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1. 发明授权

US08104621B2 Method for grading a particulate water-absorbing resin 有权
标题翻译：颗粒状吸水树脂的分级方法
公开(公告)号：US08104621B2
公开(公告)日：2012-01-31
申请号：US11813306
申请日：2005-12-31
申请人： Matthias Weismantel , Rüdiger Funk , Thomas Daniel , Uwe Stueven
发明人： Matthias Weismantel , Rüdiger Funk , Thomas Daniel , Uwe Stueven
IPC分类号： B07B1/46
CPC分类号： B07B1/56 , B07B1/40 , B07B1/46
摘要： Process for classifying a particulate water-absorbing resin using a sieving apparatus at a reduced pressure compared with the ambient pressure and a sieving apparatus for classifying a particulate water-absorbing resin at a reduced pressure compared with the ambient pressure.
摘要翻译：使用与环境压力相比减压的筛分装置对颗粒状吸水性树脂进行分级的方法以及与环境压力相比在减压下分级粒状吸水性树脂的筛分装置。

2. 发明授权

US08349946B2 Production of a water-absorbing resin to which a particulate additive is admixed 失效
标题翻译：生产混合有微粒添加剂的吸水性树脂
公开(公告)号：US08349946B2
公开(公告)日：2013-01-08
申请号：US12861338
申请日：2010-08-23
申请人： Uwe Stueven , Rüdiger Funk , Matthias Weismantel , Thomas Daniel , Annemarie Hillebrecht , Dominicus van Esbroeck , Karl J. Possemiers
发明人： Uwe Stueven , Rüdiger Funk , Matthias Weismantel , Thomas Daniel , Annemarie Hillebrecht , Dominicus van Esbroeck , Karl J. Possemiers
IPC分类号： C08G18/63
CPC分类号： C08F2/44 , C08F220/06 , C08F222/1006
摘要： The invention relates to a process for producing a water-absorbing resin by polymerization of a reaction mixture comprising at least one hydrophilic monomer and, if appropriate, at least one crosslinker in a reactor, which comprises admixing the reaction mixture with at least one first portion of a particulate additive before the reaction mixture has reached a residence time of 40% of the overall residence time in the reactor and with at least one second portion of a particulate additive when the reaction mixture has reached a residence time of 45% or more of the overall residence time in the reactor, the additive being selected from water-absorbing resin powders, fillers and mixtures thereof, the total solids content of monomer and additive being in the range from 30% to 60% by weight, the amount of additive being in the range from 5% to 50% by weight, based on the monomers, and the weight ratio of the first portion to the second portion of the additive being in the range from 10:1 to 1:5. The resin powder is recycled fine-sized material for example. Not only the residual monomer content, specifically the residual crosslinker content, but also the level of extractables in the water-absorbing resin are reduced by the method of addition described. A high fraction of additives can be incorporated without the properties of the water-absorbing resin obtained being adversely affected. The additives enter a sufficiently firm bond with the resin, so that no excessive dusting occurs on exposure to mechanical stress.
摘要翻译：本发明涉及通过聚合包含至少一种亲水单体和如果合适的反应器中至少一种交联剂的反应混合物来生产吸水树脂的方法，其包括将反应混合物与至少一个第一部分的反应混合物在反应混合物的停留时间达到总反应器停留时间的40％的停留时间和至少一个第二部分的颗粒状添加剂之前，当反应混合物达到45％或更多的停留时间时，在反应器中的总停留时间，添加剂选自吸水树脂粉末，填料及其混合物，单体和添加剂的总固体含量在30重量％至60重量％的范围内，添加剂的量为基于单体的5重量％至50重量％的范围，并且添加剂的第一部分与第二部分的重量比在10:1至 1：5。树脂粉末是例如再循环的精细尺寸的材料。通过所述的添加方法，不仅残留单体含量，特别是残留交联剂含量，而且吸水性树脂中的可萃取物的含量都降低。可以并入高分数的添加剂，而不会对获得的吸水性树脂的性能产生不良影响。添加剂与树脂进行足够牢固的粘合，使得在暴露于机械应力时不会发生过度的除尘。

