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1. 发明授权

US5182011A Process for preparing pitches 失效
标题翻译：制作球场的过程
公开(公告)号：US5182011A
公开(公告)日：1993-01-26
申请号：US616836
申请日：1990-11-21
申请人： Masatoshi Tsuchitani , Makoto Tamura , Kiyotaka Suzuki , Shuji Okada , Ryoichi Nakajima , Sakae Naito
发明人： Masatoshi Tsuchitani , Makoto Tamura , Kiyotaka Suzuki , Shuji Okada , Ryoichi Nakajima , Sakae Naito
IPC分类号： C10C1/00 , C10C3/00
CPC分类号： C10C3/00 , C10C1/00
摘要： Commercially attractive continuous processes for the preparation of mesophase pitches for manufacturing high-performance carbon fibers are disclosed. One feature resides in that conversion of a pitch into a mesophase pitch is conducted continuously by using a unique continuous dispersion-heat-treating apparatus. The other feature resides in that the raw material for hydrogenation treatment which is a pretreatment preceeding to the final heat treatment for the production of a mesophase pitch, is prepared by using a heavy oil or pitch having substantially no BTX-insoluble material as the starting raw material, subjecting the raw material to a simple four-step treatment of (1) a continuous heat treatment in a tubular heater, (2) a distillation operation, (3) a BTX-solvent extraction and (4) a distillation operation; while recycling a soluble component obtained in the step (4) to the heat treatment of step (1) and recovering a BTX-solvent insoluble component formed in step (3) as the material for the hydrogenation treatment. This feature can provide a significant increase in the yield of a mesophase pitch. Furthermore, unexpectedly, the recycle of the soluble component into the heat treatment of step (1) is helpful to improve the characteristics of the ultimate products, i.e., carbon fibers or graphite fibers. Combination of the first and the second features, of course, can provide a better commercial success. In fact, the process of the present invention can provide a carbon fiber having a tensile strength of more than 300 kg/mm.sup.2 and a graphite fiber having a tensile strength of more than 400 kg/mm.sup.2 and a modulus of elasticity of more than 60 ton/mm.sup.2. Processes with minor modifications to the above are also disclosed.
摘要翻译：公开了用于制备用于制造高性能碳纤维的中间相沥青的商业上有吸引力的连续方法。一个特征在于，通过使用独特的连续分散热处理装置连续地进行沥青转化为中间相沥青。另一个特征在于，通过使用基本上不含BTX不溶性材料的重油或沥青作为起始原料，制备作为用于生产中间相沥青的最终热处理之前的预处理的氢化处理原料材料，对原料进行简单的四步处理（1）在管式加热器中的连续热处理，（2）蒸馏操作，（3）BTX-溶剂萃取和（4）蒸馏操作; 同时将步骤（4）中获得的可溶组分再循环到步骤（1）的热处理中，并回收步骤（3）中形成的BTX-溶剂不溶组分作为氢化处理材料。该特征可以显着提高中间相沥青的产率。此外，意想不到的是，将可溶组分再循环到步骤（1）的热处理中有助于改善最终产物即碳纤维或石墨纤维的特性。结合第一和第二功能，当然可以提供更好的商业成功。事实上，本发明的方法可以提供拉伸强度大于300kg / mm 2的碳纤维和拉伸强度大于400kg / mm 2的石墨纤维和大于60吨的弹性模量 / mm2。还公开了对上述的微小修改的处理。

2. 发明授权

US07396560B2 Method for preparing organic-inorganic composite microcrystal 失效
标题翻译：有机 - 无机复合微晶制备方法
公开(公告)号：US07396560B2
公开(公告)日：2008-07-08
申请号：US10487093
申请日：2002-03-18
申请人： Hachiro Nakanishi , Hidetoshi Oikawa , Shuji Okada , Hitoshi Kasai
发明人： Hachiro Nakanishi , Hidetoshi Oikawa , Shuji Okada , Hitoshi Kasai
IPC分类号： B05D7/00 , C08F2/46 , C08J7/18
CPC分类号： C30B7/00
摘要： A method for preparation of inorganic fine particle-organic crystal hybrid fine particle comprising; pouring an organic material having π-conjugated bond as a water soluble solution into aqueous dispersion in which inorganic fine particles of 50 nm or less selected from the compound group consisting of metal fine particles, semi-conductor fine particles, fine particles of inorganic fluorescent material and fine particle of inorganic luminescent material, are dispersed, co-precipitating said inorganic fine particle which forms a core into said organic material which forms a shell in said dispersion and forming shell of fine crystal of said organic material on the surface of the core of said inorganic fine particles of 50 nm or less by controlling the size of said inorganic fine particle and by controlling the adding amount of said organic material.
摘要翻译：一种制备无机细颗粒 - 有机晶体杂化微粒的方法，包括：将具有π-共轭键的有机材料作为水溶性溶液浇注到水分散体中，其中选自由金属微粒，半导体细颗粒，无机荧光材料的微粒组成的化合物组中的50nm或更小的无机细颗粒和无机发光材料的微粒分散，将形成芯的无机细颗粒共沉淀到所述分散体中形成壳的所述有机材料中，并在所述芯的表面上形成所述有机材料的细晶的壳通过控制所述无机细颗粒的尺寸并控制所述有机材料的添加量，所述无机细颗粒为50nm以下。

