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1. 发明授权

US4557976A Heat-hardenable binder mixture 失效
标题翻译：热硬化粘合剂混合物
公开(公告)号：US4557976A
公开(公告)日：1985-12-10
申请号：US526072
申请日：1983-08-24
申请人： Michael Geist , Horst Diefenbach
发明人： Michael Geist , Horst Diefenbach
IPC分类号： C08G59/40 , C08G59/42 , C08G59/58 , C09D5/44 , C09D163/00 , C09D201/00 , B05D3/02 , B32B15/08 , B32B27/38 , C08L63/00
CPC分类号： C09D163/00 , C08G59/4042 , C08G59/42 , C08G59/4261 , C08G59/4284 , C08G59/58 , C09D201/00 , C09D5/4496 , Y10T428/31511 , Y10T428/31529 , Y10T428/31551 , Y10T428/31605
摘要： The invention relates to a heat-hardenable binder mixture which comprises(A) an organic nonacidic resin having a hydroxyl group content of at least 0.2 equivalent in 100 g of resin and having a molecular weight of at least 850, and(B) a crosslinking agent based on an organic compound which contains at least 2 carbalkoxymethyl ester groups per molecule.
摘要翻译：本发明涉及一种可热硬化的粘合剂混合物，其包含（A）在100g树脂中具有至少0.2当量的羟基含量且分子量至少为850的有机非酸树脂，和（B）交联基于每分子含有至少2个烷氧基甲基酯基团的有机化合物的试剂。

2. 发明授权

US4547409A Self-crosslinking heat-curable binder 失效
标题翻译：自交联热固性粘合剂
公开(公告)号：US4547409A
公开(公告)日：1985-10-15
申请号：US657062
申请日：1984-10-02
申请人： Michael Geist , Horst Diefenbach
发明人： Michael Geist , Horst Diefenbach
IPC分类号： C08G18/08 , C08G59/42 , C08G59/56 , C08G59/58 , C09D5/44 , C08L67/04
CPC分类号： C09D5/44 , C08G18/0814 , C08G59/4284 , C08G59/56 , C08G59/58 , Y10T428/31511 , Y10T428/31551
摘要： The invention relates to a self-crosslinking heat-curable binder, in particular for electropaints, which is based on an organic synthetic resin which contains primary and/or secondary and, if desired, also tertiary amino groups and esterified carboxyl groups and is water-dilutable due to partial or complete neutralization with acids. The esterified carboxyl groups are activated in the alcohol component by a substituent which induces a negative inductive effect.
摘要翻译：本发明涉及一种自交联热固化性粘合剂，特别是电穿孔，其基于有机合成树脂，该有机合成树脂含有伯和/或仲和如果需要也含有叔氨基和酯化的羧基，由于部分或完全用酸中和而可稀释。酯化的羧基在醇组分中通过引起负诱导作用的取代基活化。

3. 发明授权

US5712349A Water dispersible binders for cationic electrocoating finishes and a process for their preparation 失效
标题翻译：用于阳离子电泳涂饰的水分散性粘合剂及其制备方法
公开(公告)号：US5712349A
公开(公告)日：1998-01-27
申请号：US744554
申请日：1996-11-06
申请人： Horst Diefenbach , Arnold Dobbelstein , Michael Geist
发明人： Horst Diefenbach , Arnold Dobbelstein , Michael Geist
IPC分类号： C08G59/02 , C08G59/14 , C09D5/44 , C08L63/00
CPC分类号： C08G59/02 , C08G59/1433 , C09D5/4434
摘要： The invention relates to water-dispersible binders for cationic electrocoating finishes, which binders are reaction products of (A) low molecular weight epoxide resins containing aromatic groups and having an epoxide equivalent weight of below 375, (B) aliphatic and/or alicyclic polyfunctional alcohols and/or carboxylic acids having a molecular weight of below 350, (C) if appropriate up to 60% by weight, relative to the total binder, of polyfunctional alcohols, carboxylic acids and/or SH compounds having a molecular weight of 500-5,000 and (D) primary, secondary and/or tertiary amines and/or salts thereof or a sulfide/acid mixture or a phosphine/acid mixture, the reaction product of A and B containing 10-45% of aromatic groups, calculated as the phenylene group. By means of the binders, a higher layer thickness is obtained in electrocoating.
摘要翻译：本发明涉及用于阳离子电泳涂饰的水分散性粘合剂，其中粘合剂是（A）含有芳族基团且环氧当量重量低于375的低分子量环氧树脂的反应产物，（B）脂族和/或脂环族多官能醇和/或分子量低于350的羧酸，（C）如果合适，相对于总粘合剂，最多60重量％的分子量为500-5,000的多官能醇，羧酸和/或SH化合物和（D）伯，仲和/或叔胺和/或其盐或硫化物/酸混合物或膦/酸混合物，A和B的反应产物含有10-45％的芳族基团，计算为亚苯基组。通过粘合剂，在电涂覆中获得较高的层厚度。

