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1. 发明申请

US20120235084A1 LITHIUM-POROUS METAL OXIDE COMPOSITIONS AND LITHIUM REAGENT-POROUS METAL COMPOSITIONS 审中-公开
标题翻译：锂金属氧化物组合物和锂试剂多孔金属组合物
公开(公告)号：US20120235084A1
公开(公告)日：2012-09-20
申请号：US13469299
申请日：2012-05-11
申请人： Michael LEFENFELD , James L. DYE , Partha NANDI , James JACKSON
发明人： Michael LEFENFELD , James L. DYE , Partha NANDI , James JACKSON
IPC分类号： C09K3/00
CPC分类号： C07F1/02 , C01C1/026 , C01D15/00 , C01P2002/86 , C01P2002/87 , C01P2002/89 , C01P2006/16 , Y02P20/52
摘要： The invention relates to lithium metal/porous metal oxide compositions. These lithium metal compositions are prepared by mixing liquid lithium metal with a porous metal oxide in an inert atmosphere under exothermic conditions sufficient to absorb the liquid lithium metal into the porous metal oxide pores. The lithium metal/porous metal oxide compositions of the invention are preferably loaded with lithium metal up to about 40% by weight, with about 20% to 40% by weight being the most preferred loading. The invention also relates to lithium reagent-porous metal oxide compositions having RLi absorbed into a porous oxide. In formula RLi, R is an alkyl group, an alkenyl group, an alkynyl group, an aryl group, an alkaryl group, or an NR1R2 group; R1 is an alkyl group, an alkenyl group, an alkynyl group, an aryl group, an alkaryl group; and R2 is hydrogen, an alkyl group, an alkenyl group, an alkynyl group, an aryl group, and an alkaryl group. The preparation and use of these compositions are also described.
摘要翻译：本发明涉及锂金属/多孔金属氧化物组合物。这些锂金属组合物通过在惰性气氛中将液态锂金属与多孔金属氧化物混合，在足以将液态锂金属吸收到多孔金属氧化物孔中的放热条件下来制备。本发明的锂金属/多孔金属氧化物组合物优选负载高达约40重量％的锂金属，其中最优选的负载量为约20重量％至40重量％。本发明还涉及具有吸收到多孔氧化物中的RLi的锂试剂多孔金属氧化物组合物。在式RLi中，R是烷基，烯基，炔基，芳基，烷芳基或NR1R2基团; R1是烷基，烯基，炔基，芳基，烷芳基; R2是氢，烷基，烯基，炔基，芳基和烷芳基。还描述了这些组合物的制备和用途。

2. 发明申请

US20080111104A1 LITHIUM-POROUS METAL OXIDE COMPOSITIONS AND LITHIUM REAGENT-POROUS METAL COMPOSITIONS 有权
标题翻译：锂金属氧化物组合物和锂试剂多孔金属组合物
公开(公告)号：US20080111104A1
公开(公告)日：2008-05-15
申请号：US11852820
申请日：2007-09-10
申请人： Michael LEFENFELD , James L. DYE , Partha NANDI , James JACKSON
发明人： Michael LEFENFELD , James L. DYE , Partha NANDI , James JACKSON
IPC分类号： H01M4/58 , B05D5/12
CPC分类号： C07F1/02 , C01C1/026 , C01D15/00 , C01P2002/86 , C01P2002/87 , C01P2002/89 , C01P2006/16 , Y02P20/52
摘要： The invention relates to lithium metal/porous metal oxide compositions. These lithium metal compositions are prepared by mixing liquid lithium metal with a porous metal oxide in an inert atmosphere under exothermic conditions sufficient to absorb the liquid lithium metal into the porous metal oxide pores. The lithium metal/porous metal oxide compositions of the invention are preferably loaded with lithium metal up to about 40% by weight, with about 20% to 40% by weight being the most preferred loading. The invention also relates to lithium reagent-porous metal oxide compositions having RLi absorbed into a porous oxide. In formula RLi, R is an alkyl group, an alkenyl group, an alkynyl group, an aryl group, an alkaryl group, or an NR1R2 group; R1 is an alkyl group, an alkenyl group, an alkynyl group, an aryl group, an alkaryl group; and R2 is hydrogen, an alkyl group, an alkenyl group, an alkynyl group, an aryl group, and an alkaryl group. The preparation and use of these compositions are also described.
摘要翻译：本发明涉及锂金属/多孔金属氧化物组合物。这些锂金属组合物通过在惰性气氛中将液态锂金属与多孔金属氧化物混合，在足以将液态锂金属吸收到多孔金属氧化物孔中的放热条件下来制备。本发明的锂金属/多孔金属氧化物组合物优选负载高达约40重量％的锂金属，其中最优选的负载量为约20重量％至40重量％。本发明还涉及具有吸收到多孔氧化物中的RLi的锂试剂多孔金属氧化物组合物。在式RLi中，R是烷基，烯基，炔基，芳基，烷芳基或NR 1 R 2 O 2基; R 1是烷基，烯基，炔基，芳基，烷芳基; R 2是氢，烷基，烯基，炔基，芳基和烷芳基。还描述了这些组合物的制备和用途。

