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1. 发明授权

US5705193A Method for preparing granules containing one or more active principles 失效
标题翻译：制备含有一种或多种活性成分的颗粒的方法
公开(公告)号：US5705193A
公开(公告)日：1998-01-06
申请号：US666549
申请日：1996-06-20
申请人： Michel Bourgogne , Colette Meinard
发明人： Michel Bourgogne , Colette Meinard
IPC分类号： B01J2/00 , A01N25/12 , A01N25/14 , A01N53/00 , A01N53/02 , A61K9/14
CPC分类号： A01N25/14 , A01N53/00
摘要： A process for the preparation of granules containing at least one active principle with a melting point above 70.degree. C. selected from the group consisting of herbicides, fungicides and insecticides comprising dissolving the active principle in an aromatic solvent or pyrrolidone, absorbing the resulting solution on a support, optionally adding water thereto and drying the resulting product to form the granules and the granules produced thereby which have a superior biological activity than a granule dispersible in water with good stability.
摘要翻译： PCT No.PCT / FR94 / 01506 Sec。 371日期：1996年6月20日 102（e）1996年6月20日PCT 1994年12月21日PCT PCT。第WO95 / 17089号公报日期：1995年6月29日制备含有至少一种熔点高于70℃的活性成分的颗粒的方法，其选自除草剂，杀真菌剂和杀虫剂，包括将活性成分溶解在芳族溶剂或吡咯烷酮中，将所得溶液吸附在载体上，任选地向其中加入水并干燥所得产物以形成颗粒，由此生产的颗粒具有比分散在水中的具有良好稳定性的颗粒更好的生物活性。

2. 发明授权

US4492687A Light-stable pesticidal compositions 失效
标题翻译：光稳定的农药组合物
公开(公告)号：US4492687A
公开(公告)日：1985-01-08
申请号：US550082
申请日：1983-11-08
申请人： Jean-Jacques Herve , Jean-Claude Suglia , Colette Meinard
发明人： Jean-Jacques Herve , Jean-Claude Suglia , Colette Meinard
IPC分类号： A01N25/22 , A01N53/00
CPC分类号： A01N25/22 , A01N53/00 , Y10S514/972
摘要： Novel light-stable pyrethrinoid pesticidal compositions comprising (a) at least one liquid vehicle, (b) at least one surface-active agent soluble in the said liquid vehicle, (c) at least one azodyestuff stabilizer and (d) at least one ester of the formula ##STR1## .
摘要翻译：新型的光稳定的拟除虫菊酯杀虫组合物，其包含（a）至少一种液体载体，（b）至少一种可溶于所述液体载体的表面活性剂，（c）至少一种抗静电稳定剂和（d）至少一种酯的公式

3. 发明授权

US5139774A Hydrophilic polymer granules for uniform release of active principle 失效
标题翻译：用于均匀释放活性原子的水解聚合物颗粒
公开(公告)号：US5139774A
公开(公告)日：1992-08-18
申请号：US283840
申请日：1988-12-13
申请人： Colette Meinard , Jean-Claude Suglia , Claude Taranta
发明人： Colette Meinard , Jean-Claude Suglia , Claude Taranta
IPC分类号： A01N25/10 , A01N25/12
CPC分类号： A01N25/12
摘要： Granules prepared by absorbing on hydrophilic polymer granules an aqueous emulsion of at least one active principle and drying the resulting mixture to obtain granules which release the active principle in uniform manner.