4. 发明授权

US4548965A Water-dispersible binders for cationic electrocoating finishes, and process for their preparation 失效
标题翻译：用于阳离子电泳涂饰的水分散性粘合剂及其制备方法
公开(公告)号：US4548965A
公开(公告)日：1985-10-22
申请号：US648171
申请日：1984-08-31
申请人： Michael Geist , Horst Diefenbach , Arnold Dobbelstein
发明人： Michael Geist , Horst Diefenbach , Arnold Dobbelstein
IPC分类号： C08G59/04 , C08G59/14 , C08G59/62 , C09D5/44 , C09D3/58 , C09D5/02
CPC分类号： C09D5/4434
摘要： The invention relates to water-dispersible binders for cationic electrocoating finishes, which are obtained by reaction of(A) epoxy resins containing low molecular weight aromatic groups and having an epoxide equivalent weight of less than 375 with(B) aliphatic and/or alicyclic polyfunctional alcohols or carboxylic acids having a number average molecular weight of less than 350, further reaction of the product of (A) and (B) with(C) a polyfunctional alcohol having a molecular weight of more than 350, addition at the epoxide groups taking place so that the reaction products of (A) and (B) contain an amount of aromatic groups of from 10 to 45% by weight, calculated as phenylene groups, and further modification of the resulting intermediate with(D) primary and/or secondary amines or ammonium salts in order to achieve the required water-dispersibility. The binders contain, as component (C), 5 to 40% by weight, based on the total binder, of a linear polyalkylene ether diol which has on average one terminal primary and one terminal secondary hydroxyl group per molecule and corresponds to the general formula ##STR1## in which n denotes 1 to 4, preferably 1, and m denotes 4 to 35, preferably 5 to 20.
摘要翻译： PCT No.PCT / DE84 / 00003 Sec。 371日期1984年8月31日 102（e）日期1984年8月31日PCT提交1985年1月5日PCT公布。出版物WO84 / 02712 日本1984年7月19日。本发明涉及阳离子电泳涂饰用水分散性粘合剂，其通过（A）含有低分子量芳族基团且环氧当量小于375的环氧树脂与（B ）数均分子量小于350的脂族和/或脂环族多官能醇或羧酸，（A）和（B）的产物与（C）分子量大于350的多官能醇进一步反应在（A）和（B）的反应产物中含有一定量的作为亚苯基计算的10至45重量％的芳族基团并进一步改性（（ D）伯胺和/或仲胺或铵盐，以达到所需的水分散性。作为组分（C），粘合剂含有基于总粘合剂的5至40重量％的线性聚亚烷基醚二醇，其每分子平均具有一个末端伯和一个末端仲羟基，并且对应于通式其中n表示1至4，优选1，m表示4至35，优选5至20。

5. 发明授权

US4477642A Selfcrosslinking heat-hardenable binder 失效
标题翻译：自交联热硬化粘合剂
公开(公告)号：US4477642A
公开(公告)日：1984-10-16
申请号：US526071
申请日：1983-08-24
申请人： Michael Geist , Horst Diefenbach
发明人： Michael Geist , Horst Diefenbach
IPC分类号： C08G18/08 , C08G18/32 , C08G59/42 , C08G59/56 , C08G59/58 , C09D5/44 , C09D163/00 , C09D175/00 , C09D201/02 , C08G18/34
CPC分类号： C08G18/0814 , C08G18/3221 , C08G59/4284 , C08G59/56 , C08G59/58 , C09D5/4446 , C09D5/4488 , Y10T428/31529 , Y10T428/31605
摘要： The invention relates to a selfcrosslinking heat-hardenable binder, in particular for electropaints, which is based on an organic synthetic resin which contains hydroxyl groups and esterified carboxyl groups in the form of carbalkoxymethyl ester groups and is water-dilutable by partial or complete acid-neutralization of amino groups present in the resin.
摘要翻译：本发明涉及一种自交联热硬化性粘合剂，特别是用于电极的自交联热粘合剂，其基于含有羟基的有机合成树脂和以烷氧基甲基酯基形式的酯化羧基，并且可通过部分或完全酸 - 中和树脂中存在的氨基。