3. 发明申请

US20120201734A1 SILICIDE COMPOSITIONS CONTAINING ALKALI METALS AND METHODS OF MAKING THE SAME 有权
标题翻译：含有碱金属的硅氧烷组合物及其制备方法
公开(公告)号：US20120201734A1
公开(公告)日：2012-08-09
申请号：US13445557
申请日：2012-04-12
申请人： Michael LEFENFELD , James L. DYE
发明人： Michael LEFENFELD , James L. DYE
IPC分类号： C01B33/06 , B08B7/00 , F24J1/00 , C01B3/06
CPC分类号： C11D7/04 , C01B3/06 , C01B3/08 , C01B33/06 , C11D17/042 , F24V30/00 , Y02E60/364
摘要： The invention relates to a method of making alkali metal silicide compositions, and the compositions resulting from the method, comprising mixing an alkali metal with silicon and heating the resulting mixture to a temperature below about 475° C. The resulting compositions do not react with dry O2. Also, the invention relates to sodium silicide compositions having a powder X-ray diffraction pattern comprising at least three peaks with 2Theta angles selected from about 18.2, 28.5, 29.5, 33.7, 41.2, 47.4, and 56.2 and a solid state 23Na MAS NMR spectra peak at about 18 ppm. Moreover, the invention relates to methods of removing a volatile or flammable substance in a controlled manner. Furthermore, the alkali metal silicide compositions of the invention react with water to produce hydrogen gas.
摘要翻译：本发明涉及一种制备碱金属硅化物组合物的方法和由该方法得到的组合物，其包括将碱金属与硅混合并将所得混合物加热至低于约475℃的温度。所得组合物不与干 O2。此外，本发明涉及具有粉末X射线衍射图的硅化钠组合物，其包含至少三个具有选自约18.2,28.5,29.5,33.7,41.2,47.4和56.2的2θ角的峰和固态23Na MAS NMR光谱峰值约为18ppm。此外，本发明涉及以受控方式除去挥发性或易燃物质的方法。此外，本发明的碱金属硅化物组合物与水反应产生氢气。

4. 发明申请

US20100166648A1 SILICA GEL COMPOSITIONS CONTAINING ALKALI METALS AND ALKALI METAL ALLOYS 有权
标题翻译：含有碱金属和碱金属合金的二氧化硅凝胶组合物
公开(公告)号：US20100166648A1
公开(公告)日：2010-07-01
申请号：US12723588
申请日：2010-03-12
申请人： Michael LEFENFELD , James L. Dye
发明人： Michael LEFENFELD , James L. Dye
IPC分类号： C01B3/08 , C07C15/28 , C07C1/00
CPC分类号： B01J35/002 , B01J20/02 , B01J20/103 , B01J20/28047 , B01J20/28078 , B01J20/28097 , B01J20/281 , B01J20/291 , B01J20/3078 , B01J20/3204 , B01J20/3236 , B01J23/04 , B01J37/023 , B01J37/08 , B01J2220/42 , B01J2220/54 , B01J2220/56 , B01J2220/58 , C01B3/001 , C01B3/06 , C07C2/861 , C07C2/868 , C07D333/76 , Y02E60/324 , Y02E60/36 , C07C15/18 , C07C15/14
摘要： The invention relates to Group 1 metal/silica gel compositions comprising silica gel and an alkali metal or alloy, wherein Group 1 metals or alloys are absorbed into the silica gel pores. The invention relates to producing hydrogen gas comprising contacting a Group 1 metal/silica gel composition with water, and further relates to an alkali metal reduction of an organic compound, the improvement comprising contacting the organic compound with a Group 1 metal/silica gel composition. In these embodiments, the Group 1 metal/silica gel composition reacts with dry O2. The invention also relates to producing hydrogen gas comprising contacting a Group 1 metal/silica gel composition with water, and further relates to an alkali metal reduction of an organic compound, the improvement comprising contacting the organic compound with a Group 1 metal/silica gel composition. In these embodiments, the Group 1 metal/silica gel composition produced does not react with dry O2.
摘要翻译：本发明涉及包含硅胶和碱金属或合金的第1族金属/硅胶组合物，其中第1族金属或合金被吸收到硅胶孔中。本发明涉及生产氢气，包括使第1族金属/硅胶组合物与水接触，还涉及有机化合物的碱金属还原，其改进包括使有机化合物与第1族金属/硅胶组合物接触。在这些实施方案中，第1族金属/硅胶组合物与干燥的O 2反应。本发明还涉及生产氢气，包括使第1族金属/硅胶组合物与水接触，还涉及有机化合物的碱金属还原，其改进包括使有机化合物与第1族金属/硅胶组合物。在这些实施方案中，所生产的第1族金属/硅胶组合物不与干燥的O 2反应。