4. 发明授权

US4376113A Stable suspensions and powders of stable microcapsules and their preparation 失效
标题翻译：稳定的悬浮液和稳定的微胶囊粉末及其制备方法
公开(公告)号：US4376113A
公开(公告)日：1983-03-08
申请号：US181359
申请日：1980-08-26
申请人： Jean-Claude Suglia , Colette Meinard
发明人： Jean-Claude Suglia , Colette Meinard
IPC分类号： A61K9/64 , A01N25/28 , A61K9/50 , A61K39/12 , B01J13/02 , B01J13/10 , C12N11/04 , A61K9/34
CPC分类号： C12N11/04 , A01N25/28 , A61K9/5047 , A61K9/5057 , B01J13/10 , C12N2710/14051 , Y10T428/2984
摘要： A process for the preparation of stable suspensions and powders of stable microcapsules containing at least one active material having a variable porosity comprising preparing a colloidal solution of equal parts by weight of gelatin and acacia gum with a total concentration of 4 to 6% by weight of the final emulsion, preparing an oil solution, suspension or emulsion of the active material at a concentration of 1 to 5% by weight of the final emulsion and containing a variable amount of organosoluble ethyl hydroxyethylcellulose, mixing the said two compositions with stirring at a temperature near 50.degree. C. in the presence of an emulsifying agent to form an "oil in water" emulsion, effecting consecutively coacervation and microencapsulation of the emulsified droplets containing the active material by adjusting the pH to 4.2 to 4.4 by addition of an acid and then cooling the mixture to about 20.degree. C. with stirring, reticulating the walls of the formed microcapsules by reaction with glutaric aldehyde and tannin with stirring at about 20.degree. C. and either forming a concentrated suspension of microcapsules by slow addition at 20.degree. C. of a water soluble ethyl hydroxyethylcellulose to the eticulated microcapsules or adding an antiagglomeration agent with stirring to the reticulated microcapsules at 20.degree. C. and drying the resulting powder and the microcapsules produced thereby which are stable with respect to physico chemical influences and to exterior elements generally, such as sunlight and temperature changes so that the encapsulated active material maintains its activity.
摘要翻译：制备稳定的悬浮液和稳定的微胶囊的粉末的方法，所述稳定的微胶囊含有至少一种具有可变孔隙率的活性物质，包括制备等份重量的明胶和阿拉伯树胶的胶体溶液，其总浓度为4至6重量％最终乳液，以最终乳液的1至5重量％的浓度制备活性物质的油溶液，悬浮液或乳液，并含有可变量的有机溶剂乙基羟乙基纤维素，在搅拌下将所述两种组合物在温度在乳化剂存在下接近50℃以形成“水包油”乳液，通过加入酸将pH调节至4.2至4.4，从而连续地凝聚和微囊化包含活性物质的乳化液滴，然后在搅拌下将混合物冷却至约20℃，通过与戊二烯反应将形成的微胶囊的壁网状化在约20℃搅拌下，通过在20℃下缓慢加入水溶性乙基羟乙基纤维素形成微胶囊的浓缩悬浮液，并在搅拌下向搅拌下加入抗凝聚剂至网状微胶囊干燥得到的粉末和由此产生的微胶囊，其相对于物理化学影响是稳定的，并且通常包括阳光和温度变化，从而使包封的活性材料保持其活性。

