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1. 发明申请

US20140121411A1 PROCESS FOR SEPARATING MONOCHLOROACETIC ACID AND DICHLOROACETIC ACID VIA EXTRACTIVE DISTILLATION 有权
标题翻译：通过萃取蒸馏分离单氯酸和二氯酸的方法
公开(公告)号：US20140121411A1
公开(公告)日：2014-05-01
申请号：US14126270
申请日：2012-03-13
申请人： Mark Theodorus Gerardus Jongmans , Johannes Josef Pragt , Gerrald Bargeman , Boelo Schuur , Jacobus Theodorus Josef Aaldering , André Banier De Haan , Melle Rinze Nieuwhof , Paul Verwer , Anton Alexandru Kiss , Antoon Jacob Berend Ten Kate , Cornelis Johannes Govardus Van Strien
发明人： Mark Theodorus Gerardus Jongmans , Johannes Josef Pragt , Gerrald Bargeman , Boelo Schuur , Jacobus Theodorus Josef Aaldering , André Banier De Haan , Melle Rinze Nieuwhof , Paul Verwer , Anton Alexandru Kiss , Antoon Jacob Berend Ten Kate , Cornelis Johannes Govardus Van Strien
IPC分类号： C07C51/50
CPC分类号： C07C51/50 , C07C51/44 , C07C51/46 , C07C51/48 , C07C51/62 , C07C53/16
摘要： The present invention pertains to a process for separating monochloroacetic acid and dichloroacetic acid from one another via extractive distillation, comprising the steps of (i) contacting a mixture comprising monochloroacetic acid and dichloroacetic acid with an extractive agent which is chemically stable and which has a BF3 affinity of between 65 kJ/mole and 110 kJ/mole, (ii) distilling the mixture to obtain a monochloroacetic acid stream and a stream comprising dichloroacetic acid and the extractive agent, and (iii) regenerating the extractive agent.
摘要翻译：本发明涉及通过萃取蒸馏将一氯乙酸和二氯乙酸彼此分离的方法，包括以下步骤：（i）使包含一氯乙酸和二氯乙酸的混合物与化学稳定的萃取剂接触，并具有BF 3 65kJ / mol和110kJ /摩尔之间的亲和力，（ii）蒸馏混合物以获得一氯乙酸流和包含二氯乙酸和萃取剂的流，和（iii）再生提取剂。

2. 发明授权

US09073848B2 Process for separating monochloroacetic acid and dichloroacetic acid via extractive distillation 有权
标题翻译：通过萃取蒸馏分离一氯乙酸和二氯乙酸的方法
公开(公告)号：US09073848B2
公开(公告)日：2015-07-07
申请号：US14126270
申请日：2012-03-13
申请人： Mark Theodorus Gerardus Jongmans , Johannes Josef Pragt , Gerrald Bargeman , Boelo Schuur , Jacobus Theodorus Josef Aaldering , André Banier De Haan , Melle Rinze Nieuwhof , Paul Verwer , Anton Alexandru Kiss , Antoon Jacob Berend Ten Kate , Cornelis Johannes Govardus Van Strien
发明人： Mark Theodorus Gerardus Jongmans , Johannes Josef Pragt , Gerrald Bargeman , Boelo Schuur , Jacobus Theodorus Josef Aaldering , André Banier De Haan , Melle Rinze Nieuwhof , Paul Verwer , Anton Alexandru Kiss , Antoon Jacob Berend Ten Kate , Cornelis Johannes Govardus Van Strien
IPC分类号： C07C51/50 , C07C51/44 , C07C51/48 , C07C51/62 , C07C51/46
CPC分类号： C07C51/50 , C07C51/44 , C07C51/46 , C07C51/48 , C07C51/62 , C07C53/16
摘要： The present invention pertains to a process for separating monochloroacetic acid and dichloroacetic acid from one another via extractive distillation, comprising the steps of (i) contacting a mixture comprising monochloroacetic acid and dichloroacetic acid with an extractive agent which is chemically stable and which has a BF3 affinity of between 65 kJ/mole and 110 kJ/mole, (ii) distilling the mixture to obtain a monochloroacetic acid stream and a stream comprising dichloroacetic acid and the extractive agent, and (iii) regenerating the extractive agent.
摘要翻译：本发明涉及通过萃取蒸馏将一氯乙酸和二氯乙酸彼此分离的方法，包括以下步骤：（i）使包含一氯乙酸和二氯乙酸的混合物与化学稳定的萃取剂接触，并具有BF 3 65kJ / mol和110kJ /摩尔之间的亲和力，（ii）蒸馏混合物以获得一氯乙酸流和包含二氯乙酸和萃取剂的流，和（iii）再生提取剂。