5. 发明申请

US20120199789A1 SILICA GEL COMPOSITIONS CONTAINING ALKALI METALS AND ALKALI METAL ALLOYS 有权
标题翻译：含有碱金属和碱金属合金的二氧化硅凝胶组合物
公开(公告)号：US20120199789A1
公开(公告)日：2012-08-09
申请号：US13197942
申请日：2011-08-04
申请人： Michael LEFENFELD , James L. Dye
发明人： Michael LEFENFELD , James L. Dye
IPC分类号： C09K3/00
CPC分类号： B01J35/002 , B01J20/02 , B01J20/103 , B01J20/28047 , B01J20/28078 , B01J20/28097 , B01J20/281 , B01J20/291 , B01J20/3078 , B01J20/3204 , B01J20/3236 , B01J23/04 , B01J37/023 , B01J37/08 , B01J2220/42 , B01J2220/54 , B01J2220/56 , B01J2220/58 , C01B3/001 , C01B3/06 , C07C2/861 , C07C2/868 , C07D333/76 , Y02E60/324 , Y02E60/36 , C07C15/18 , C07C15/14
摘要： The invention relates to Group 1 metal/silica gel compositions comprising silica gel and an alkali metal or alloy, wherein Group 1 metals or alloys are absorbed into the silica gel pores. The invention relates to producing hydrogen gas comprising contacting a Group 1 metal/silica gel composition with water, and further relates to an alkali metal reduction of an organic compound, the improvement comprising contacting the organic compound with a Group 1 metal/silica gel composition. In these embodiments, the Group 1 metal/silica gel composition reacts with dry O2. The invention also relates to producing hydrogen gas comprising contacting a Group 1 metal/silica gel composition with water, and further relates to an alkali metal reduction of an organic compound, the improvement comprising contacting the organic compound with a Group 1 metal/silica gel composition. In these embodiments, the Group 1 metal/silica gel composition produced does not react with dry O2.
摘要翻译：本发明涉及包含硅胶和碱金属或合金的第1族金属/硅胶组合物，其中第1族金属或合金被吸收到硅胶孔中。本发明涉及生产氢气，包括使第1族金属/硅胶组合物与水接触，还涉及有机化合物的碱金属还原，其改进包括使有机化合物与第1族金属/硅胶组合物接触。在这些实施方案中，第1族金属/硅胶组合物与干燥的O 2反应。本发明还涉及生产氢气，包括使第1族金属/硅胶组合物与水接触，还涉及有机化合物的碱金属还原，其改进包括使有机化合物与第1族金属/硅胶组合物。在这些实施方案中，所生产的第1族金属/硅胶组合物与干燥的O 2不反应。