6. 发明授权

US4788260A Water-dispersible binders for cationic electropaints, and a process for their preparation 失效
标题翻译：用于阳离子电极的水分散性粘合剂及其制备方法
公开(公告)号：US4788260A
公开(公告)日：1988-11-29
申请号：US471738
申请日：1983-03-03
申请人： Wolfgang Batzill , Horst Diefenbach , Michael Geist , Eberhard Schupp
发明人： Wolfgang Batzill , Horst Diefenbach , Michael Geist , Eberhard Schupp
IPC分类号： C08G59/00 , C08G59/02 , C08G59/14 , C08G59/56 , C08G59/62 , C09D5/44 , C08F283/04 , C08L63/00
CPC分类号： C09D5/4446 , C08G59/02 , C08G59/56 , C08G59/621
摘要： The invention relates to water-dispersible binders which are intended for cationic electropaints and are based on reaction products which are formed from modified epoxy resins and primary and/or secondary amines and which can, if desired, also contain crosslinking agents, pigments, flow-control agents and other customary auxiliaries. They contain as reaction products those which have been prepared by reacting(A) low molecular weight epoxy resins which contain epoxy compound aromatic groups and have an epoxide equivalent weight of less than 375 with(B) aliphatic and/or alicyclic polyfunctional alcohols having hydroxyl groups or carboxylic acids having carboxylic groups and both having a molecular weight of less than 350 and addition of the hydroxyl groups and carboxylic groups to the epoxy groups of (A) in such a way that the reaction products of (A) and (B) contain 10-45% of aromatic groups, calculated as the phenylene group, and have terminal epoxy groups.(C) reacting the terminal epoxy groups of the reaction products of (A) and (B), and thus chain-lengthening, with the phenolic hydroxyl groups of a mononuclear or polynuclear phenol which has at least two phenolic hydroxyl groups and at east one .alpha.,.beta.-olefinically unsaturated amidomethyl group of the following general formula ##STR1## as a substituent on the aromatic rings(s) and in which R.sup.1 and R.sup.2 are identical to or different from one another and represent hydrogen or a methyl group, and(D) reacting the intermediate procuct obtained from (A), (B) and (C) with a primary or secondary amine or an ammonium salt.
摘要翻译：本发明涉及用于阳离子电穿孔剂的水分散性粘合剂，并且基于由改性环氧树脂和伯胺和/或仲胺形成的反应产物，并且如果需要，其也可以含有交联剂，颜料，控制剂和其他常规助剂。它们包含作为反应产物的那些反应产物，它们是通过（A）含有环氧化合物芳族基团并且具有小于375的环氧当量的低分子量环氧树脂与（B）具有羟基的脂族和/或脂环族多官能醇反应而制备的或具有羧基的羧酸，并且分子量小于350，并且以（A）和（B）的反应产物含有（A）和（B）的反应产物的方式向（A）的环氧基添加羟基和羧基， 10-45％芳族基团，以亚苯基计算，并具有末端环氧基团。（C）将（A）和（B）的反应产物的末端环氧基与链长延长与具有至少两个酚羟基的单核或多核苯酚的酚羟基反应，并在东一 α，α-烯属不饱和酰胺基甲基，作为芳环上的取代基，其中R 1和R 2彼此相同或不同，表示氢或甲基，和（D）使得自（A），（B）和（C）得到的中间产物与伯胺或仲胺或铵盐反应。

