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1. 发明授权

US5391661A Process for producing a styrenic polymer and a catalyst for use therein 失效
标题翻译：制备苯乙烯聚合物的方法及其中使用的催化剂
公开(公告)号：US5391661A
公开(公告)日：1995-02-21
申请号：US965290
申请日：1993-02-02
申请人： Shoji Naganuma , Masami Watanabe , Norio Tomotsu
发明人： Shoji Naganuma , Masami Watanabe , Norio Tomotsu
IPC分类号： C08F4/16 , C08F4/42 , C08F4/60 , C08F4/619 , C08F4/6192 , C08F4/642 , C08F4/659 , C08F4/6592 , C08F4/76 , C08F4/80 , C08F10/00 , C08F12/00 , C08F12/04 , C08F12/08 , C08F4/54
CPC分类号： C08F12/04 , C08F10/00 , C08F12/08 , C08F4/61908 , C08F4/6192
摘要： There are disclosed a catalyst well suited for producing a styrenic polymer having a high degree of syndiotactic configuration which comprises a transition-metal compound such as pentamethylcyclopentadienyltrimethyltitanium and a coordination complex compound comprising an anion in which a plurality of radicals are bonded to a metal and a quaternary ammonium salt, the compound being exemplified by orthocyano-N-methylpyridinium tetra(pentafluorophenyl)borate, or comprises an alkylating agent such as triisobutylaluminum in addition to the above two compounds; and a process for producing a styrenic polymer having a high degree of syndiotactic configuration by polymerizing a styrenic monomer using the aforementioned catalyst. Consequently, a styrenic polymer having a high degree of syndiotactic configuration can be produced effectively without the use of an expensive aluminoxane required in a large amount if used.
摘要翻译： PCT No.PCT / JP92 / 00736 Sec。 371日期：1993年2月2日 102（e）日期1993年2月2日PCT提交1992年6月9日PCT公布。公开号WO92 / 22589 公开了一种非常适合于生产具有高度间同立构构型的苯乙烯类聚合物的催化剂，其包含过渡金属化合物如五甲基环戊二烯基三甲基钛和包含阴离子的配位络合物，其中多个基团键合到金属和季铵盐，该化合物例如是四（五氟苯基）硼酸正氰基-N-甲基吡啶鎓，或除了上述两种化合物之外还包括烷基化剂如三异丁基铝; 以及通过使用上述催化剂聚合苯乙烯类单体来制备具有高程度间同立构构型的苯乙烯类聚合物的方法。因此，如果使用的话，可以有效地制造具有高程度间同立构构型的苯乙烯类聚合物，而不需要大量使用昂贵的铝氧烷。

2. 发明授权

US5294685A Process for producing a styrenic polymer having a high degree of syndiotacticity 失效
标题翻译：制备具有高度间同立构规整度的苯乙烯类聚合物的方法
公开(公告)号：US5294685A
公开(公告)日：1994-03-15
申请号：US79860
申请日：1993-06-22
申请人： Masami Watanabe , Shoji Naganuma , Norio Tomotsu
发明人： Masami Watanabe , Shoji Naganuma , Norio Tomotsu
IPC分类号： C08F4/643 , C08F4/60 , C08F4/646 , C08F4/649 , C08F4/659 , C08F4/6592 , C08F4/76 , C08F4/80 , C08F10/00 , C08F12/00 , C08F12/04 , C08F12/08
CPC分类号： C08F12/04 , C08F12/12 , C08F2420/04 , Y10S526/943
摘要： There are disclosed a catalyst which comprises a specific transition-metal compound (A) and a specific coordination complex compound (B) instead of aluminoxane, and a process for producing a styrene polymer at a reduced cost with improved efficiency by the use of the above catalyst.The catalyst according to the present invention is inexpensive compared with the conventional catalyst containing aluminoxane as the major ingredient, and exhibits a high activity in the polymerization of a styrenic monomer into styrene polymer with a high degree of syndiotacticity as well as a high yield and conversion rate.
摘要翻译：公开了代替铝氧烷包含特定的过渡金属化合物（A）和特定的配位络合物（B）的催化剂，以及通过使用上述方法以降低的成本生产苯乙烯聚合物的方法提高了效率催化剂。根据本发明的催化剂与含有铝氧烷作为主要成分的常规催化剂相比是廉价的，并且在苯乙烯单体聚合成具有高度间同立构规整度的苯乙烯聚合物中表现出高的活性以及高产率和转化率率。