6. 发明申请

US20100316917A1 SILICIDE COMPOSITIONS CONTAINING ALKALI METALS AND METHODS OF MAKING THE SAME 有权
标题翻译：含有碱金属的硅氧烷组合物及其制备方法
公开(公告)号：US20100316917A1
公开(公告)日：2010-12-16
申请号：US12854510
申请日：2010-08-11
申请人： Michael LEFENFELD , James L. DYE
发明人： Michael LEFENFELD , James L. DYE
IPC分类号： H01M8/06 , C01B33/06 , C01B3/04 , C02F1/68
CPC分类号： C11D7/04 , C01B3/06 , C01B3/08 , C01B33/06 , C11D17/042 , F24V30/00 , Y02E60/364
摘要： The invention relates to a method of making alkali metal silicide compositions, and the compositions resulting from the method, comprising mixing an alkali metal with silicon and heating the resulting mixture to a temperature below about 475° C. The resulting compositions do not react with dry O2. Also, the invention relates to sodium silicide compositions having a powder X-ray diffraction pattern comprising at least three peaks with 2Theta angles selected from about 18.2, 28.5, 29.5, 33.7, 41.2, 47.4, and 56.2 and a solid state 23Na MAS NMR spectra peak at about 18 ppm. Moreover, the invention relates to methods of removing a volatile or flammable substance in a controlled manner. Furthermore, the alkali metal silicide compositions of the invention react with water to produce hydrogen gas.
摘要翻译：本发明涉及一种制备碱金属硅化物组合物的方法和由该方法得到的组合物，其包括将碱金属与硅混合并将所得混合物加热至低于约475℃的温度。所得组合物不与干 O2。此外，本发明涉及具有粉末X射线衍射图的硅化钠组合物，其包含至少三个具有选自约18.2,28.5,29.5,33.7,41.2,47.4和56.2的2θ角的峰和固态23Na MAS NMR光谱峰值约为18ppm。此外，本发明涉及以受控方式除去挥发性或易燃物质的方法。此外，本发明的碱金属硅化物组合物与水反应产生氢气。

7. 发明申请

US20090105430A1 USE OF ALKALI METAL-SILICA GEL (M-SG) MATERIALS IN SOLVENT AND MONOMER DRYING AND PURIFICATION FOR THEIR USE IN ANIONIC POLYMERIZATION 有权
标题翻译：碱性金属硅胶（M-SG）在溶剂中的应用和单体干燥和纯化在阴离子聚合中的应用
公开(公告)号：US20090105430A1
公开(公告)日：2009-04-23
申请号：US12239296
申请日：2008-09-26
申请人： Mana ITO , Stephane CARLOTTI , Alain DEFFIEUX , Michael LEFENFELD
发明人： Mana ITO , Stephane CARLOTTI , Alain DEFFIEUX , Michael LEFENFELD
IPC分类号： C08F2/10
CPC分类号： C07C7/12 , C07C7/14841 , C08F4/025 , C08F4/463 , C08F6/003 , C08F112/08 , Y10S526/912 , C07C11/18 , C07C15/46 , C07C13/18
摘要： Stage I Group 1 metal/porous metal oxide compositions or Stage II Group 1 metal/porous metal oxide compositions are shown to be useful to remove impurities and act as drying agents for various types of solvents and for olefinic monomers used in anionic polymerizations. One important advantage of these compositions is their ability to dry simultaneously solvent and monomers, without inducing a significant polymerization of the latter. Another important characteristic is the capacity of the compositions to be totally inactive toward conventional anionic polymerization which allows them to be left in situ during the polymerization itself.
摘要翻译：阶段I第1族金属/多孔金属氧化物组合物或II级第1族金属/多孔金属氧化物组合物被证明可用于除去杂质并用作各种类型的溶剂和用于阴离子聚合的烯烃单体的干燥剂。这些组合物的一个重要优点是它们能够同时干燥溶剂和单体，而不会引起后者的显着聚合。另一个重要的特征是组合物对于常规的阴离子聚合完全无活性的能力，这允许它们在聚合本身期间留在原位。

8. 发明申请

US20120115054A1 WATER REACTIVE HYDROGEN FUEL CELL POWER SYSTEM 有权
标题翻译：水反应氢燃料电池系统
公开(公告)号：US20120115054A1
公开(公告)日：2012-05-10
申请号：US13291815
申请日：2011-11-08
申请人： Andrew P. WALLACE , John M. MELACK , Michael LEFENFELD
发明人： Andrew P. WALLACE , John M. MELACK , Michael LEFENFELD
IPC分类号： H01M8/06
CPC分类号： H01M8/04208 , C01B3/06 , C01B3/065 , C01B3/08 , F17C11/005 , H01M8/04216 , H01M8/065 , Y02E60/321 , Y02E60/362
摘要： A water reactive hydrogen fueled power system includes devices and methods to combine reactant fuel materials and aqueous solutions to generate hydrogen. The generated hydrogen is converted in a fuel cell to provide electricity. The water reactive hydrogen fueled power system includes a fuel cell, a water feed tray, and a fuel cartridge to generate power for portable power electronics. The removable fuel cartridge is encompassed by the water feed tray and fuel cell. The water feed tray is refillable with water by a user. The water is then transferred from the water feed tray into the fuel cartridge to generate hydrogen for the fuel cell which then produces power for the user.
摘要翻译：水反应性氢燃料动力系统包括将反应物燃料和水溶液组合以产生氢的装置和方法。所产生的氢气在燃料电池中转化以提供电力。水反应性氢燃料电力系统包括燃料电池，供水盘和用于为便携式电力电子产生电力的燃料盒。可拆卸的燃料盒被供水盘和燃料电池包围。供水托盘可由用户重新填充水。然后将水从供水盘传送到燃料盒中，以产生用于燃料电池的氢气，然后为用户产生电力。