3. 发明授权

US07186289B2 Nickel powder and production method therefor 失效
标题翻译：镍粉及其制备方法
公开(公告)号：US07186289B2
公开(公告)日：2007-03-06
申请号：US10970849
申请日：2004-10-19
申请人： Toshihiro Kato , Shuji Okada , Shoji Futaki
发明人： Toshihiro Kato , Shuji Okada , Shoji Futaki
IPC分类号： B22F1/00 , C22B5/00 , H01B1/22
CPC分类号： C22C1/0433 , B22F1/0096 , B22F9/24 , H01B1/22
摘要： There is provided a nickel powder suitable as conductive particles for use in conductive paste and conductive resin, that is inexpensive, has superior weather resistance, low resistivity when kneaded with resin, and is stable when used in the long-term, and a production method therefor.A nickel powder is produced by a two stage reduction and precipitation process from an aqueous solution containing a bivalent nickel salt, wherein an average primary particle diameter is 0.2 μm to 2.0 μm as measured with a scanning electron microscope (SEM), wherein an average secondary particle diameter is 8 μm to 50 μm according to laser particle size distribution measurement, wherein a tap density is 0.5 g/ml to 2.0 g/ml, wherein a cobalt content is 1 to 20 weight %. The cobalt may be contained in only the surface layer of the nickel powder at a content of 1 weight % to 40 weight %.
摘要翻译：提供了适合作为导电性糊料和导电性树脂使用的导电性粒子的镍粉末，价格便宜，具有优异的耐候性，与树脂捏合时的低电阻率，长期使用时稳定，制造方法因此。通过二级还原沉淀法从含有二价镍盐的水溶液中制备镍粉，其中平均一次粒径为0.2μm至2.0μm，用扫描电子显微镜（SEM）测量，其中平均次级根据激光粒度分布测定，粒径为8μm〜50μm，振实密度为0.5g / ml〜2.0g / ml，钴含量为1〜20重量％。钴可以仅含有1重量％至40重量％的含量的镍粉表面层。

4. 发明申请

US20060039984A1 Process for producing fine porous polyimide particle 审中-公开
标题翻译：微孔聚酰亚胺微粒的制造方法
公开(公告)号：US20060039984A1
公开(公告)日：2006-02-23
申请号：US10537497
申请日：2003-07-09
申请人： Hachiro Nakanishi , Hitoshi Kasai , Hirohiko Miura , Hidetoshi Oikawa , Shuji Okada
发明人： Hachiro Nakanishi , Hitoshi Kasai , Hirohiko Miura , Hidetoshi Oikawa , Shuji Okada
IPC分类号： A61K9/14 , B29B9/00
CPC分类号： C08J9/28 , C08J2201/0543 , C08J2201/0546 , C08J2379/08 , C08L79/08
摘要： A method for preparation of porous polyimide microparticles comprising, forming polyamide acid microparticles by pouring polymer solution prepared by dissolving polyamide acid containing 0.5 to 80 weight % of alkali metal salt to polyamide acid by 0.1 to 15 weight % concentration into a poor solvent selected from the group consisting of aliphatic solvents, alicyclic solvents, aromatic solvents, CS2 and mixture of two or more these solvents and the temperature of which is adjusted to the range from −20° C. to 60° C., wherein particle size of said polyamide acid microparticles is adjusted to 50 nm to 10000 nm by controlling the temperature of said poor solvent, pore size of said polyamide acid microparticles is adjusted to the range from 20 nm to 500 nm and porosity of said polyamide acid microparticles is adjusted to the range from 0.1% to 30% by controlling a content or a kind of said alkali metal salt, then treating said polyamide acid microparticles by chemical imidation or thermal imidation, or by thermal imidation after chemical imidation so that the particle size distribution, pore size and porosity of said polyamide acid microparticles can be maintained.
摘要翻译：一种多孔聚酰亚胺微粒的制备方法，其特征在于，包括：将聚合物溶液倒入聚酰胺酸性微粒中形成聚酰胺酸微粒，所述聚合物溶液是将含有0.5〜80重量％的碱金属盐的聚酰胺酸溶解在0.1〜15重量％浓度的聚酰胺酸中，由脂族溶剂，脂环族溶剂，芳族溶剂，CS 2和两种或更多种这些溶剂的混合物组成的组，其温度调节至-20℃至60℃。通过控制所述不良溶剂的温度将所述聚酰胺酸微粒的粒径调整为50nm〜10000nm，将所述聚酰胺酸微粒的孔径调整为20nm〜500nm，将所述聚酰胺酸的孔隙率通过控制所述碱金属盐的含量或种类将微粒调节至0.1％至30％的范围，然后通过化学酰亚胺化处理所述聚酰胺酸微粒或热酰亚胺化，或通过化学酰亚胺化后的热酰亚胺化，使得可以维持所述聚酰胺酸微粒的粒度分布，孔径和孔隙率。