7. 发明授权

US4686249A Heat-hardenable binder mixture of amino resin and hydroxy epoxides 失效
标题翻译：氨基树脂和羟基环氧化物的热可硬化粘合剂混合物
公开(公告)号：US4686249A
公开(公告)日：1987-08-11
申请号：US769697
申请日：1985-08-27
申请人： Horst Diefenbach , Michael Geist
发明人： Horst Diefenbach , Michael Geist
IPC分类号： C08K5/00 , C08G59/00 , C08G59/40 , C08K5/10 , C08L33/00 , C08L33/02 , C08L63/00 , C08L67/00 , C08L101/00 , C09D5/03 , C09D5/44 , C09D5/46 , C09D133/06 , C09D201/02 , C08L79/00
CPC分类号： C09D133/06 , C09D201/02 , C09D5/4496 , Y10T428/31511 , Y10T428/31529 , Y10T428/31551 , Y10T428/31605 , Y10T428/31699 , Y10T428/31935
摘要： A heat-hardenable binder mixture based on organic resins comprises an organic resin having primary and/or secondary and, if appropriate, also additional tertiary amino groups and a crosslinking agent based on an organic compound which contains at least 2 .beta.-hydroxyalkyl ester groups. The binder mixture can additionally contain pigments, fillers, crosslinking catalysts, corrosion inhibitors and other paint auxiliaries. The binder mixture is used in a process for preparing coatings by applying a coating agent in the form of a film to a substrate and subsequently hardening the film by stoving.
摘要翻译：基于有机树脂的热可硬化粘合剂混合物包括具有伯和/或仲和有时也适用的另外的叔氨基的有机树脂和基于含有至少2个β-羟基烷基酯基团的有机化合物的交联剂。粘合剂混合物可另外含有颜料，填料，交联催化剂，腐蚀抑制剂和其它涂料助剂。粘合剂混合物用于通过将膜形式的涂布剂施加到基材上并随后通过烘烤硬化来制备涂层的方法。

8. 发明授权

US4495335A Self-crosslinking heat-curable binder 失效
标题翻译：自交联热固性粘合剂
公开(公告)号：US4495335A
公开(公告)日：1985-01-22
申请号：US472639
申请日：1983-03-07
申请人： Michael Geist , Horst Diefenbach
发明人： Michael Geist , Horst Diefenbach
IPC分类号： C08G18/08 , C08G59/42 , C08G59/56 , C08G59/58 , C09D5/44 , C09D201/02 , C08L67/04
CPC分类号： C08G59/58 , C08G18/0814 , C08G59/4284 , C08G59/56 , C09D5/4446 , C09D5/4465 , C09D5/4488
摘要： The invention relates to a self-crosslinking heatcurable binder, in particular for electropaints, which is based on an organic synthetic resin which contains primary and/or secondary and, if desired, also tertiary amino groups and esterified carboxyl groups and is water-dilutable due to partial or complete neutralization with acids. The esterified carboxyl groups are activated in the alcohol component by a substituent which induces a negative inductive effect.
摘要翻译：本发明涉及一种自交联热固性粘合剂，特别是对于电极，其基于有机合成树脂，该有机合成树脂包含伯和/或仲和如果需要也含有叔氨基和酯化的羧基并且是可水稀释的部分或完全用酸中和。酯化的羧基在醇组分中通过引起负诱导作用的取代基活化。

9. 发明授权

US4477530A Heat-hardenable binder mixture 失效
标题翻译：热硬化粘合剂混合物
公开(公告)号：US4477530A
公开(公告)日：1984-10-16
申请号：US425078
申请日：1982-09-23
申请人： Horst Diefenbach , Michael Geist
发明人： Horst Diefenbach , Michael Geist
IPC分类号： C08K5/00 , C08G59/00 , C08G59/40 , C08K5/10 , C08L33/00 , C08L33/02 , C08L63/00 , C08L67/00 , C08L101/00 , C09D5/03 , C09D5/44 , C09D5/46 , C09D133/06 , C09D201/02 , B32B27/38 , B05D3/02
CPC分类号： C09D133/06 , C09D201/02 , C09D5/4496 , Y10T428/31511 , Y10T428/31529 , Y10T428/31551 , Y10T428/31605 , Y10T428/31699 , Y10T428/31935
摘要： A heat-hardenable binder mixture based on organic resins comprises an organic resin having primary and/or secondary and, if appropriate, also additional tertiary amino groups and a crosslinking agent based on an organic compound which contains at least 2 .beta.-hydroxyalkyl ester groups. The binder mixture can additionally contain pigments, fillers, crosslinking catalysts, corrosion inhibitors and other paint auxiliaries. The binder mixture is used in a process for preparing coatings by applying a coating agent in the form of a film to a substrate and subsequently hardening the film by stoving.
摘要翻译： PCT No.PCT / DE82 / 00015 Sec。 371日期1982年9月23日 102（e）1982年9月23日PCT PCT。1982年1月26日PCT。基于有机树脂的热可硬化粘合剂混合物包括具有伯和/或次级的有机树脂，如果合适的话，还有另外的叔氨基和基于含有至少2个β-羟基烷基酯基团的有机化合物的交联剂。粘合剂混合物可另外含有颜料，填料，交联催化剂，腐蚀抑制剂和其它涂料助剂。粘合剂混合物用于通过将膜形式的涂布剂施加到基材上并随后通过烘烤硬化来制备涂层的方法。