9. 发明申请

US20100249476A1 CATALYTIC DEHYDRATION OF ALCOHOLS USING PHASE PURE SINGLE- AND MULTI-SITE HETEROGENEOUS CATALYSTS 有权
标题翻译：使用单相和多种异源催化剂的醇的催化脱氢
公开(公告)号：US20100249476A1
公开(公告)日：2010-09-30
申请号：US12692561
申请日：2010-01-22
申请人： Michael LEFENFELD , Robert RAJA , Alexander James PATERSON , Matthew Edward POTTER
发明人： Michael LEFENFELD , Robert RAJA , Alexander James PATERSON , Matthew Edward POTTER
IPC分类号： C07C1/00 , C01B25/45 , C01B25/36
CPC分类号： B01J29/84 , B01J29/85 , B01J35/1057 , C01B37/065 , C01B37/08 , C01B39/54 , C07C1/24 , C07C2529/84 , C07C2529/85 , Y02P20/52 , C07C11/04 , C07C11/09 , C07C11/06 , C07C15/46
摘要： The disclosure describes a new class of isomorphously metal-substituted aluminophosphate materials with high phase purity that are capable of performing selective Brönsted acid catalyzed chemical transformations, such as transforming alcohols to olefins, with high conversions and selectivities using mild conditions. Isomorphous substitutions of functional metal ions for both the aluminum ions and the phosphorous ions were successful in various AlPO structures, along with multiple metal substitutions into a single aluminum site and/or a phosphorous site. This invention can be used towards the catalytic conversion of hydroxylated compounds of linear and/or branched moiety with the possibility of being substituted to their respective hydrocarbon products, preferably light olefins containing 2 to 10 carbon atoms, among other chemistries.
摘要翻译：本公开描述了一类具有高相纯度的同晶金属取代的磷酸铝材料，其能够使用温和条件进行选择性布朗斯台德酸催化的化学转化，例如将醇转化为烯烃，具有高转化率和选择性。铝离子和磷离子的功能金属离子的同晶取代在各种AlPO结构中成功，以及多个金属取代成单个铝位点和/或磷位置。本发明可以用于线性和/或支化部分的羟基化化合物的催化转化，并且可以将其取代为各自的烃产物，优选含有2至10个碳原子的轻质烯烃等化学物质。

10. 发明申请

US20090187486A1 METHOD AND APPARATUS FOR DELIVERING TARGETED CONTENT 审中-公开
标题翻译：用于传递目标内容的方法和装置
公开(公告)号：US20090187486A1
公开(公告)日：2009-07-23
申请号：US12355452
申请日：2009-01-16
申请人： Michael LEFENFELD , Randall DAVIS
发明人： Michael LEFENFELD , Randall DAVIS
IPC分类号： G06Q30/00 , G06F17/30
CPC分类号： G06Q30/0277 , G06Q30/02
摘要： Embodiments of the present invention permit a user to receive content that is directly targeted to that particular user's interests, including a method for targeting content that is arranged on a page that is displayable by a computing device, including the steps of displaying a list of categories of available advertising content, wherein the available advertising content is stored in a database, receiving a selection of at least one of the categories of the advertising content from a user, selecting advertising content from the database that corresponds to the selection of categories received from the user, and transmitting a page including the selected advertising content to a computing device for display on the computing device. In addition, embodiments of the present invention allow the tracking of content from when it is initially shared, to when revenue is generated based on an action of a user on the shared content portion.
摘要翻译：本发明的实施例允许用户接收直接针对该特定用户兴趣的内容，包括用于定位布置在可由计算设备显示的页面上的内容的方法，包括以下步骤：显示类别列表可用的广告内容，其中所述可用的广告内容存储在数据库中，从用户接收对所述广告内容的类别中的至少一个的选择，从所述数据库中选择与从所述广告内容接收的类别的选择相对应的广告内容用户，并且将包括所选择的广告内容的页面发送到计算设备以在所述计算设备上显示。此外，本发明的实施例允许从原始共享的内容到内容的跟踪，基于用户对共享内容部分的动作来生成收入。

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