3. 发明申请

US20100324212A1 Production of a Water-Absorbing Resin to Which a Particulate Additive is Admixed 失效
标题翻译：混合颗粒添加剂的吸水树脂的生产
公开(公告)号：US20100324212A1
公开(公告)日：2010-12-23
申请号：US12861338
申请日：2010-08-23
申请人： Uwe Stueven , Rüdiger Funk , Matthias Weismantel , Thomas Daniel , Annemarie Hillebrecht , Dominicus van Esbroeck , Karl J. Possemiers
发明人： Uwe Stueven , Rüdiger Funk , Matthias Weismantel , Thomas Daniel , Annemarie Hillebrecht , Dominicus van Esbroeck , Karl J. Possemiers
IPC分类号： C08K3/34
CPC分类号： C08F2/44 , C08F220/06 , C08F222/1006
摘要： The invention relates to a process for producing a water-absorbing resin by polymerization of a reaction mixture comprising at least one hydrophilic monomer and, if appropriate, at least one crosslinker in a reactor, which comprises admixing the reaction mixture with at least one first portion of a particulate additive before the reaction mixture has reached a residence time of 40% of the overall residence time in the reactor and with at least one second portion of a particulate additive when the reaction mixture has reached a residence time of 45% or more of the overall residence time in the reactor, the additive being selected from water-absorbing resin powders, fillers and mixtures thereof, the total solids content of monomer and additive being in the range from 30% to 60% by weight, the amount of additive being in the range from 5% to 50% by weight, based on the monomers, and the weight ratio of the first portion to the second portion of the additive being in the range from 10:1 to 1:5. The resin powder is recycled fine-sized material for example. Not only the residual monomer content, specifically the residual crosslinker content, but also the level of extractables in the water-absorbing resin are reduced by the method of addition described. A high fraction of additives can be incorporated without the properties of the water-absorbing resin obtained being adversely affected. The additives enter a sufficiently firm bond with the resin, so that no excessive dusting occurs on exposure to mechanical stress.
摘要翻译：本发明涉及通过聚合包含至少一种亲水单体和如果合适的反应器中至少一种交联剂的反应混合物来生产吸水树脂的方法，其包括将反应混合物与至少一个第一部分的反应混合物在反应混合物的停留时间达到总反应器停留时间的40％的停留时间和至少一个第二部分的颗粒状添加剂之前，当反应混合物达到45％或更多的停留时间时，在反应器中的总停留时间，添加剂选自吸水树脂粉末，填料及其混合物，单体和添加剂的总固体含量在30重量％至60重量％的范围内，添加剂的量为基于单体的5重量％至50重量％的范围，并且添加剂的第一部分与第二部分的重量比在10:1至 1：5。树脂粉末是例如再循环的精细尺寸的材料。通过所述的添加方法，不仅残留单体含量，特别是残留交联剂含量，而且吸水性树脂中的可萃取物的含量都降低。可以并入高分数的添加剂，而不会对获得的吸水性树脂的性能产生不良影响。添加剂与树脂进行足够牢固的粘合，使得在暴露于机械应力时不会发生过度的除尘。

