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1. 发明授权

US10062920B2 Powder supplying device and electrode manufacturing apparatus 有权
公开(公告)号：US10062920B2
公开(公告)日：2018-08-28
申请号：US14779677
申请日：2014-03-11
申请人： Masahiro Umeda , Yasuhiro Sakashita , Koichi Tanihara , Naohiro Hasama , Ryo Nakatani
发明人： Masahiro Umeda , Yasuhiro Sakashita , Koichi Tanihara , Naohiro Hasama , Ryo Nakatani
IPC分类号： H01M10/04 , B05C19/06 , B05B5/08 , B05C19/04 , H01M4/04 , B30B15/30 , B05C19/00 , B05B5/16 , B05B7/14 , B05B5/04 , B05C11/02
CPC分类号： H01M10/0404 , B05B5/0418 , B05B5/081 , B05B5/084 , B05B5/1683 , B05B7/144 , B05C11/023 , B05C19/008 , B05C19/04 , B05C19/06 , B30B15/308 , H01M4/0435 , Y10S118/16
摘要： A powder supplying device (2) includes a case (6) in which a storage portion (6a) is formed for temporarily storing powder (10), the case (6) having an inlet (6b) formed in an upper end of the storage portion (6a), and a rectangular outlet (6c) formed in a lower end of the storage portion (6a); a rotor (7) that is arranged in the case (6) and transports the powder (10) in the storage portion (6a) to the outlet (6c) by rotating; and a mesh body (8) through which the powder (10) that has been transported to the outlet (6c) passes. The powder supplying device (2) supplies the powder (10) onto an upper surface of an electrode foil (5). The rotor (7) has a brush-like shape, with a plurality of hair members (7b) radially implanted pointing radially outward with an axial center (G) of the rotor (7) as the center.

2. 发明授权

US4530768A Method for the disposal of waste water containing iron-cyanide complexes 失效
标题翻译：处理含有氰化铁配合物的废水的方法
公开(公告)号：US4530768A
公开(公告)日：1985-07-23
申请号：US577354
申请日：1984-02-06
申请人： Koichi Tanihara , Keiko Tamai , Seiji Yasuda
发明人： Koichi Tanihara , Keiko Tamai , Seiji Yasuda
IPC分类号： C02F9/00 , C02F1/70
CPC分类号： C02F1/5245 , C02F2101/18 , Y10S210/904
摘要： The invention provides an improvement in the disposal of a waste water coining iron-cyanide complexes including ferricyanides by the reduction of the ferricyanide ions into ferrocyanide in the presence of a zinc salt to precipitate the ferrocyanide ions in the form of zinc ferrocyanide. The improvement comprises the use of a sulfite, e.g. sodium sulfite, and a thiosulfate, e.g. sodium thiosulfate, in combination as the reducing agent whereby the reduction of the ferricyanide ions is complete within a relatively short time without being affected by the atmospheric oxygen or other factors.
摘要翻译：本发明通过在锌盐存在下将铁氰化物离子还原成亚铁氰化物，使包含铁氰化物的氰化铁络合物的废水的处理得到改进，以亚铁氰化锌的形式沉淀亚铁氰化物离子。改进之处在于使用亚硫酸盐，例如亚硫酸钠和硫代硫酸盐，例如硫代硫酸钠，作为还原剂组合，由此铁氰化物离子的还原在相对短的时间内完成，而不受大气氧或其它因素的影响。

3. 发明授权

US4986969A Method for recovering gallium value from aqueous solution of crude aluminum salt 失效
标题翻译：从粗铝盐水溶液中回收镓值的方法
公开(公告)号：US4986969A
公开(公告)日：1991-01-22
申请号：US394940
申请日：1989-08-17
申请人： Koichi Tanihara
发明人： Koichi Tanihara
IPC分类号： C01G15/00 , C01F7/47 , C22B58/00
CPC分类号： C22B58/00
摘要： An efficient method is proposed for the recovery of a trace amount of a gallium value from an aqueous solution containing a large amount of an aluminum salt as the principal solute as in the solution which is prepared by dissolving the precipitates obtained by neutralizing a Bayer's solution with carbon dioxide in hydrochloric or sulfuric acid. The method comprises admixing the aqueous solution with a water-soluble ferrocyanide compound, e.g., sodium ferrocyanide, as a precipitant of gallium ferrocyanide in such a controlled small amount as not to exceed 2.5 times by moles of the gallium ions in the starting solution so that coprecipitation of aluminum ferrocyanide is minimized.
摘要翻译：提出了一种从含有大量铝盐作为主要溶质的水溶液中回收痕量镓值的有效方法，如通过将通过将拜耳溶液中和而获得的沉淀物溶解而制备的溶液，二氧化碳在盐酸或硫酸中。该方法包括将水溶液与水溶性亚铁氰化物化合物（例如亚铁氰化钠）混合，作为亚砷氰酸镓的沉淀剂，其控制量少至不超过起始溶液中镓离子摩尔数的2.5倍，使得铝氰化亚铝的共沉淀最小化。