3. 发明授权

US07135597B2 Process for the preparation of monochloroacetic acid 失效
标题翻译：一氯乙酸的制备方法
公开(公告)号：US07135597B2
公开(公告)日：2006-11-14
申请号：US10529144
申请日：2003-10-02
申请人： Jeroen Crouzen , Johannes Joseph Gorissen , Cornelis Johannes Govardus Van Strien
发明人： Jeroen Crouzen , Johannes Joseph Gorissen , Cornelis Johannes Govardus Van Strien
IPC分类号： C07C51/00
CPC分类号： C07C51/363 , Y02P20/127 , C07C53/16
摘要： The invention pertains to a process for the production of monochloroacetic acid from chlorine and acetic acid in the presence of a catalyst by reactive distillation. The process and the required reactive distillation apparatus is much less complex than conventional reactors and yields a monochloroacetic acid product having a low content of over-chlorinated products.
摘要翻译：本发明涉及通过反应蒸馏在催化剂存在下由氯和乙酸生产一氯乙酸的方法。该方法和所需的反应蒸馏装置比常规反应器复杂得多，并产生具有低含量过氯化产物的一氯乙酸产物。

4. 发明授权

US08778189B2 Use of an adsorbent for the removal of liquid, gaseous and/or dissolved constituents from a process stream 有权
标题翻译：使用吸附剂从工艺流中除去液体，气态和/或溶解成分
公开(公告)号：US08778189B2
公开(公告)日：2014-07-15
申请号：US12280918
申请日：2007-03-05
申请人： Dirk Thomas Meijer , Cornelis Johannes Govardus Van Strien
发明人： Dirk Thomas Meijer , Cornelis Johannes Govardus Van Strien
IPC分类号： B01D11/04 , B01D15/08 , B01D15/10 , B01J20/02 , B01J20/26 , C02F1/26 , C02F1/28 , B01D15/00 , B01J20/18 , B01J20/20 , B01J20/28 , C02F9/00
CPC分类号： B01D11/04 , B01D15/00 , B01J20/18 , B01J20/20 , B01J20/26 , B01J20/261 , B01J20/267 , B01J20/28052 , B01J20/28078 , B01J20/28097 , C02F1/26 , C02F1/28 , C02F1/281 , C02F1/283 , C02F1/285 , C02F1/288 , C02F9/00
摘要： A method for removing liquid, gaseous and/or dissolved constituents from an aqueous stream includes contacting the aqueous stream with a porous material and then contacting the aqueous stream with an adsorbent material. The porous material includes pores having an average diameter of approximately 0.01 μm to approximately 50 μm and an extraction liquid immobilized within at least a portion of the pores.
摘要翻译：从水流中除去液体，气态和/或溶解成分的方法包括使含水物流与多孔材料接触，然后使含水物流与吸附材料接触。多孔材料包括平均直径为约0.01μm至约50μm的孔和固定在孔的至少一部分内的萃取液。