3. 发明授权

US5600005A Process for producing tetrakisflorophenylborate 失效
标题翻译：制备四氟苯基硼酸盐的方法
公开(公告)号：US5600005A
公开(公告)日：1997-02-04
申请号：US465892
申请日：1995-06-06
申请人： Shoji Naganuma , Masami Watanabe , Norio Tomotsu
发明人： Shoji Naganuma , Masami Watanabe , Norio Tomotsu
IPC分类号： C07F5/02 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F12/08
CPC分类号： C08F10/00 , C07F5/027 , C08F12/08 , C08F110/06 , C08F4/65912 , C08F4/65927
摘要： A process for preparing a tetrakisfluorophenylborate which is useful as a catalyst component for the polymerization of olefins or as a raw material for synthesizing the same, efficiently at a high productivity per unit amount of a solvent and at a high yield. A mixed solvent of ether and an aliphatic hydrocarbon is used as a reaction solvent for preparing tetrakisphenylborate according to the following reaction formula,4M.sup.4 --C.sub.6 Y.sup.3.sub.5 +BCl.sub.3 .fwdarw.M.sup.4 B(C.sub.6 Y.sup.3.sub.5).sub.4wherein M.sup.4 is an alkali or alkaline earth metal, or represents R.sup.6.sub.2 Al, wherein R.sup.6 is an alkyl group, and Y.sup.3 is a hydrogen atom or a halogen atom.
摘要翻译：制备可用作烯烃聚合的催化剂组分或用于合成烯烃的原料的四氟氟苯硼酸盐的方法，以每单位溶剂的高生产率和高收率有效地制备。根据以下反应式使用醚和脂族烃的混合溶剂作为制备四苯基硼酸的反应溶剂，其中M4是碱金属或碱土金属，或代表R62Al，其中R6是烷基，Y3是氢原子或卤素原子。

4. 发明授权

US5461127A Polymerization catalysts and process for producing polymers 失效
标题翻译：聚合催化剂和聚合物的制备方法
公开(公告)号：US5461127A
公开(公告)日：1995-10-24
申请号：US124650
申请日：1993-09-22
申请人： Shoji Naganuma , Masami Watanabe
发明人： Shoji Naganuma , Masami Watanabe
IPC分类号： C08F4/603 , C08F4/659 , C08F4/6592 , C08F10/00 , C08F4/643
CPC分类号： C08F10/00 , C08F4/65908 , C08F4/65912 , C08F4/6592
摘要： A polymerization catalyst comprising a polycation complex (A) represented by the following Formula, [(CUHC).sub.n MX.sub.m ].sup.j+ .multidot.([Y].sup.-)j; [(CUHC): a cyclic unsaturated hydrocarbon group], more particularly, a polymerization catalyst comprising the reaction product of a transition metal compound and an ionic compound (b) capable of forming an ionic complex when reacted with a transition metal compound, and the above-mentioned compound (b), is disclosed.
摘要翻译：包含由下式表示的聚阳离子络合物（A）的聚合催化剂[（CUHC）nMXm] j + x（[Y] - ）j; [（CUHC）：环状不饱和烃基]，更具体地说，是包含过渡金属化合物与能够与过渡金属化合物反应形成离子性络合物的离子性化合物（b）的反应产物的聚合催化剂，上述化合物（b）。