4. 发明授权

US6046131A Method for the preparation of a cesium-separating sorbent 有权
标题翻译：铯分离吸附剂的制备方法
公开(公告)号：US6046131A
公开(公告)日：2000-04-04
申请号：US136044
申请日：1998-08-18
申请人： Koichi Tanihara
发明人： Koichi Tanihara
IPC分类号： B01J20/06 , B01J20/02 , B01J20/10 , B01J20/26 , B01J20/32 , C01D17/00
CPC分类号： B01J20/28019 , B01J20/103 , B01J20/223 , B01J20/26 , B01J20/261 , B01J20/28004 , B01J20/28014 , B01J20/28069 , B01J20/28078 , B01J20/28097 , B01J20/3204 , B01J20/321 , B01J20/3265 , B01J20/3425 , B01J20/3433 , B01J20/3475
摘要： The invention provides a method for the preparation of a sorbent capable of efficiently and selectively sorbing cesium ions from an aqueous solution. The method comprises impregnating the pores of a high-porosity carrier material such as silica gel and porous adsorbent resin with water-soluble potassium or sodium hexacyanoferrate (II) and contacting the carrier material with a solution of a copper salt in a solvent in which the water-soluble hexacyanoferrate (II) is hardly soluble such as ethyl alcohol to convert the water-soluble hexacyanoferrate (II) into water-insoluble copper hexacyanoferrate (II). The cesium ions sorbed on the sorbent can be readily desorbed and the sorbent can readily be regenerated. Alternatively, the carrier material is impregnated with a water-soluble hexacyanoferrate (III) which is converted into copper hexacyanoferrate (III) followed by a reducing reaction of the same into copper hexacyanoferrate (II).
摘要翻译：本发明提供了一种制备能够有效和选择性地从水溶液中吸附铯离子的吸附剂的方法。该方法包括用水溶性钾或六氰基铁酸钾（II）浸渍高孔隙率载体材料如硅胶和多孔吸附树脂的孔，并使载体材料与铜盐在溶剂中的溶液接触，其中水溶性六氰基铁酸盐（II）几乎不溶于乙醇，将水溶性六氰基铁酸盐（II）转化为水不溶性六氰基铁氰酸铜（II）。吸附剂上吸附的铯离子可以很容易地解吸，吸附剂可以很容易地被再生。或者，载体材料用水溶性六氰基铁酸盐（III）浸渍，将其转化为六氰基铁酸铜（III），随后将其还原为六氰合铁酸铜（II）。

5. 发明授权

US4388474A Method for the preparation of guanidine sulfamate 失效
标题翻译：制备氨基磺酸胍的方法
公开(公告)号：US4388474A
公开(公告)日：1983-06-14
申请号：US241236
申请日：1981-03-06
申请人： Koichi Tanihara
发明人： Koichi Tanihara
IPC分类号： C07C279/02 , C07C67/00 , C07C239/00 , C07C307/02 , C07C143/837
CPC分类号： C07C307/02
摘要： The invention provides a novel method for the preparation of guanidine sulfamate from the reaction mixture of urea and an ammonium aqua-ammonosulfate, e.g. ammonium imidosulfonate, obtained by the reaction under atmospheric pressure followed by hydrolysis with water. Different from conventional procedures, the hydrolysis in the inventive method is carried out at a temperature not exceeding 100.degree. C. or, preferably, at about 70.degree. C., in which the retardation of the reaction velocity at the lower temperature is compensated for by admixing the aqueous solution of the reaction mixture with a portion of the hydrolysis product obtained in the preceding run. After completion of the hydrolysis reaction, the hydrolysis product is admixed with calcium hydroxide or oxide and the desired guanidine sulfamate is obtained from the liquid portion from which the excess of the calcium ions has been removed.
摘要翻译：本发明提供了一种从尿素和氨基硫酸铵的反应混合物制备氨基磺酸胍的新方法，通过在大气压下反应然后用水水解获得的亚氨基磺酸铵。与常规方法不同，本发明方法中的水解在不超过100℃或优选在约70℃的温度下进行，其中在较低温度下的反应速度的延迟由将反应混合物的水溶液与前述流程中获得的水解产物的一部分混合。水解反应完成后，水解产物与氢氧化钙或氧化物混合，所需的氨基磺酸氨基磺酸盐由已除去过量钙离子的液体部分得到。

6. 发明授权

US5601722A Method for the preparation of an ion exchanger for cesium ions and method for the regeneration thereof 失效
标题翻译：铯离子离子交换剂的制备方法及其再生方法
公开(公告)号：US5601722A
公开(公告)日：1997-02-11
申请号：US554980
申请日：1995-11-13
申请人： Koichi Tanihara
发明人： Koichi Tanihara
IPC分类号： B01J39/08 , B01J41/04 , B01J47/00 , B01J49/00 , C01D17/00 , G21F9/12 , F23G7/00
CPC分类号： G21F9/12 , B01J41/04 , B01J47/006 , B01J49/0013 , C22B3/42 , Y02P10/234
摘要： Proposed is a method for the preparation of an efficient ion exchanger useful for separation and recovery of cesium ions from an aqueous solution such as strongly acidic waste solutions containing radioactive species of cesium. The method comprises the steps of (a) adsorption of hexacyanoferrate (II) ions on to porous particles of an anion exchange resin, (b) conversion of the hexacyanoferrate (II) ions into water-insoluble copper salt thereof in situ in the resin pores, (c) an oxidation treatment of the resin particles and (d) a reduction treatment in the presence of potassium ions followed by contacting of the resin particles with an aqueous solution containing copper ions. A method for the regeneration of the ion exchanger after adsorption of cesium ions is also proposed.
摘要翻译：提出了一种用于制备有效的离子交换剂的方法，其用于从诸如含有放射性铯的强酸性废溶液的水溶液中分离和回收铯离子。该方法包括以下步骤：（a）将六氰基铁酸盐（II）离子吸附在阴离子交换树脂的多孔颗粒上，（b）将六氰基铁酸盐（II）离子原位转化为树脂孔中的水不溶性铜盐，（c）树脂颗粒的氧化处理和（d）在钾离子存在下进行还原处理，然后使树脂颗粒与含有铜离子的水溶液接触。还提出了在吸附铯离子之后再生离子交换剂的方法。

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