5. 发明申请

US20100311998A1 CHELATING AGENT BASED IONIC LIQUIDS, A PROCESS TO PREPARE THEM, AND THEIR USE 审中-公开
公开(公告)号：US20100311998A1
公开(公告)日：2010-12-09
申请号：US12671667
申请日：2008-07-31
申请人： Cornelia Adriana De Wolf , Boris Kuzmanovic , Johanna Hendrika Bemelaar , Cornelis Johannes Govardus Van Strien , Martin Heus , Antoon Ten Kate
发明人： Cornelia Adriana De Wolf , Boris Kuzmanovic , Johanna Hendrika Bemelaar , Cornelis Johannes Govardus Van Strien , Martin Heus , Antoon Ten Kate
IPC分类号： C07F5/06 , C07C229/26 , C07F11/00 , C07C229/46
CPC分类号： C07C229/16 , C07C211/63 , C07C215/40 , C07C229/76 , C07F9/5407
摘要： The present invention relates to ionic liquids of the formula: (Mm+)xH+ynN+R1R2R3R4Z—N(—CHXCOO−)pY2-p or (Mm+)xH+ynP+R1R2R3R4Z—N(—CHXCOO−)pY2-p wherein any one of R1 to R4 independently represents a hydrogen, alkyl, cycloalkyl, aryl or aralkyl group that may be unsubstituted or substituted with one or more groups selected from OH, Cl, Br, F, I, phenyl, NH2, CN, NO2, an ether group, COOR5, CHO, COR5 or OR5, wherein R5 is an alkyl or cycloalkyl group, and wherein two of the groups R1 to R4 together with the N atom may form a heteroaromatic or heterocyclic group such as a pyridinium, pyrrolidinium or imidazolium group; the Z—N(—CHXCOO−)pY2-p is the anion derived from a chelating agent, wherein Z is a group selected from hydrogen, alkyl, an alkyl group optionally substituted with one or more carboxylate groups, hydroxyl groups and/or optionally containing one or more ether functionalities, or Z is a group of the formula —CH2—CHR6—R7—N—(CH2COO−)2, R6 is hydrogen or a C1-C3 alkyl group, R7 is a single bond, a C1-C3 alkylene group or one or more groups of the formula —N(CH2COO−)—CH2—CHR6—R8—, R8 is a single bond or a C1-C3 alkylene group, p is 2 or 1, X is H, an aryl group that may be unsubstituted or substituted with an OH and/or CH3 substituent, or CH2COO−, and when p is 1, Y is H, a benzyl group that may be unsubstituted or substituted with an OH and/or CH3 group, or a phenyl group that may be unsubstituted or substituted with an OH and/or CH3 substituent, Mm+ is a m-valent metal cation, n is 1 or higher, x is from 0 to 5, y is from 0 to 3, the total positive charge of (Mm+)x, H+y, and nN+R1R2R3R4 or nP+R1R2R3R4 equals the negative charge of the Z—N(—CHXCOO−)pY2-p anion, wherein at least one of the following conditions is fulfilled: i) the chelating agent has a connectivity index 1X/3X of below 2.17, ii) at least two different cations are present in the salt, whereby a proton cation does not count as one of the at least two, iii) at least one cation is a bivalent, trivalent, tetravalent or pentavalent cation, and having a melting point below 120° C. The invention further relates to a process to prepare them and their use.

6. 发明授权

US08361300B2 Method to electrodeposit metals using ionic liquids 失效
标题翻译：使用离子液体电沉积金属的方法
公开(公告)号：US08361300B2
公开(公告)日：2013-01-29
申请号：US12279517
申请日：2007-02-12
申请人： Boris Kuzmanovic , Cornelis Johannes Govardus Van Strien , Colin Eric Bartel , Michael Zeitler , Johanna Christina Speelman
发明人： Boris Kuzmanovic , Cornelis Johannes Govardus Van Strien , Colin Eric Bartel , Michael Zeitler , Johanna Christina Speelman
IPC分类号： C25D3/00
CPC分类号： C25D3/665
摘要： The present invention relates to a method to electroplate or electropolish a metal on a substrate wherein an ionic liquid is selected from the group of N+R1R2R3R4 X− or N+R5R6R7R8 Y− is employed as electrolyte, and a metal salt added to the ionic liquid is employed as the metal source or a metal anode is used as the metal source, wherein any one of R1 to R8 independently represents a hydrogen, alkyl, cycloalkyl, aryl, or aralkyl group that may be substituted with a group selected from OH, Cl, Br, F, I, phenyl, NH2, CN, NO2, COOR9, CHO, COR9, or OR9, at least one of R5 to R8 is a fatty alkyl chain, and one or more of R5 to R8 can be a (poly)oxyalkylene group wherein the alkylene is a C1 to C4 alkylene and the total number of oxyalkylene units can be from 1 to 50 oxyalkylene units, and at least one of R1 to R8 is a C1 to C4 alkyl chain, R9 is an alkyl or cycloalkyl group, X− is an anion having an N-acyl sulphonylimide anion (—CO—N−—SO2—) functionality, Y− is an anion compatible with the N+R5R6R7R8 ammonium cation, such as a halogenide anion, a carboxylate anion, a sulphate (both organic and inorganic sulphate), sulphonate, carbonate, nitrate, nitrite, thiocyanate, hydroxide, or sulphonylimide anion.
摘要翻译：本发明涉及一种在基板上电镀或电解金属的方法，其中离子液体选自N + R1R2R3R4X-或N + R5R6R7R8Y-的组，用作电解质，并将金属盐加入到离子使用液体作为金属源或使用金属阳极作为金属源，其中R 1至R 8中的任何一个独立地表示可以被选自下列基团的氢，烷基，环烷基，芳基或芳烷基取代：OH， Cl，Br，F，I，苯基，NH2，CN，NO2，COOR9，CHO，COR9或OR9，R5至R8中的至少一个为脂肪烷基链，R5至R8中的一个或多个可为（聚）氧化烯基，其中亚烷基是C1-C4亚烷基，氧化烯单元的总数可以是1至50个氧化烯单元，并且R 1至R 8中的至少一个是C 1至C 4烷基链，R 9是烷基或环烷基，X-是具有N-酰基磺酰亚胺阴离子（-CO-N-SO 2 - ）官能团的阴离子，Y-是阴离子与N + R5R6R7R8铵阳离子如卤化物阴离子，羧酸根阴离子，硫酸盐（有机和无机硫酸盐），磺酸盐，碳酸盐，硝酸盐，亚硝酸盐，硫氰酸盐，氢氧化物或磺酰亚胺阴离子相容。

