence on the sample surface to vary over a wide range while maintaining optical alignments and continuing to center the radiation on the same sample area.
摘要翻译：用于反射光谱法的变角反射附件，其特征在于位于样品表面上方的一对固定椭圆体反射器和位于样品表面相对两侧的一对可转动的平面镜。光谱仪光束在第一平面镜处被聚焦，从第一平面反射镜将其从第一椭圆反射器反射到样品表面处的焦点。反射光束跟随相应的路径回到光谱仪。一致地转动反射镜导致样品表面上的光束入射角在宽范围内变化，同时保持光学对准并且继续将辐射对准在相同的样品区域上。

9. 发明授权

US5035504A Liquid analysis with internal reflection spectroscopy 失效
标题翻译：用内反射光谱法进行液体分析
公开(公告)号：US5035504A
公开(公告)日：1991-07-30
申请号：US512451
申请日：1990-04-23
申请人： Milan Milosevic , Nicolas J. Harrick
发明人： Milan Milosevic , Nicolas J. Harrick
IPC分类号： G01N21/55
CPC分类号： G01N21/552
摘要： Novel internal reflection plates and spectroscopy systems using such plates especially for analyzing liquids. The plates have a generally trapezoidal shape with beveled ends, and are oriented relative to an incident radiation beam such that the beam reflects from the bevel and propagates down the plate by multiple internal reflections form its major surfaces.
摘要翻译：新型内反射板和使用这种板的光谱系统，特别用于分析液体。板具有大致梯形形状，具有倾斜的端部，并且相对于入射的辐射束定向，使得光束从斜面反射并且通过多个内部反射从其主表面向下传播。

10. 发明授权

US08218139B2 Optical multipass cell for repeated passing of light through the same point 有权
标题翻译：用于反复通过相同点的光的多通道单元
公开(公告)号：US08218139B2
公开(公告)日：2012-07-10
申请号：US12767172
申请日：2010-04-26
申请人： Milan Milosevic , Violet Milosevic
发明人： Milan Milosevic , Violet Milosevic
IPC分类号： G01J3/44
CPC分类号： G02B17/004 , G01J3/02 , G01J3/021 , G01J3/42 , G01N21/031 , G01N21/645 , G01N21/65 , G01N2021/6463 , G01N2201/0636
摘要： The present invention is a multipass unipoint optical cell used for the improved analysis of samples by transmission, reflection, Raman or fluorescence spectroscopy by the multiple reimaging of light through the same analysis point. The cell comprises two or more identical optical reimaging elements each consisting of two symmetrically opposing, identical, confocal, and coaxial parabolic reflective surfaces. These reimaging optical elements can be arranged around the common focal point, which thus becomes the analysis point, to form different multipass unipoint optical cell configurations, all the passes crossing in the analysis point where a sample is brought to interact with light, the effect of said interaction being enhanced in proportion to the number of passes.
摘要翻译：本发明是一种多通道单点光学单元，用于通过透射，反射，拉曼或荧光光谱，通过相同分析点对光进行多重成像，改进样品分析。单元包括两个或更多个相同的光学成像元件，每个元件由两个对称相对的，相同的共聚焦和同轴的抛物面反射表面组成。这些成像光学元件可以布置在公共焦点周围，从而成为分析点，以形成不同的多通道单点光学单元配置，所有通过在样品与光相互作用的分析点中交叉的所有通过，所述相互作用与通过次数成正比地增加。

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