5. 发明授权

US6013748A Aromatic ester compound and second-order non-linear optical material therewith 失效
标题翻译：芳香族酯化合物和二级非线性光学材料
公开(公告)号：US6013748A
公开(公告)日：2000-01-11
申请号：US46658
申请日：1998-03-24
申请人： Hiroo Matsuda , Takashi Fukuda , Shinji Yamada , Tatsumi Kimura , Masao Kato , Xuan-Ming Duan , Shuji Okada , Hachiro Nakanishi
发明人： Hiroo Matsuda , Takashi Fukuda , Shinji Yamada , Tatsumi Kimura , Masao Kato , Xuan-Ming Duan , Shuji Okada , Hachiro Nakanishi
IPC分类号： C07C69/92 , C07C205/43 , C07C255/55 , C08F2/00 , G02F1/361
CPC分类号： C07C255/55 , C07C205/43 , C07C69/92 , G02F1/3615
摘要： Disclosed is a novel aromatic ester compound represented by the general formula ##STR1## in which Pn is a 1,4-phenylene group, R.sup.1 is an alkyl group having 1 to 4 carbon atoms, R.sup.2 is a group selected from the group consisting of perfluoroalkyl groups having 1 to 4 carbon atoms, cyano group, nitro group, 2,2-dicyanoethenyl group and methylsulfonyl group and the subscript n is a number of 2, 3 or 4. These aromatic ester compounds are useful as a second-order non-linear optical material in the ultraviolet wavelength range so that a resin film containing the compound has a good second-order non-linear optical coefficient d.sub.33 of 2-4.times.10.sup.-9 esu.
摘要翻译：公开了一种由通式表示的新型芳族酯化合物，其中Pn是1,4-亚苯基，R1是具有1-4个碳原子的烷基，R2是选自具有1个碳原子的全氟烷基至4个碳原子，氰基，硝基，2,2-二氰基乙烯基和甲基磺酰基，下标n为2,3或4.这些芳族酯化合物可用作二级非线性光学材料在紫外线波长范围内，含有该化合物的树脂膜的二次非线性光学系数d33为2-4×10-9 esu。

6. 发明授权

US5057248A Method for production of polymeric nonlinear optical material 失效
标题翻译：聚合非线性光学材料的生产方法
公开(公告)号：US5057248A
公开(公告)日：1991-10-15
申请号：US313448
申请日：1989-02-22
申请人： Hiroo Matsuda , Shuji Okada , Hachiro Nakanishi , Masao Kato
发明人： Hiroo Matsuda , Shuji Okada , Hachiro Nakanishi , Masao Kato
IPC分类号： G02F1/35 , C08F8/00 , G02F1/355 , G02F1/361
CPC分类号： G02F1/3615
摘要： A polymeric nonlinear optical material is produced by mixing a polyelectrolyte solution with an ionic pigment solution thereby obtaining a solution containing a composite of said polyelectrolyte and said ionic pigment, and separating said composite from said solution.
摘要翻译：聚合物非线性光学材料通过将聚电解质溶液与离子颜料溶液混合从而得到含有所述聚电解质和所述离子颜料的复合物并将所述复合材料与所述溶液分离的溶液来制备。