4. 发明授权

US07786211B2 Production of a water-absorbing resin to which a particulate additive is admixed 有权
标题翻译：生产混合有微粒添加剂的吸水性树脂
公开(公告)号：US07786211B2
公开(公告)日：2010-08-31
申请号：US12158502
申请日：2006-12-28
申请人： Uwe Stueven , Rüdiger Funk , Matthias Weismantel , Thomas Daniel , Annemarie Hillebrecht , Dominicus van Esbroeck , Karl J. Possemiers
发明人： Uwe Stueven , Rüdiger Funk , Matthias Weismantel , Thomas Daniel , Annemarie Hillebrecht , Dominicus van Esbroeck , Karl J. Possemiers
IPC分类号： C08G18/63
CPC分类号： C08F2/44 , C08F220/06 , C08F222/1006
摘要： The invention relates to a process for producing a water-absorbing resin by polymerization of a reaction mixture comprising at least one hydrophilic monomer and, if appropriate, at least one crosslinker in a reactor, which comprises admixing the reaction mixture with at least one first portion of a particulate additive before the reaction mixture has reached a residence time of 40% of the overall residence time in the reactor and with at least one second portion of a particulate additive when the reaction mixture has reached a residence time of 45% or more of the overall residence time in the reactor, the additive being selected from water-absorbing resin powders, fillers and mixtures thereof, the total solids content of monomer and additive being in the range from 30% to 60% by weight, the amount of additive being in the range from 5% to 50% by weight, based on the monomers, and the weight ratio of the first portion to the second portion of the additive being in the range from 10:1 to 1:5. The resin powder is recycled fine-sized material for example. Not only the residual monomer content, specifically the residual crosslinker content, but also the level of extractables in the water-absorbing resin are reduced by the method of addition described. A high fraction of additives can be incorporated without the properties of the water-absorbing resin obtained being adversely affected. The additives enter a sufficiently firm bond with the resin, so that no excessive dusting occurs on exposure to mechanical stress.
摘要翻译：本发明涉及通过聚合包含至少一种亲水单体和如果合适的反应器中至少一种交联剂的反应混合物来生产吸水树脂的方法，其包括将反应混合物与至少一个第一部分的反应混合物在反应混合物的停留时间达到总反应器停留时间的40％的停留时间和至少一个第二部分的颗粒状添加剂之前，当反应混合物达到45％或更多的停留时间时，在反应器中的总停留时间，添加剂选自吸水树脂粉末，填料及其混合物，单体和添加剂的总固体含量在30重量％至60重量％的范围内，添加剂的量为基于单体的5重量％至50重量％的范围，并且添加剂的第一部分与第二部分的重量比在10:1至 1：5。树脂粉末是例如再循环的精细尺寸的材料。通过所述的添加方法，不仅残留单体含量，特别是残留交联剂含量，而且吸水性树脂中的可萃取物的含量都降低。可以并入高分数的添加剂，而不会对获得的吸水性树脂的性能产生不良影响。添加剂与树脂进行足够牢固的粘合，使得在暴露于机械应力时不会发生过度的除尘。

5. 发明申请

US20080202987A1 Method for Grading a Particulate Water-Absorbing Resin 有权
标题翻译：颗粒状吸水树脂分级方法
公开(公告)号：US20080202987A1
公开(公告)日：2008-08-28
申请号：US11813306
申请日：2005-12-31
申请人： Matthias Weismantel , Rudiger Funk , Thomas Daniel , Uwe Stueven
发明人： Matthias Weismantel , Rudiger Funk , Thomas Daniel , Uwe Stueven
IPC分类号： B07B9/02 , B07B1/46 , B07B1/40
CPC分类号： B07B1/56 , B07B1/40 , B07B1/46
摘要： Process for classifying a particulate water-absorbing resin using a sieving apparatus at a reduced pressure compared with the ambient pressure and a sieving apparatus for classifying a particulate water-absorbing resin at a reduced pressure compared with the ambient pressure.
摘要翻译：使用与环境压力相比减压的筛分装置对颗粒状吸水性树脂进行分级的方法以及与环境压力相比在减压下分级粒状吸水性树脂的筛分装置。