5. 发明授权

US4440756A Light-stable pesticidal compositions 失效
公开(公告)号：US4440756A
公开(公告)日：1984-04-03
申请号：US271989
申请日：1981-06-09
申请人： Jean-Jacques Herve , Jean-Claude Suglia , Colette Meinard
发明人： Jean-Jacques Herve , Jean-Claude Suglia , Colette Meinard
IPC分类号： A01N53/02 , A01N25/22 , A01N37/34 , A01N53/00 , A01N53/04 , A01N53/06 , A01N53/08
CPC分类号： A01N25/22 , A01N53/00 , Y10S514/97 , Y10S514/972
摘要： Novel light-stable pyrethrinoid pesticidal compositions comprising (a) at least one liquid vehicle, (b) at least one surface-active agent soluble in the said liquid vehicle, (c) at least one azodyestuff stabilizer selected from the group consisting of a mixture of 1-[{4-(phenylazo)-phenyl)}-azo]-3-naphthalenol and 4-[{4-(phenylazo)-phenyl}-azo]-phenol (a component of Scarlet R), 1-[4-(4-phenylazo-phenyl)-azo]-naphthalene (Red organol BS), 1-[{2-methyl-4-(2-methylphenylazo)-phenyl}-azo]-2-naphthalenol (Red Sudan IV), 1-[(2-methoxyphenol)-azo]-2-naphthaphenol (Vermillion organol); 1-[(1-naphthalenyl)-azo]-2-naphthalenol (Scarlet 2R for fat), 1-(phenylazo)-2-naphthalenol (Sudan I), 1-[(2-hydroxy-4-methyl-phenyl)-azo]-2-naphthalenol (Sudan II), 1-[{dimethyl-4-[(dimethyl)-phenyl]-azo}-phenylazo]-2-naphthalenol (Red to fat 5B), N-ethyl-1-[{4-(phenylazo)-phenyl}-azo]-2-naphthalenylamine (Red to fat 7B), 1-[{1-naphthalenyl}-azo]-2,4-benzene-diamine (Brown RR to fat), 2-[(2-methoxyphenyl)-azo]-phenol (Red to fat G), disodium 4-hydroxy-3-[(4-sulfo-1-naphthalenyl)-azo]-1-naphthalene sulfonate (azo ruby), 4-[(4-ethoxyphenyl)-azo]-1-naphthalenol (Brown to fat B), 2,4-dihydro-5-methyl-2-phenyl-4-(phenylazo)-3H-pyrazol-3-one (Yellow to fat 3G), N,N-diethyl-4-(phenylazo)-benzeneamine (Yellow to fat GGN), 2,3-dihydro-2,2-dimethyl-6-[(4-phenylazo)-1-naphthalenyl]-azo-1H-perimidine (Black to fat HB), N-[4-phenyl)-(4-phenylamino)-1-naphthalenyl]-azo methylene-2,5-cyclohexadien-1-ylidene-N-methyl-methaniminium chloride (Blue to fat B) and 1-[{4-(phenylazo)-phenyl}-azo]-2-naphthalenol and (d) at least one ester of the formula ##STR1## wherein Y is selected from the group consisting of ##STR2## in its various stereoisomeric forms and mixtures thereof, Z is alkyl of 1 to 6 carbon atoms, Y is selected from the group consisting of hydrogen, halogen, --CN, --NO.sub.3, alkyl of 1 to 4 carbon atoms and alkoxy of 1 to 4 carbon atoms, n is 0, 1, 2 or 3, W is selected from the group consisting of ##STR3## X.sub.1 is selected from the group consisting of hydrogen, fluorine, chlorine and bromine, X.sub.2 is selected from the group consisting of fluorine, chlorine and bromine, X.sub.3 is selected from the group consisting of chlorine, bromine and iodine, X.sub.4 is a halogen and X.sub.5 is a halogen optionally other than that of X.sub.4 and due to asymetric carbon atom in W, the compounds are in the A isomer or B isomer form or mixtures thereof and R is selected from the group consisting of ##STR4## and benzyl optionally substituted with at least one member of the group consisting of alkyl of 1 to 4 carbon atoms, alkenyl of 2 to 6 carbon atoms, alkenyloxy of 2 to 6 carbon atoms, alkadienyl of 4 to 8 carbon atoms, methylenedioxy, benzyl and halogens, R.sub.1 is selected from the group consisting of hydrogen and methyl, R.sub.2 is selected from the group consisting of monocyclic aryl and --CH.sub.2 --C.tbd.CH, R.sub.3 is an aliphatic of 2 to 6 carbon atoms having at least one carbon-carbon insaturation, R.sub.4 is selected from the group consisting of hydrogen, --CN, CH.sub.3 and --C.tbd.CH, R.sub.5 is selected from the group consisting of chlorine and methyl, n is 0, 1 or 2, R.sub.6, R.sub.7, R.sub.8 and R.sub.9 are individually selected from the group consisting of hydrogen, chlorine and methyl and S/I indicates that the ring may be aromatic, dihydro or tetrahydro the alcoholic moiety R-OH being capable of containing one or more asymetric carbon atoms and of existing in the form of various stereoisomers and their use to combat pests.

