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1. 再颁专利

USRE39222E1 Process for preparing 2,6-dialkylnaphthalene 有权
公开(公告)号：USRE39222E1
公开(公告)日：2006-08-01
申请号：US10076431
申请日：2002-02-19
申请人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul McWilliams , Susan Patricia Donnelly
发明人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul McWilliams , Susan Patricia Donnelly
IPC分类号： C07C1/00 , C07C4/12 , C07C5/22 , C07C2/68 , C08G63/181
CPC分类号： C07C4/12 , C07C15/24 , C07C2521/04 , C07C2523/26 , C07C2523/75 , C07C2523/883 , C07C2529/06 , C08G63/189
摘要： A process for producing 2,6-dialkylnaphthalene from a hydrocarbon feedstock that contains at least one component selected from the group consisting of dialkylnaphthalene isomers, monoalkylnaphthalene isomers, polyalkylnaphthalenes, and naphthalene, is provided that includes the following steps: I. separating the hydrocarbon feedstock and/or a dealkylation product fed from step III into a naphthalene fraction, a monoalkylnaphthalene fraction, a dialkylnaphthalene fraction and a remaining products fraction; II. separating and purifying 2,6-dialkylnaphthalene from the dialkylnaphthalene fraction of step I; III. dealkylating the hydrocarbon feedstock and/or the remaining products fraction of step I and feeding the dealkylation product to step I; and IV. alkylating the naphthalene and monoalkylnaphthalene fractions of step I; wherein the hydrocarbon feedstock is fed to step I or step III.

2. 发明授权

US6011190A Process for preparing dialkylnaphthalene 失效
标题翻译：制备二烷基萘的方法
公开(公告)号：US6011190A
公开(公告)日：2000-01-04
申请号：US887052
申请日：1997-07-02
申请人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul McWilliams
发明人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul McWilliams
IPC分类号： B01J29/04 , C07B61/00 , C07C2/66 , C07C6/12 , C07C15/24 , C07C1/01 , C07C2/64 , C07C2/68 , C07C5/22
CPC分类号： C07C15/24 , C07C2/66 , C07C6/126 , C07C2529/70
摘要： 2,6-Dialkylnaphthalene is prepared from a feedstock comprising naphthalene and an alkylating agent, by a process comprising the steps:(I) transalkylating isomers of dialkylnaphthalene and naphthalene to produce monoalkylnaphthalene and isomers of dialkylnaphthalene;(II) separating the product obtained in step (I) into naphthalene, monoalkylnaphthalene, dialkylnaphthalene and other components;(III) alkylating the monoalkylnaphthalene fraction from step (II) with an alkylating agent to produce dialkylnaphthalene; and(IV) separating 2,6-dialkylnaphthalene from the dialkylnaphthalene fraction in step (II),wherein at least step (I) or step (III) is conducted in the presence of a catalyst having a composition comprising a synthetic zeolite having an X-ray diffraction pattern with an interplanar d-spacing (.ANG.)______________________________________ 12.36 .+-. 0.4 11.03 .+-. 0.2 8.83 .+-. 0.14 6.18 .+-. 0.12 6.00 .+-. 0.10 4.06 .+-. 0.07 3.91 .+-. 0.07 3.42 .+-. 0.06. ______________________________________
摘要翻译： 2,6-二烷基萘由包含萘和烷基化剂的原料制备，通过包括以下步骤的方法制备：（I）将烷基萘和萘的异构体转烷基化以产生单烷基萘和二烷基萘的异构体; （II）将步骤（I）中获得的产物分离成萘，单烷基萘，二烷基萘等组分; （III）用烷基化剂烷基化来自步骤（II）的单烷基萘馏分以制备二烷基萘; 和（IV）在步骤（II）中从二烷基萘馏分中分离2,6-二烷基萘，其中至少步骤（I）或步骤（III）在具有包含具有X 具有面间d间距（ANGSTROM）的-ray衍射图 - 12.36 +/- 0.4-11.03 +/- 0.2-8.83 +/- 0.14-6.18 +/- 0.12- 6.00 +/- 0.10-4.06 +/- 0.07- 3.91 +/- 0.07 - 3.42 +/- 0.06。 -

