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1. 发明授权

US4263266A Process for the preparation of crystalline, alkaline, aluminosilicate 失效
标题翻译：制备结晶，碱性，硅铝酸盐的方法
公开(公告)号：US4263266A
公开(公告)日：1981-04-21
申请号：US86128
申请日：1979-10-18
申请人： Max Michel , Georges Vrisakis , Laurent Seigneurin , Gilbert Bouge
发明人： Max Michel , Georges Vrisakis , Laurent Seigneurin , Gilbert Bouge
IPC分类号： C01B39/02 , C01B39/16 , C11D3/12 , C01B33/28
CPC分类号： C11D3/128 , C01B33/2815 , Y10S423/24
摘要： A crystalline, alkali metal aluminosilicate of type 4A is prepared by reaction between an aqueous solution of an alkali metal silicate and an aqueous solution of an alkali metal aluminate, and includes the steps of (i) introducing a flow of at least a portion of at least one of said reactant solutions into a reaction zone; (ii) co-introducing with said flow (i) an in line flow of at least a portion of the other reactant solution into said reaction zone; (iii) thus establishing in said reaction zone a liquid mixture of said aqueous reactant solutions and said liquid admixture comprising a gel-formation medium; (iv) establishing gel-formation elevated temperatures within said gel-formation medium to effect formation of a mixture comprising an aluminosilicate gel-phase and a mother liquid; (v) recycling said gel-phase/mother liquor to said flow (i); (vi) maintaining said gel-phase comprising said gel-formation medium under such elevated temperatures for such period of time as to effect crystallization of the aluminosilicate, and whereby a suspension of aluminosilicate crystals of type 4A in liquid phase results; and (vii) thence recovering said aluminosilicate crystals from said resulting liquid phase.The resultant aluminosilicate crystals are useful, e.g., detergent additives.
摘要翻译：通过碱金属硅酸盐的水溶液和碱金属铝酸盐的水溶液之间的反应制备4A型结晶的碱金属硅铝酸盐，并且包括以下步骤：（i）引入至少一部分在所述反应物溶液中的至少一种进入反应区; （ii）与所述流（i）共同引入至少一部分其它反应物溶液的入口流入所述反应区; （iii）因此在所述反应区域中建立所述反应物水溶液和所述液体混合物的液体混合物，其包含凝胶形成介质; （iv）在所述凝胶形成介质内建立凝胶形成升高的温度以形成包含硅铝酸盐凝胶相和母液的混合物; （v）将所述凝胶相/母液再循环至所述流（i）; （vi）将所述凝胶形成介质的所述凝胶相在这样升高的温度下保持一段时间，以使铝硅酸盐发生结晶，由此产生液相中的4A型硅铝酸盐晶体的悬浮液; 和（vii）从所述液相中回收所述硅铝酸盐晶体。所得的铝硅酸盐晶体是有用的，例如洗涤剂添加剂。

2. 发明授权

US4315839A Spheroidal alumina particulates having bifold porosity and process for their preparation 失效
标题翻译：具有双孔孔隙的球状氧化铝颗粒及其制备方法
公开(公告)号：US4315839A
公开(公告)日：1982-02-16
申请号：US124778
申请日：1980-02-26
申请人： Gilbert Bouge , Roland Jacques , Regis Poisson , Laurent Seigneurin
发明人： Gilbert Bouge , Roland Jacques , Regis Poisson , Laurent Seigneurin
IPC分类号： B01J2/08 , B01J21/04 , B01J35/10 , C01F7/02 , C01F7/14 , B01J35/08
CPC分类号： B01J21/04 , B01J2/08 , B01J35/10 , C01F7/02 , C01F7/141 , B01J35/1019 , B01J35/1042 , B01J35/1061 , B01J35/109 , C01P2002/02 , C01P2002/60 , C01P2002/70 , C01P2004/32 , C01P2004/61 , C01P2006/12 , C01P2006/13 , C01P2006/14 , C01P2006/16 , C01P2006/21 , Y10S502/503
摘要： Spheroidal alumina particulates having bifold porosity are prepared by (i) intimately admixing, at a pH of less than about 7.5, (a) a sol of a member selected from the group consisting of ultrafine boehmite and pseudo-boehmite, said sol being devoid of amorphous alumina and the concentration by weight thereof, in content by weight of Al.sub.2 O.sub.3, being between 5 and 25%, with (b) from 30 to 95% by weight, based upon the total solids content of the admixture, of spheroidal alumina particulates essentially completely in at least one of the phases eta, gamma, delta and theta, such particulates having a micropore volume ranging from about 0.4 to 1 cm.sup.3 /g, a specific surface ranging from about 100 to 350 m.sup.2 /g, and particle diameters ranging from about 1 to 50 microns; (ii) prilling said intimate admixture into spheroidal particulates and gelling the same; and then, (iii) recovering, drying and calcining said gelled particulates at a temperature of from 550.degree. to 1100.degree. C.The resultant particulates having bifold porosity are useful as catalysts or catalyst supports.
摘要翻译：通过（i）在小于约7.5的pH下，（a）选自由超细勃姆石和假勃姆石组成的组中的成员的溶胶紧密混合，制备具有双重孔隙度的球状氧化铝颗粒，所述溶胶不含无定形氧化铝及其以Al 2 O 3的重量含量为5-25％的重量浓度，（b）基于混合物的总固体含量为30至95重量％，基本上为球形氧化铝颗粒完全在相中的至少一个阶段eta，γ，δ和θ，这样的微粒具有约0.4至1cm 3 / g的微孔体积，约100至350m 2 / g的比表面积，约1至50微米; （ii）将所述紧密混合物造粒成球状颗粒并凝胶化; 然后，（iii）在550℃至1100℃的温度下回收，干燥和煅烧所述凝胶状颗粒。所得到的具有二叉孔隙的颗粒可用作催化剂或催化剂载体。