7. 发明授权

US5003569A Method using x-rays to determine thickness of organic films 失效
标题翻译：使用X射线来确定有机膜的厚度的方法
公开(公告)号：US5003569A
公开(公告)日：1991-03-26
申请号：US493322
申请日：1990-03-14
申请人： Shuji Okada , Hiro Matsuda , Hachiro Nakanishi , Masao Kato
发明人： Shuji Okada , Hiro Matsuda , Hachiro Nakanishi , Masao Kato
IPC分类号： G01B15/02
CPC分类号： G01B15/02
摘要： A thickness determination method for organic films comprises the steps of: irradiating an organic film to be measured with x-rays at a certain angle of incidence, finding an angle of reflection at which the x-ray intensity reaches a peak, and finding the thickness of the film from the angle of this peak.
摘要翻译：有机膜的厚度测定方法包括以下步骤：用X射线以一定的入射角度照射被测量的有机膜，求出X射线强度达到峰值的反射角度，求出厚度的电影从这个峰的角度。

8. 发明申请

US20110061777A1 FERRITIC STAINLESS STEEL SHEET HAVING SUPERIOR PUNCHING WORKABILITY AND METHOD FOR MANUFACTURING THE SAME 审中-公开
标题翻译：具有超级冲压加工性能的不锈钢不锈钢板及其制造方法
公开(公告)号：US20110061777A1
公开(公告)日：2011-03-17
申请号：US12673651
申请日：2008-06-18
申请人： Tomohiro Ishii , Yoshimasa Funakawa , Shuji Okada , Masayuki Ohta
发明人： Tomohiro Ishii , Yoshimasa Funakawa , Shuji Okada , Masayuki Ohta
IPC分类号： C21D8/02 , C22C38/18
CPC分类号： C22C38/02 , B21B3/02 , C21D1/32 , C21D1/673 , C21D6/002 , C21D8/0436 , C21D8/0473 , C21D2211/004 , C21D2211/005 , C22C38/04 , C22C38/42 , C22C38/48 , C22C38/50
摘要： A ferritic stainless steel sheet and a method for manufacturing the ferritic stainless steel sheet include a composition which contains 0.0030 to 0.012 mass percent of C, 0.13 mass percent or less of Si, 0.25 mass percent or less of Mn, 0.04 mass percent or less of P, 0.005 mass percent or less of S, 0.06 mass percent or less of Al, 0.0030 to 0.012 mass percent of N, 20.5 to 23.5 mass percent of Cr, 0.3 to 0.6 mass percent of Cu, 0.5 mass percent or less of Ni, 0.3 to 0.5 mass percent of Nb, 0.05 to 0.15 mass percent of Ti, and the balance being Fe and inevitable impurities is hot-rolled at a finishing temperature of 900° C. or more and at a coiling temperature of 400 to 550° C., softening annealing is performed on an obtained hot-rolled steel sheet, picking is further performed, and cold rolling is subsequently performed.
摘要翻译：铁素体系不锈钢板和铁素体系不锈钢板的制造方法中，含有C：0.0030〜0.012质量％，Si：0.13质量％以下，Mn：0.25质量％以下，0.04质量％以下 P：0.005质量％以下，Al：0.06质量％以下，N：0.0030〜0.012质量％，Cr：20.5〜23.5质量％，Cu：0.3〜0.6质量％，Ni：0.5质量％ Nb：0.3〜0.5质量％，Ti：0.05〜0.15质量％，余量为Fe和不可避免的杂质，在终轧温度为900℃以上，卷取温度为400〜550℃下进行热轧对获得的热轧钢板进行软化退火，进一步进行进行，随后进行冷轧。