3. 再颁专利

USRE41136E1 Process for preparing 2,6-dialkylnaphthalene 有权
标题翻译：制备2,6-二烷基萘的方法
公开(公告)号：USRE41136E1
公开(公告)日：2010-02-16
申请号：US10053690
申请日：2002-01-24
申请人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul McWilliams , Susan Patricia Donnelly
发明人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul McWilliams , Susan Patricia Donnelly
IPC分类号： C07C1/00 , C07C2/68 , C07C5/22 , C07C4/12 , C08G63/02 , C08G63/00
CPC分类号： C07C4/12 , C07C15/24 , C07C2521/04 , C07C2523/26 , C07C2523/75 , C07C2523/883 , C07C2529/06 , C08G63/189
摘要： The present invention relates to a process of preparing dialkylnaphthylenes and polyalkylenenaphthyleneates dialkylnaphthalenes and polyalkylenenaphthalates.
摘要翻译：本发明涉及制备二烷基萘和聚亚烷基亚萘基二烷基萘和聚亚烷基亚萘基酯的方法。

4. 发明授权

US5723711A Process for preparing 2-methylnaphthalene 失效
标题翻译： 2-甲基萘的制备方法
公开(公告)号：US5723711A
公开(公告)日：1998-03-03
申请号：US744828
申请日：1996-11-06
申请人： Masahiro Motoyuki , Koji Yamamoto , John Paul McWilliams , Ajit Vishwanath Sapre
发明人： Masahiro Motoyuki , Koji Yamamoto , John Paul McWilliams , Ajit Vishwanath Sapre
IPC分类号： B01J29/06 , C07C5/22 , C07C5/27 , C07C15/24
CPC分类号： C07C5/2737 , C07C2529/70
摘要： A process for producing 2-methylnaphthalene from a feedstock containing 1-methylnaphthalene by contacting the feedstock with a catalyst composition, in which the process comprising isomerization of 1-methylnaphthalene, wherein the catalyst composition comprising a synthetic zeolite characterized by an X-ray diffraction pattern including interplanar d-spacing as set forth in Table A of the specification.
摘要翻译：通过使原料与催化剂组合物接触，由含有1-甲基萘的原料生产2-甲基萘的方法，其中所述方法包括1-甲基萘的异构化，其中所述催化剂组合物包含以X射线衍射图案为特征的合成沸石包括说明书的表A所示的平面间距d。

5. 发明授权

US6018087A Isomerization of dimethylnaphthalene to produce 2,6-dimethylnaphthalene 失效
标题翻译：二甲基萘异构化生成2,6-二甲基萘
公开(公告)号：US6018087A
公开(公告)日：2000-01-25
申请号：US948666
申请日：1997-10-10
申请人： Masahiro Motoyuki , Koji Yamamoto , Shingo Yoshida , Seiichi Yamamoto , Ajit Vishwanath Sapre , John Paul Mc Williams , Susan Patricia Donnelly , Stuart Damon Hellring
发明人： Masahiro Motoyuki , Koji Yamamoto , Shingo Yoshida , Seiichi Yamamoto , Ajit Vishwanath Sapre , John Paul Mc Williams , Susan Patricia Donnelly , Stuart Damon Hellring
IPC分类号： C07C15/24 , C08G63/189 , C07C5/22 , C08G63/06
CPC分类号： C07C15/24 , C08G63/189
摘要： The present invention relates to a method of preparing 2,6-dimethylnaphthalene from a feed stream that contains hydrocarbons which contain dimethylnaphthalene isomers. The method includes the following steps:I. distillation and concentration of the dimethylnaphthalene isomers from the feed stream, to form a dimethylnaphthalene fraction,II. isomerization of the dimethylnaphthalene fraction to enrich the dimethylnaphthalene fraction in 2,6-dimethylnaphthalene, to form a 2,6-enriched dimethylnaphthalene fraction,III. purification of 2,6-dimethylnaphthalene from the 2,6-enriched dimethylnaphthalene fraction,wherein step II is conducted in the presence of a catalyst composition containing a synthetic zeolite characterized by an X-ray diffraction pattern including interplanar d-spacing (.ANG.)12.36.+-.10.411.03.+-.0.28.83.+-.10.146.18.+-.0.126.00.+-.0.104.06.+-.0.073.91.+-.0.013.42.+-.0.06,wherein the purification includes crystallization under pressure.
摘要翻译：本发明涉及从含有二甲基萘异构体的烃的进料流中制备2,6-二甲基萘的方法。该方法包括以下步骤：I.从进料流中蒸馏并浓缩二甲基萘异构体，形成二甲基萘馏分。二甲基萘馏分的异构化以富集2,6-二甲基萘中的二甲基萘馏分，形成富2,6-二甲基萘馏分。从2,6-富二甲基萘馏分中纯化2,6-二甲基萘，其中步骤II在含有合成沸石的催化剂组合物的存在下进行，该催化剂组合物的特征在于包括平面d间距（ANGSTROM）12.36的X射线衍射图 +/- 10.4 11.03 +/- 0.2 8.83 +/- 10.14 6.18 +/- 0.12 6.00 +/- 0.10 4.06 +/- 0.07 3.91 +/- 0.01 3.42 +/- 0.06，其中纯化包括在压力下的结晶。