10. 发明授权

US4436878A Water-dispersible binders for cationic electropaints, and a process for their preparation 失效
标题翻译：用于阳离子电极的水分散性粘合剂及其制备方法
公开(公告)号：US4436878A
公开(公告)日：1984-03-13
申请号：US471739
申请日：1983-03-03
申请人： Wolfgang Batzill , Horst Diefenbach , Michael Geist , Eberhard Schupp
发明人： Wolfgang Batzill , Horst Diefenbach , Michael Geist , Eberhard Schupp
IPC分类号： C08G59/00 , C08G59/02 , C08G59/14 , C08G59/56 , C08G59/62 , C09D5/44 , C08L63/00
CPC分类号： C08G59/621 , C08G59/02 , C08G59/1477 , C08G59/56 , C09D5/4446 , Y10S524/901
摘要： The invention relates to water-dispersible binders which are intended for cationic electropaints and are based on reaction products which are formed from modified epoxy resins and primary and/or secondary amines and which can, if desired, also contain crosslinking agents, pigments, flow-control agents and other customary auxiliaries. The reaction products have been prepared by reacting(A) Low molecular weight epoxy resins which contain aromatic groups and have an epoxide equivalent weight of less than 375 with(B) aliphatic and/or alicyclic polyfunctional alcohols or carboxylic acids having a molecular weight of less than 350 by addition to the epoxy group in such a way that the reaction products contain 10-45% of aromatic groups, calculated as phenylene group, and reacting the reaction products of A and B with(C) if desired up to 60% by weight, relative to total binder, of polyfunctional alcohols, carboxylic acids and/or SH compounds having a molecular weight of 300-5,000, the molar ratios of (A), (B) and, if desired, (C) being chosen in such a way that the resulting intermediate product has terminal epoxy groups,(D) by reacting the intermediate product by the addition of a phenolic hydroxyl group of a monophenol and/or diphenol to the epoxy groups, the monophenol or diphenol having as a substituent on the aromatic ring(s) at least one grouping of the general formula ##STR1## in which R.sup.1 and R.sup.2 are identical to or different from one another and represent hydrogen or a methyl group, and by adding a primary and/or secondary amine before or after the reaction of the phenolic hydroxyl groups with the epoxy groups, to at least some of the double bonds of the grouping of the formula (I).
摘要翻译：本发明涉及用于阳离子电穿孔剂的水分散性粘合剂，并且基于由改性环氧树脂和伯胺和/或仲胺形成的反应产物，并且如果需要，其也可以含有交联剂，颜料，控制剂和其他常规助剂。反应产物通过（A）含有芳族基团并且具有小于375的环氧当量重量的低分子量环氧树脂与（B）分子量较小的（B）脂族和/或脂环族多官能醇或羧酸反应制备通过加入环氧基，使反应产物含有10-45％的芳族基团，以亚苯基计算，并且如果需要，将A和B的反应产物与（C）反应直到60％相对于总粘合剂，分子量为300-5,000的多官能醇，羧酸和/或SH化合物的重量，（A），（B）的摩尔比和如果需要，（C）选自于所得到的中间产物具有末端环氧基的方式，（D）通过将酚类羟基和/或二酚加成到环氧基上，通过使中间产物与酚类作为取代基的单酚或二酚反应芳香至少一个通式为其中R 1和R 2彼此相同或不同并且代表氢或甲基的通式（I）的至少一个基团，并且通过加入伯胺和/或仲胺在酚羟基与环氧基反应之前或之后，至少部分式（I）的组的双键。

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