6. 发明申请

US20080306209A1 Production of a Water-Absorbing Resin to Which a Particulate Additive is Admixed 有权
标题翻译：混合颗粒添加剂的吸水树脂的生产
公开(公告)号：US20080306209A1
公开(公告)日：2008-12-11
申请号：US12158502
申请日：2006-12-28
申请人： Uwe Stueven , Rudiger Funk , Matthias Weismantel , Thomas Daniel , Annemarie Hillebrecht , Dominicus van Esbroeck , Karl J. Possemiers
发明人： Uwe Stueven , Rudiger Funk , Matthias Weismantel , Thomas Daniel , Annemarie Hillebrecht , Dominicus van Esbroeck , Karl J. Possemiers
IPC分类号： C08F2/44 , C08K3/32 , C08K5/04 , C08K3/34
CPC分类号： C08F2/44 , C08F220/06 , C08F222/1006
摘要： The invention relates to a process for producing a water-absorbing resin by polymerization of a reaction mixture comprising at least one hydrophilic monomer and, if appropriate, at least one crosslinker in a reactor, which comprises admixing the reaction mixture with at least one first portion of a particulate additive before the reaction mixture has reached a residence time of 40% of the overall residence time in the reactor and with at least one second portion of a particulate additive when the reaction mixture has reached a residence time of 45% or more of the overall residence time in the reactor, the additive being selected from water-absorbing resin powders, fillers and mixtures thereof, the total solids content of monomer and additive being in the range from 30% to 60% by weight, the amount of additive being in the range from 5% to 50% by weight, based on the monomers, and the weight ratio of the first portion to the second portion of the additive being in the range from 10:1 to 1:5. The resin powder is recycled fine-sized material for example. Not only the residual monomer content, specifically the residual crosslinker content, but also the level of extractables in the water-absorbing resin are reduced by the method of addition described. A high fraction of additives can be incorporated without the properties of the water-absorbing resin obtained being adversely affected. The additives enter a sufficiently firm bond with the resin, so that no excessive dusting occurs on exposure to mechanical stress.
摘要翻译：本发明涉及通过聚合包含至少一种亲水单体和如果合适的反应器中至少一种交联剂的反应混合物来生产吸水树脂的方法，其包括将反应混合物与至少一个第一部分的反应混合物在反应混合物的停留时间达到总反应器停留时间的40％的停留时间和至少一个第二部分的颗粒状添加剂之前，当反应混合物达到45％或更多的停留时间时，在反应器中的总停留时间，添加剂选自吸水树脂粉末，填料及其混合物，单体和添加剂的总固体含量在30重量％至60重量％的范围内，添加剂的量为基于单体的5重量％至50重量％的范围，并且添加剂的第一部分与第二部分的重量比在10:1至 1：5。树脂粉末是例如再循环的精细尺寸的材料。通过所述的添加方法，不仅残留单体含量，特别是残留交联剂含量，而且吸水性树脂中的可萃取物的含量都降低。可以并入高分数的添加剂，而不会对获得的吸水性树脂的性能产生不良影响。添加剂与树脂进行足够牢固的粘合，使得在暴露于机械应力时不会发生过度的除尘。