6. 发明授权

US6018086A Process for preparing 2,6-dialkylnaphthalene 失效
标题翻译：制备2,6-二烷基萘的方法
公开(公告)号：US6018086A
公开(公告)日：2000-01-25
申请号：US948299
申请日：1997-10-10
申请人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul Mc Williams , Susan Patricia Donnelly
发明人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul Mc Williams , Susan Patricia Donnelly
IPC分类号： C07C2/86 , C07B61/00 , C07C4/12 , C07C5/22 , C07C6/12 , C07C7/14 , C07C15/24 , C08G63/189 , C08G63/78 , C07C1/00 , C07C2/68
CPC分类号： C07C4/12 , C07C15/24 , C08G63/189 , C07C2521/04 , C07C2523/26 , C07C2523/75 , C07C2523/883 , C07C2529/06
摘要： The present invention relates to a process of preparing dialkylnaphthylenes and polyalkylenenaphthyleneates.
摘要翻译：本发明涉及制备二烷基萘和聚亚烷基亚乙烯二酸酯的方法。

7. 发明授权

US6121501A Process for preparing 2,6-dialkylnaphthalene 有权
标题翻译：制备2,6-二烷基萘的方法
公开(公告)号：US6121501A
公开(公告)日：2000-09-19
申请号：US288847
申请日：1999-04-09
申请人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul Mc Williams , Susan Patricia Donnelly
发明人： Masahiro Motoyuki , Koji Yamamoto , Ajit Vishwanath Sapre , John Paul Mc Williams , Susan Patricia Donnelly
IPC分类号： C07C2/86 , C07B61/00 , C07C4/12 , C07C5/22 , C07C6/12 , C07C7/14 , C07C15/24 , C08G63/189 , C08G63/78 , C07C1/00 , C07C2/68
CPC分类号： C07C4/12 , C07C15/24 , C08G63/189 , C07C2521/04 , C07C2523/26 , C07C2523/75 , C07C2523/883 , C07C2529/06
摘要： A process for producing 2,6-dialkylnaphthalene from a hydrocarbon feedstock that contains at least one component selected from the group consisting of dialkylnaphthalene isomers, monoalkylnaphthalene isomers, polyalkylnaphthalenes, and naphthalene, is provided that includes the following steps:I. separating the hydrocarbon feedstock and/or a dealkylation product fed from step III into a naphthalene fraction, a monoalkylnaphthalene fraction, a dialkylnaphthalene fraction and a remaining products fraction;II. separating and purifying 2,6-dialkylnaphthalene from the dialkylnaphthalene fraction of step I;III. dealkylating the hydrocarbon feedstock and/or the remaining products fraction of step I and feeding the dealkylation product to step I; andIV. alkylating the naphthalene and monoalkylnaphthalene fractions of step I;wherein the hydrocarbon feedstock is fed to step I or step III.
摘要翻译：提供了一种从烃原料生产2,6-二烷基萘的方法，该方法含有至少一种选自二烷基萘异构体，单烷基萘异构体，聚烷基萘和萘的组分，其包括以下步骤：I.分离烃原料和/或从步骤III进料至萘馏分，单烷基萘馏分，二烷基萘馏分和剩余产物馏分的脱烷基化产物; 二，从步骤I的二烷基萘部分分离和纯化2,6-二烷基萘; 三，将烃原料和/或步骤I的剩余产物馏分脱烷基化，并将脱烷基产物进料至步骤I; 和IV。烷基化步骤I的萘和单烷基萘馏分; 其中将烃原料进料至步骤I或步骤III。