5. 发明授权

US08614093B2 Pharmaceutical composition for treating or preventing cancer by inducing dendritic cell-like differentiation from monocytes to improve anticancer immune activity 有权
标题翻译：通过从单核细胞诱导树突状细胞样分化来治疗或预防癌症以提高抗癌免疫活性的药物组合物
公开(公告)号：US08614093B2
公开(公告)日：2013-12-24
申请号：US12934394
申请日：2009-03-24
申请人： Hiromi Kumon , Yasutomo Nasu , Masami Watanabe , Yuji Kashiwakura
发明人： Hiromi Kumon , Yasutomo Nasu , Masami Watanabe , Yuji Kashiwakura
IPC分类号： C12N5/00 , C12N5/02 , C12N5/071
CPC分类号： A61K38/18 , A61K38/00 , C07K14/4703 , C07K14/4747 , C12N5/0639 , C12N2501/22 , C12N2501/2304 , C12N2501/415
摘要： According to the present invention, a composition for inducing or activating dendritic cell-like cells so as to treat or prevent cancer by immunotherapy is provided.Specifically, the following is provided: an agent for activating cancer immunity, which comprises, as an active ingredient, the following REIC protein: (a) a protein consisting of the amino acid sequence shown in SEQ ID NO: 2; or (b) a protein consisting of an amino acid sequence derived from the amino acid sequence shown in SEQ ID NO: 2 by substitution, deletion, or addition of one or more amino acid(s) and having the activity of inducing differentiation from monocytes into dendritic cell-like cells.
摘要翻译：根据本发明，提供了用于诱导或激活树突状细胞样细胞以通过免疫治疗来治疗或预防癌症的组合物。具体而言，提供以下功能：用于激活癌症免疫的药剂，其包含作为活性成分的以下REIC蛋白质：（a）由SEQ ID NO：2所示的氨基酸序列组成的蛋白质; 或（b）通过取代，缺失或添加一个或多个氨基酸并且具有诱导从单核细胞分化的活性的由源自SEQ ID NO：2所示氨基酸序列的氨基酸序列组成的蛋白质进入树突状细胞样细胞。

6. 发明授权

US07759489B2 Transition metal complex compound and organic electroluminescence device using the compound 失效
标题翻译：使用该化合物的过渡金属络合物和有机电致发光器件
公开(公告)号：US07759489B2
公开(公告)日：2010-07-20
申请号：US11516585
申请日：2006-09-07
申请人： Masami Watanabe , Toshikazu Hirao , Toshiyuki Moriuchi , Lisheng Mao , Hsyueh-Liang Wu
发明人： Masami Watanabe , Toshikazu Hirao , Toshiyuki Moriuchi , Lisheng Mao , Hsyueh-Liang Wu
IPC分类号： C07F15/00 , H05B33/14
CPC分类号： C07F15/0033 , C09K11/06 , C09K2211/185 , H01L51/0067 , H01L51/0071 , H01L51/0072 , H01L51/0084 , H01L51/0085 , H01L51/009 , H05B33/14 , Y10S428/917
摘要： Provided are an organic electroluminescence device having high luminous efficiency and a long emission lifetime, and a transition metal complex compound realizing the organic electroluminescence device. In the transition metal complex compound, three ligands are crosslinked with a crosslinking group having a saturated cyclic structure or a saturated polycyclic structure in a tripod manner. The organic electroluminescence device includes an organic thin film layer composed of one or multiple layers including at least a light emitting layer, the organic thin film layer being interposed between a pair of electrodes. In the organic electroluminescence device, at least one layer of the organic thin film layer contains the transition metal complex compound.
摘要翻译：提供了具有高发光效率和长发光寿命的有机电致发光器件和实现有机电致发光器件的过渡金属络合物。在过渡金属配位化合物中，三个配位体以三脚架方式与具有饱和环状结构或饱和多环结构的交联基团交联。有机电致发光元件包括由至少包含发光层的一层或多层构成的有机薄膜层，有机薄膜层介于一对电极之间。在有机电致发光器件中，有机薄膜层的至少一层含有过渡金属络合物。