9. 发明申请

US20060076298A1 Novel process for producing pigment nanoparticle 失效
标题翻译：制备颜料纳米颗粒的新方法
公开(公告)号：US20060076298A1
公开(公告)日：2006-04-13
申请号：US10525228
申请日：2003-04-02
申请人： Hachiro Nakanishi , Koichi Baba , Hitoshi Kasai , Hidetoshi Oikawa , Shuji Okada
发明人： Hachiro Nakanishi , Koichi Baba , Hitoshi Kasai , Hidetoshi Oikawa , Shuji Okada
IPC分类号： B01D1/00 , C02F1/52
CPC分类号： B01D9/0054 , B01J3/008 , C09B67/0014 , C09B67/0096 , C09B67/0097 , Y02P20/544
摘要： The process for producing highly concentrated nanometer-size fine particles of an organic pigment, which comprises dissolving the organic pigment in an amide solvent, especially an organic solvent comprising at least 50 vol % 1-methyl-2-pyrrodinone, and pouring the resultant organic pigment solution with stirring into a poor solvent which is not compatible with the organic pigment. The pigment may be a quinacridone pigment, phthalocyanine pigment etc. Any atmospheric pressure to a sub-critical and/or supercritical state can be employed as the production conditions.
摘要翻译：用于生产有机颜料的高度浓缩的纳米尺寸微粒的方法，其包括将有机颜料溶解在酰胺溶剂中，特别是包含至少50体积％1-甲基-2-吡咯烷酮的有机溶剂中，并将所得有机颜料颜料溶液搅拌成与有机颜料不相容的不良溶剂。颜料可以是喹吖啶酮颜料，酞菁颜料等。作为生产条件，可以使用亚临界和/或超临界状态的任何大气压。

10. 发明授权

US5281250A Powder material for rare earth-iron-boron based permanent magnets 失效
标题翻译：稀土 - 铁硼永磁体用粉末材料
公开(公告)号：US5281250A
公开(公告)日：1994-01-25
申请号：US838092
申请日：1992-02-20
申请人： Atsushi Hamamura , Katsumi Okayama , Yuji Kaneko , Yasuhiro Okajima , Kaname Takeya , Shuji Okada
发明人： Atsushi Hamamura , Katsumi Okayama , Yuji Kaneko , Yasuhiro Okajima , Kaname Takeya , Shuji Okada
IPC分类号： B22F1/00 , C22C38/00 , H01F1/057 , H01F1/06
CPC分类号： H01F1/0573 , H01F1/0571
摘要： A powder for producing permanent magnets, comprising a blend of powders [A] and [B] or [C] wherein:alloy powder [A] has an R.sub.2 Fe.sub.14 B phase and contains, in atomic percent, from 11 to 13% of at least one rare element, R, inclusive of Y, from 4 to 12% of B, and the balance Fe; or optionally, said powder has an R.sub.2 (Fe,Co).sub.14 B phase, an R.sub.2 (Fe,Ni).sub.14 B phase or an R.sub.2 (Fe,Co,Ni).sub.14 B phase, containing at least one selected from the group consisting of 10% or less of Co and 3% or less of Ni as a partially substitute for Fe;powder [B] is an intermetallic compound having an intermetallic compound phase of R with Fe or Co inclusive of an R.sub.3 Co phase (provided that Co may be partially substituted for by Fe), containing, in atomic percent, from 13 to 45% of at least one rare element, R, inclusive of Y, and the balance Co (provided that Co may be partially substituted for by Fe),powder [C] is an intermetallic compound having an intermetallic compound phase of R with Fe or Co inclusive of an R.sub.3 Co phase (provided that Co may be partially substituted for by Fe) and an R.sub.2 Fe.sub.14 B phase, containing, in atomic percent, from 13 to 45% of at least one rare element, R, inclusive of Y, 12% or less of B and the Co (provided that Co may be partially substituted for by Fe).
摘要翻译：一种用于制造永磁体的粉末，其包含粉末（A）和（B）或（C）的混合物，其中：合金粉末（A）具有R2Fe14B相，原子百分比含有11至13％的至少一种稀有元素R，包括Y，B的4〜12％，余量为Fe; 或任选地，所述粉末具有R2（Fe，Co）14B相，R2（Fe，Ni）14B相或R2（Fe，Co，Ni）14B相，其含有选自10％以下的Co和3％以下的Ni作为Fe的部分替代物; 粉末（B）是具有与Fe或Co的金属间化合物相的金属间化合物，包括R3Co相（其中Co可以部分被Fe取代），原子百分比含有13〜45％的至少一种稀有元素R（包括Y）和余量Co（条件是Co可以部分被Fe取代），粉末（C）是金属间化合物的金属间化合物，其中R与Fe或Co包括 R3Co相（其中Co可以被Fe部分取代）和R2Fe14B相，其中原子百分比含有13至45％的至少一种稀有元素R，包括Y，12％或更少的B和 Co（Co可以部分地被Fe代替）。

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