3. 发明授权

US4344928A Process for preparing alumina particulates, at least a fraction of which being ultrafine boehmite 失效
$Process for preparing alumina particulates, at least a fraction of which being ultrafine boehmite$
标题翻译：制备氧化铝微粒的方法，其至少一部分是超细勃姆石
公开(公告)号：US4344928A
公开(公告)日：1982-08-17
申请号：US124777
申请日：1980-02-26
申请人： Thierry Dupin , Gilbert Bouge , Laurent Seigneurin
发明人： Thierry Dupin , Gilbert Bouge , Laurent Seigneurin
IPC分类号： C01F7/02 , C01F7/44 , C09C1/40
CPC分类号： C01F7/448 , C01F7/02 , C01F7/447 , C09C1/407 , C01P2002/01 , C01P2002/02 , C01P2002/04 , C01P2002/60 , C01P2002/72 , C01P2004/03 , C01P2004/10 , C01P2004/22 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2006/12
摘要： Aqueous suspensions of alumina particulates, at least a portion of which comprising ultrafine boehmite, are prepared by maintaining a pH
摘要翻译：氧化铝颗粒的水性悬浮液，其至少一部分包含超细勃姆石，通过将不良结晶和/或无定形活性氧化铝粉末的pH <9水性制剂保持在这样的时间段来制备，以实现至少部分转化这种氧化铝粉末成为超细勃姆石。

4. 发明授权

US4388288A Preparation of shaped titanium dioxide catalyst/carrier and catalysis of gaseous sulfur compounds therewith 失效
标题翻译：成型二氧化钛催化剂/载体的制备和气态硫化合物的催化
公开(公告)号：US4388288A
公开(公告)日：1983-06-14
申请号：US256978
申请日：1981-04-23
申请人： Thierry Dupin , Gilbert Bouge , Regis Poisson
发明人： Thierry Dupin , Gilbert Bouge , Regis Poisson
IPC分类号： B01D53/86 , B01J21/06 , C01B17/04 , C01B17/16 , C01B31/26
CPC分类号： B01J21/063 , B01D53/8603 , C01B17/0434 , C01B17/0456 , C01B17/165
摘要： Shaped titanium oxide catalysts/carriers useful, e.g., for sulfur recovery via Claus catalysis, are prepared by (i) intimately admixing powdered, poorly crystalline and/or amorphous titanium oxide, said titanium oxide powder being characterized by a weight loss on ignition ranging from 1 to 50%, water and from 0 to about 15% by weight of a shaping additive, (ii) next shaping the intimate admixture which results, and (iii) thence, optionally after drying, calcining the product shaped article.
摘要翻译：用于例如通过克劳斯催化进行硫回收的有形钛氧化钛催化剂/载体是通过以下方法来制备的：（i）将粉末状，结晶性差的和/或无定形的氧化钛紧密混合，所述氧化钛粉末的特征在于重量损失， 1至50％，水和0至约15重量％的成型添加剂，（ii）接下来对形成的紧密混合物进行成型，和（iii）然后任选地在干燥之后煅烧产品成型制品。

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