8. 发明授权

US5844064A Process for preparing dialkylnaphthalene 失效
标题翻译：制备二烷基萘的方法
公开(公告)号：US5844064A
公开(公告)日：1998-12-01
申请号：US974231
申请日：1997-11-19
申请人： Masahiro Motoyuki , Koji Yamamoto , John Paul McWilliams , Robert Glenn Bundens
发明人： Masahiro Motoyuki , Koji Yamamoto , John Paul McWilliams , Robert Glenn Bundens
IPC分类号： B01J29/06 , C07B61/00 , C07C5/27 , C07C6/12 , C07C15/24 , C08G63/189 , C08G63/02 , C08G63/00
CPC分类号： C08G63/189 , C07C15/24 , C07C6/126 , C07C2529/70
摘要： A process for producing alkylnaphthalene from a feedstock comprising isomers of dialkylnaphthalene and naphthalene by contacting the feedstock with a catalyst composition, in which the process comprising transalkylation between isomers of dialkylnaphthalene and naphthalene to produce monoalkylnaphthalene, and isomerization of dialkylnaphthalene, wherein the catalyst composition comprising a synthetic zeolite characterized by an X-ray diffraction pattern including interplanar d-spacing as set forth in Table A of the specification.
摘要翻译：通过使原料与催化剂组合物接触，由原料包含二烷基萘和萘的异构体制备烷基萘的方法，其中该方法包括二烷基萘和萘的异构体之间的烷基转移以产生单烷基萘，和二烷基萘的异构化，其中催化剂组合物包含其特征在于包括本说明书的表A所示的平面d间距的X射线衍射图案。

9. 发明授权

US5744670A Process for preparing dialkylnaphthalene 失效
公开(公告)号：US5744670A
公开(公告)日：1998-04-28
申请号：US661114
申请日：1996-06-10
申请人： Masahiro Motoyuki , Koji Yamamoto , John Paul McWilliams , Robert Glenn Bundens
发明人： Masahiro Motoyuki , Koji Yamamoto , John Paul McWilliams , Robert Glenn Bundens
IPC分类号： B01J29/06 , C07B61/00 , C07C5/27 , C07C6/12 , C07C15/24 , C08G63/189 , C07C2/00 , C07C2/66 , C07C5/22
CPC分类号： C08G63/189 , C07C15/24 , C07C6/126 , C07C2529/70
摘要： A process for producing alkylnaphthalene from a feedstock comprising isomers of dialkylnaphthalene and naphthalene by contacting the feedstock with a catalyst composition, in which the process comprising transalkylation between isomers of dialkylnaphthalene and naphthalene to produce monoalkylnaphthalene, and isomerization of dialkylnaphthalene, wherein the catalyst composition comprising a synthetic zeolite characterized by an X-ray diffraction pattern including interplanar d-spacing as set forth in Table A of the specification.

10. 发明授权

US06706939B2 Method for concentrating 2,6-dimethylnaphthalene 有权
标题翻译：浓缩2,6-二甲基萘的方法
公开(公告)号：US06706939B2
公开(公告)日：2004-03-16
申请号：US10193228
申请日：2002-07-12
申请人： Noboru Nakao , Koji Yamamoto , Masahiro Motoyuki
发明人： Noboru Nakao , Koji Yamamoto , Masahiro Motoyuki
IPC分类号： C07C712
CPC分类号： C07C7/13 , C07C15/24
摘要： A method for concentrating 2,6-dimethylnaphthalene in a dimethylnaphthalene isomer mixture includes supplying the dimethylnaphthalene isomer mixture to an adsorption column packed with Y-type zeolite. In this instance, by setting the value derived from the expression (u1/3/&egr;)d−5/3 at 14 (m5/3 s−1/3 kg−1) or more, the concentration ratio of 2,6-dimethylnaphthalene to 2,7-dimethylnaphthalene can be 2.0 or more. u here represents the linear velocity (m/s) of the dimethylnaphthalene isomer mixture supplied to an adsorption column, &egr; represents the packing density (kg/m3) of Y-type zeolite, and d represents the grain size (m) of the Y-type zeolite.
摘要翻译：将2,6-二甲基萘浓缩在二甲基萘异构体混合物中的方法包括将二甲基萘异构体混合物供应到填充有Y型沸石的吸附塔上。在这种情况下，通过在14（m <5/3> s <-1 / 3> kg -1）处设定从表达式（u <1/3 /ε）d <-5/3>导出的值）以上时，2,6-二甲基萘与2,7-二甲基萘的浓度比可以为2.0以上。这里表示供给吸附塔的二甲基萘异构体混合物的线速度（m / s），ε表示Y型沸石的填充密度（kg / m 3），d表示粒径（μm）的Y型沸石。

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