7. 发明申请

US20070132372A1 AMINE BASED COMPOUND AND ORGANIC ELECTROLUMINESCENCE DEVICE USING THE SAME 审中-公开
标题翻译：基于胺的化合物和使用该化合物的有机电致发光器件
公开(公告)号：US20070132372A1
公开(公告)日：2007-06-14
申请号：US11551845
申请日：2006-10-23
申请人： Tetsuya Inoue , Masami Watanabe , Hirofumi Kondo
发明人： Tetsuya Inoue , Masami Watanabe , Hirofumi Kondo
IPC分类号： H01J1/62 , C07D241/36 , H01J63/04
CPC分类号： C07D241/38 , C09K11/06 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , H01L51/0058 , H01L51/0059 , H01L51/0072 , H01L51/0081 , H01L51/5012 , H01L51/5088 , H05B33/14
摘要： The present invention provides an organic electroluminescence device which: brings physical properties, that is, a low ionization potential, large band gap energy, high injection efficiency, and a high mobility into balance in an excellent manner; has high heat resistance; and shows high current efficiency and a long lifetime while maintaining good luminance/voltage characteristics and good current density/voltage characteristics, and a novel amine-based compound for realizing the device. The amine-based compound is of a specific structure containing a quinoxaline ring. The organic electroluminescence device includes an organic thin film layer composed of one or more layers including at least a light emitting layer, the organic thin film layer being interposed between a cathode and an anode. In the organic electroluminescence device, at least one layer of the organic thin film layer contains the amine-based compound alone or as a component of a mixture.
摘要翻译：本发明提供了一种有机电致发光器件，其以极好的方式将物理性质，即低电离电位，大带隙能量，高注入效率和高迁移率平衡化; 具有高耐热性; 并且在保持良好的亮度/电压特性和良好的电流密度/电压特性的同时显示出高电流效率和长寿命，以及用于实现该器件的新颖的胺基化合物。胺类化合物是含有喹喔啉环的特定结构。有机电致发光器件包括由至少包含发光层的一层或多层构成的有机薄膜层，该有机薄膜层介于阴极和阳极之间。在有机电致发光器件中，有机薄膜层的至少一层仅含有胺类化合物或作为混合物的成分。

8. 发明授权

US5586544A Fuel injection amount control system for internal combustion engines and intake passage wall temperature-estimating device used therein 失效
标题翻译：用于内燃机的燃料喷射量控制系统和其中使用的进气通道壁温度估计装置
公开(公告)号：US5586544A
公开(公告)日：1996-12-24
申请号：US351210
申请日：1994-11-30
申请人： Toru Kitamura , Akira Katoh , Katsuhiro Kumagai , Sachito Fujimoto , Hiroshi Kitagawa , Shunichi Tsuzuki , Jun Takahashi , Masami Watanabe
发明人： Toru Kitamura , Akira Katoh , Katsuhiro Kumagai , Sachito Fujimoto , Hiroshi Kitagawa , Shunichi Tsuzuki , Jun Takahashi , Masami Watanabe
IPC分类号： F02D41/04 , F02D41/06 , F02D41/14 , F02D41/32
CPC分类号： F02D41/047 , F02D2200/0414
摘要： A fuel injection mount control system for an internal combustion engine includes an ECU which calculates a first amount of fuel directly drawn into each combustion chamber out of an amount of fuel injected into the intake passage via a corresponding fuel injection valve, a second amount of fuel carried off fuel adhering to the wall surface of the intake passage into the combustion chamber, and an amount of fuel to be injected into the intake passage, based on the first fuel amount and the second fuel amount, calculates an air-fuel ratio correction amount, based on an output form an air-fuel ratio sensor arranged in the exhaust system, and corrects the amount of fuel to be injected into the intake passage by the air-fuel ratio correction amount. Further, the ECU corrects the second fuel amount, based on the air-fuel ratio correction amount.
摘要翻译：一种用于内燃机的燃料喷射安装控制系统包括：ECU，其经由相应的燃料喷射阀计算经由相应的燃料喷射阀喷射到进气通道中的燃料量中直接吸入每个燃烧室的第一燃料量;第二量的燃料将附着在进气通道的壁面上的燃料排出到燃烧室内，并且基于第一燃料量和第二燃料量喷射到进气通道中的燃料量计算空燃比校正量基于布置在排气系统中的空燃比传感器的输出形式，并且通过空燃比校正量来校正要喷射到进气通道中的燃料量。此外，ECU基于空燃比校正量来校正第二燃料量。

