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1. 发明授权

US5091072A Process for preparing pitches 失效
标题翻译：制备勺子的方法
公开(公告)号：US5091072A
公开(公告)日：1992-02-25
申请号：US504723
申请日：1990-04-03
申请人： Masatoshi Tsuchitani , Makoto Tamura , Kiyotaka Suzuki , Sjuji Okada , Ryoichi Nakajima , Sakae Naito
发明人： Masatoshi Tsuchitani , Makoto Tamura , Kiyotaka Suzuki , Sjuji Okada , Ryoichi Nakajima , Sakae Naito
IPC分类号： C10C1/00 , C10C3/00
CPC分类号： C10C1/00 , C10C3/00
摘要： Commercially attractive continuous processes for the preparation of mesophase pitches for manufacturing high-performance carbon fibers are disclosed. One feature resides in that conversion of a pitch into a mesophase pitch is conducted continuously by using a unique continuous dispersion-heat-treating apparatus. The other feature resides in that the raw material for hydrogenation treatment which is a pretreatment preceeding to the final heat treatment for the production of a mesophase pitch, is prepared by using a heavy oil or pitch having substantially no BTX-insoluble material as the starting raw material, subjecting the raw material to a simple four-step treatment of (1) a continuous heat treatment in a tubular heater, (2) a distillation operation, (3) a BTX-solvent extraction and (4) a distillation operation; while recycling a soluble component obtained in the step (4) to the heat treatment of step (1) and recovering a BTX-solvent insoluble component formed in step (3) as the material for the hydrogenation treatment. This feature can provide a significant increase in the yield of a mesophase pitch. Furthermore, unexpectedly, the recycle of the soluble component into the heat treatment of step (1) is helpful to improve the characteristics of the ultimate products, i.e., carbon fibers or graphite fibers. Combination of the first and the second features, of course, can provide a better commercial success. In fact, the process of the present invention can provide a carbon fiber having a tensile strength of more than 300 kg/mm.sup.2 and a graphite fiber having a tensile strength of more than 400 kg/mm.sup.2 and a modulus of elasticity of no more than 60 ton/mm.sup.2. Processes with minor modifications to the above are also disclosed.

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