6. 发明授权

US5945113A Pesticidal paste compositions 失效
标题翻译：杀虫剂组合物
公开(公告)号：US5945113A
公开(公告)日：1999-08-31
申请号：US718431
申请日：1996-09-26
申请人： Colette Meinard , Jean-Claude Suglia
发明人： Colette Meinard , Jean-Claude Suglia
IPC分类号： A01N25/04 , A01N25/34 , A01N53/00 , A01N53/08 , A01N25/08
CPC分类号： A01N25/34 , A01N25/04 , A01N53/00
摘要： A readily, water-dispersible pesticide formulation in the form of a thick paste containing 1 to 80% by weight of the pesticide, 0.30 to 2.0% by weight of a micropore-generating agent and 30 to 50% by weight of effervescent agents the percentages being based on the total weight of the formulation.
摘要翻译： PCT No.PCT / FR95 / 00471 Sec。 371日期：1996年9月24日 102（e）1996年9月24日PCT 1995年4月12日提交PCT公布。第WO95 / 28082号公报日期1995年10月26日一种容易的水分散农药制剂，其形式为含有1至80重量％农药的稠糊剂，0.30-2.0重量％的微孔发生剂和30至50重量％泡腾剂的百分比基于制剂的总重量。

7. 发明授权

US5087456A Method of combatting pests by applying novel granules to the soil 失效
标题翻译：通过将新的颗粒应用于土壤来组合PESTS的方法
公开(公告)号：US5087456A
公开(公告)日：1992-02-11
申请号：US486798
申请日：1990-03-01
申请人： Colette Meinard , Jean-Claude Suglia , Claude Taranta
发明人： Colette Meinard , Jean-Claude Suglia , Claude Taranta
IPC分类号： A01N25/10 , A01N25/12
CPC分类号： A01N25/12
摘要： Granules prepared by absorbing on hydrophilic polymer of acrylic acid polymers and/or acrylamide polymers granules an aqueous emulsion of at least one active principle such as pyrethrinoids and drying the resulting mixture to obtain granules which release the active principle in uniform manner.
摘要翻译：通过吸收丙烯酸聚合物和/或丙烯酰胺聚合物的亲水性聚合物制备的颗粒将至少一种活性成分如拟除虫菊酯的水性乳液颗粒化并干燥得到的混合物，得到以均匀的方式释放活性成分的颗粒。

8. 发明授权

US5051306A Microencapsulation product and process 失效
标题翻译：微胶囊化产品和工艺
公开(公告)号：US5051306A
公开(公告)日：1991-09-24
申请号：US527111
申请日：1990-05-21
申请人： Colette Meinard , Claude Taranta
发明人： Colette Meinard , Claude Taranta
IPC分类号： B01J13/14 , A01N25/28 , B01J13/16
CPC分类号： B01J13/16 , A01N25/28 , Y10S514/963 , Y10T428/2985 , Y10T428/2987
摘要： An active principle microencapsulated in an envelope formed by interfacial polymerization of two non-miscible phases A and B, organic phase A comprising at least one water insoluble active principle which do not react with each other, a polyfunctional monomer a and a solvent for the active principle and aqueous phase B comprising a polyfunctional monomber b and a catalyst which allows a progressive diffusion of the active principle and protects the same from the environment.
摘要翻译：通过两个不混溶相A和B的界面聚合形成的包膜微胶囊化的活性成分，包含至少一种不相互反应的水不溶性活性成分的有机相A，多官能单体a和活性溶剂原理和水相B，其包含多官能单体b和催化剂，其允许活性成分的逐渐扩散并保护其不受环境影响。

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