9. 发明授权

US5171919A Process for producing propylene based oligomers 失效
标题翻译：生产基于丙烯的低聚物的方法
公开(公告)号：US5171919A
公开(公告)日：1992-12-15
申请号：US777788
申请日：1991-10-17
申请人： Masami Watanabe , Nobuhide Ishihara
发明人： Masami Watanabe , Nobuhide Ishihara
IPC分类号： C07C2/34
CPC分类号： C07C2/34 , C07C2531/14 , C07C2531/22 , Y10S526/943
摘要： A process for producing a propylene based oligomer which comprises polymerizing propylene alone or propylene and an olefin other than propylene in the presence of a catalyst comprising:(A) a transition metal compound represented by the general formula (I):(R.sub.5 C.sub.5).sub.m MX.sub.4-m (I) wherein R.sub.5 C.sub.5 may be the same as or different from each other and is a hydrocarbon group-substituted cyclopentadienyl group; M is a zirconium atom or hafnium atom; X may be the same as or different from each other and is a hydrogen atom, halogen atom or hydrocarbon group; m is an integer of from 1 to 4; and(B) a compound capable of forming an ionic complex when reacted with a transition metal compound, is disclosed.According to the present invention, a propylene oligomer can be produced without using a promoter such as aluminoxane or with use of a small amount of an organoaluminum compound. Therefore, according to the present invention, such propylene based oligomers can be produced at reduced cost with use of the process comprising a simplified deashing step.

10. 发明授权

US4512874A Method for producing mesophase continuously 失效
标题翻译：连续生产中间相的方法
公开(公告)号：US4512874A
公开(公告)日：1985-04-23
申请号：US507587
申请日：1983-06-24
申请人： Masami Watanabe
发明人： Masami Watanabe
IPC分类号： C10C3/00 , D01F9/14
CPC分类号： C10C3/002
摘要： A method for producing continuously 100% mesophase composed only of Q.I. component and Q.S. component in which a raw material of petroleum origin pitch is subjected continuously to a heat-treatment step in an amount necessary to produce a 100% mesophase taken out from a mesophase-growing and coalescing step, transferring the heat-formed pitch formed in the heat treatment step to a mesophase growing and coalescing step, taking out a definite amount of a non-mesophase pitch from the mesophase growing and coalescing step after stirring and heating treatment to return it to the heat-treatment step to repeat the stirring and heating treatment, and at the same time to take out 100% mesophase having constant properties from the mesophase growing and coalescing step.
摘要翻译：连续生产仅由Q.I.组成的100％中间相的方法。组件和Q.S. 其中将石油来源沥青的原料连续地进行到从中间相生长和聚结步骤中取出的产生100％中间相所需量的热处理步骤的组分，转移在热量中形成的热成形沥青处理步骤进行中间相生长和聚结步骤，在搅拌和加热处理之后从中间相生长和聚结步骤中取出一定量的非中间相沥青以将其返回到热处理步骤以重复搅拌和加热处理，同时从中间相生长和聚结步骤中取出具有恒定性能的100％中间相。

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