7. 发明授权

US06503979B1 Method for cross-linking hydrogels with bis- and poly-2-oxazolidinones 失效
标题翻译：用双 - 和多 - 2-恶唑烷酮交联水凝胶的方法
公开(公告)号：US06503979B1
公开(公告)日：2003-01-07
申请号：US09622853
申请日：2000-08-28
申请人： Rüdiger Funk , Volker Frenz , Ulrich Riegel , Matthias Weismantel , Fritz Engelhardt , Thomas Daniel
发明人： Rüdiger Funk , Volker Frenz , Ulrich Riegel , Matthias Weismantel , Fritz Engelhardt , Thomas Daniel
IPC分类号： C08F830
CPC分类号： C08J3/245 , A61L15/60 , C08F8/30 , C08G73/06 , C08J2300/14 , Y10S524/916
摘要： The invention contains a process for the surface postcrosslinking of water-absorbing polymers in which the polymers are treated with a surface postcrosslinking solution and during or after the treatment are postcrosslinked by means of an increase in temperature and are dried, wherein the crossiinker comprises a bis-2-oxazolidinone or a poly-2-oxazolidinone comprising structural units of the formula in which R1 is branched or unbranched C1-C18-alkylene, branched or unbranched C2-C18-alkenylene, C5-C18-cycloalkylene, phenylene, naphthylene, anthracenylene, hydrocarbon-substituted phenylene, naphthylene or anthracenylene or another substituted or unsubstituted C6-C18-arylene radical, R2 is branched or unbranched C1-C18-alkylene and n is an integer from 1 to 50 or a mixture of bis-2-oxazolidinones and poly-2-oxazolidinones dissolved in an inert solvent.
摘要翻译：本发明包含用于表面后吸附聚合物的方法，其中聚合物用表面后交联溶液处理，并且在处理期间或之后通过温度升高进行后交联并干燥，其中交联剂包含双 -2-恶唑烷酮或包含结构单元的聚-2-恶唑烷酮，其中R1是支链或非支链C1-C18-亚烷基，支链或非支链C2-C18-亚烯基，C5-C18-亚环烷基，亚苯基，亚萘基，蒽亚基，烃取代的亚苯基，亚萘基或亚蒽基或其它取代或未取代的C 6 -C 18亚芳基，R 2是支链或非支链的C 1 -C 18 - 亚烷基，n是1至50的整数或双-2-恶唑烷酮和聚 -2-恶唑烷酮溶解在惰性溶剂中。

8. 发明授权

US07199211B2 (Meth)acrylic esters of polyalkoxylated trimethylolpropane 失效
标题翻译：（甲基）丙烯酸酯，聚烷氧基化三羟甲基丙烷
公开(公告)号：US07199211B2
公开(公告)日：2007-04-03
申请号：US10517042
申请日：2003-06-06
申请人： Andreas Popp , Thomas Daniel , Jürgen Schröder , Thomas Jaworek , Rüdiger Funk , Reinhold Schwalm , Matthias Weismantel , Ulrich Riegel
发明人： Andreas Popp , Thomas Daniel , Jürgen Schröder , Thomas Jaworek , Rüdiger Funk , Reinhold Schwalm , Matthias Weismantel , Ulrich Riegel
IPC分类号： C08G63/78 , C08G63/82
CPC分类号： C08G65/3322 , A61L15/60 , C07C67/08 , C08G65/2609 , Y10T428/249921 , C07C69/54
摘要： The present invention relates to novel (meth)acrylic esters of polyalkoxylated trimethylolpropane of the formula where AO is for each AO independently at each instance EO, PO or BO where EO is O—CH2-CH2- PO is independently at each instance O—CH2-CH(CH3)- or O—CH(CH3)-CH2- BO is independently at each instance O—CH2-CH(CH2-CH3)- or O—CH(CH2-CH3)-CH2- p1+p2+p3 is 28, 29, 30, 31, 32, 33, 34, 35, 36, 37, 38, 39, 40, 41, 42, 43, 44, 45, 46, 47, 48, 49, 50, 51, 52, 53, 54, 55, 56, 57, 58, 59, 60, 61, 62, 63, 64, 65, 66, 67, 68, 69, 70, 71, 72, 73, 74 or 75, R1, R2 and R3 are independently H or CH3, a simplified process for preparing these esters and the use of reaction mixtures thus obtainable.
摘要翻译：本发明涉及下式的聚烷氧基化三羟甲基丙烷的新型（甲基）丙烯酸酯

9. 发明授权

US07259212B2 (Meth)acrylic esters of polyalkoxylated trimethylolpropane 失效
标题翻译：（甲基）丙烯酸酯，聚烷氧基化三羟甲基丙烷
公开(公告)号：US07259212B2
公开(公告)日：2007-08-21
申请号：US10516698
申请日：2003-06-10
申请人： Andreas Popp , Thomas Daniel , Jürgen Schröder , Thomas Jaworek , Rüdiger Funk , Reinhold Schwalm , Matthias Weismantel , Ulrich Riegel
发明人： Andreas Popp , Thomas Daniel , Jürgen Schröder , Thomas Jaworek , Rüdiger Funk , Reinhold Schwalm , Matthias Weismantel , Ulrich Riegel
IPC分类号： C08F2/02 , C08F2/62 , C08F1/02 , C08F1/62
CPC分类号： C08G65/3322 , A61L15/60 , C07C67/08 , C08G65/2609 , C07C69/54
摘要： The present invention relates to novel (meth)acrylic esters of polyalkoxylated trimethylolpropane of the formula where EO is O—CH2-CH2- PO is independently at each instance O—CH2-CH(CH3)- or O—CH(CH3)-CH2- n1, n2 and n3 are independently 4, 5 or 6, n1+n2+n3 is 14, 15 or 16, m1, m2 and m3 are independently 1, 2 or 3, m1+m2+m3 is 4, 5 or 6, R1, R2 and R3 are independently H or CH3, a simplified process for preparing these esters and the use of reaction mixtures thus obtainable.
摘要翻译：本发明涉及下式的聚烷氧基化三羟甲基丙烷的新型（甲基）丙烯酸酯：其中EO为O-CH 2 -CH 2 - ，PO各自独立地为O-CH 2 -CH（CH 3） - 或O-CH（CH 3）-CH 2 - n1，n2和n3分别为4,5或6，n1 + n2 + n3为14,15或16，m1，m2和m3分别为1,2或3，m1 + m2 + m3为4,5或6 ，R 1，R 2和R 3独立地为H或CH 3，制备这些酯的简化方法以及由此得到的反应混合物的用途。

10. 发明授权

US06472478B1 Process for crosslinking hydrogels with bis- and poly-2- oxazolidinones 有权
标题翻译：用双 - 和多 - 2-恶唑烷酮交联水凝胶的方法
公开(公告)号：US06472478B1
公开(公告)日：2002-10-29
申请号：US09601349
申请日：2000-08-18
申请人： Rüdiger Funk , Volker Frenz , Ulrich Riegel , Matthias Weismantel , Fritz Engelhardt , Thomas Daniel
发明人： Rüdiger Funk , Volker Frenz , Ulrich Riegel , Matthias Weismantel , Fritz Engelhardt , Thomas Daniel
IPC分类号： C08F830
CPC分类号： A61L15/60 , C08F8/30 , Y10S524/916 , Y10T442/699
摘要： The invention relates to a process for the gel or surface postcrosslinking of water-absorbing polymers in which the polymers are treated with a surface postcrosslinking solution and during or after the treatment are postcrosslinked and dried by means of an increase in temperature, the crosslinker being a compound of the formula in which R1 and R2 independently of one another are H, hydroxyl, phenyl or C1-C6-alkyl, R3 is hydrogen, C1-C12-alkyl, C1-C12-alkenyl or C6-C12-aryl and R4 and R5 independently of one another are C1-C12-alkyl, C1-C12-alkenyl, C6-C12-aryl, hydroxyl, C1-C12-alkoxy or hydrogen, dissolved in an inert solvent, to water-absorbing polymers which can be obtained by said process, and to their use in hygiene articles, packaging materials and nonwovens.
摘要翻译：本发明涉及一种吸水聚合物的凝胶或表面后交联方法，其中聚合物用表面后交联溶液处理，并且在处理之间或之后，通过温度升高进行后交联和干燥，交联剂为 R 1和R 2彼此独立地是H，羟基，苯基或C 1 -C 6烷基的化合物，R 3是氢，C 1 -C 12 - 烷基，C 1 -C 12 - 烯基或C 6 -C 12 - 芳基，R 4和R 5 彼此独立地是溶解在惰性溶剂中的C 1 -C 12烷基，C 1 -C 12 - 烯基，C 6 -C 12 - 芳基，羟基，C 1 -C 12 - 烷氧基或氢，可以通过所述过程，以及它们在卫生用品，包装材料和无纺布中的应用。

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