7. 发明申请

US20100252446A1 Method to Electrodeposit Metals Using Ionic Liquids in the Presence of an Additive 审中-公开
标题翻译：在添加剂存在下使用离子液体电沉积金属的方法
公开(公告)号：US20100252446A1
公开(公告)日：2010-10-07
申请号：US12671830
申请日：2008-07-30
申请人： Boris Kuzmanovic , Lamberdine Johanna Willemina Maria Nabuurs-Willems , Cornelis Johannes Govardus Van Strien , Franz Winfried Welter , Johanna Christina Speelman
发明人： Boris Kuzmanovic , Lamberdine Johanna Willemina Maria Nabuurs-Willems , Cornelis Johannes Govardus Van Strien , Franz Winfried Welter , Johanna Christina Speelman
IPC分类号： C25F3/16 , C25D5/00
CPC分类号： C25D3/665 , C25D3/02 , C25F3/16
摘要： The present invention pertains to the use of an additive selected from the group consisting of amorphous silica, graphite powder, and a mixture thereof in a process to electroplate or electropolish a metal on a substrate using an ionic liquid as the electrolyte to increase metal layer thickness. It furthermore pertains to a method to electroplate or electropolish a metal on a metal substrate wherein an ionic liquid is employed as electrolyte, wherein a metal salt added to said ionic liquid or a metal anode is employed as metal source, and wherein said ionic liquid comprises said additive.
摘要翻译：本发明涉及使用选自无定形二氧化硅，石墨粉末及其混合物的添加剂在使用离子液体作为电解质来电镀或电镀基板上的金属的方法中的用途，以增加金属层厚度。此外，本发明还涉及一种在金属基底上电镀或电解金属的方法，其中使用离子液体作为电解质，其中加入所述离子液体或金属阳极的金属盐用作金属源，并且其中所述离子液体包含所述添加剂。

8. 发明申请

US20090236227A1 METHOD TO ELECTRODEPOSIT METALS USING IONIC LIQUIDS 失效
标题翻译：使用离子液体电沉积金属的方法
公开(公告)号：US20090236227A1
公开(公告)日：2009-09-24
申请号：US12279517
申请日：2007-02-12
申请人： Boris Kuzmanovic , Cornelis Johannes Govardus Van Strien , Colin Eric Bartel , Michael Zeitler , Johanna Christina Speelman
发明人： Boris Kuzmanovic , Cornelis Johannes Govardus Van Strien , Colin Eric Bartel , Michael Zeitler , Johanna Christina Speelman
IPC分类号： C25D5/00 , C25F3/16
CPC分类号： C25D3/665
摘要： The present invention relates to a method to electroplate or electropolish a metal on a substrate wherein an ionic liquid selected from the group of N+R1R2R3R4X− or N+R5R6R7R8Y− is employed as electrolyte, and a metal salt added to the ionic liquid is employed as the metal source or a metal anode is used as the metal source, wherein any one of R1 to R8 independently represents a hydrogen, alkyl, cycloalkyl, aryl, or aralkyl group that may be substituted with a group selected from OH, Cl, Br, F, I, phenyl, NH2, CN, NO2, COOR9, CHO, COR9, or OR9, at least one of R5 to R8 is a fatty alkyl chain, and one or more of R5 to R8 can be a (poly)oxyalkylene group wherein the alkylene is a C1 to C4 alkylene and the total number of oxyalkylene units can be from 1 to 50 oxyalkylene units, and at least one of R1 to R8 is a C1 to C4 alkyl chain, R9 is an alkyl or cycloalkyl group, X- is an anion having an N-acyl sulphonylimide anion (—CO—N−—SO2—) functionality, Y− is an anion compatible with the N+R5R6R7R8 ammonium cation, such as a halogenide anion, a carboxylate anion, a sulphate (both organic and inorganic sulphate), sulphonate, carbonate, nitrate, nitrite, thiocyanate, hydroxide, or sulphonylimide anion.
摘要翻译：本发明涉及一种在基板上电镀或电解金属的方法，其中使用选自N + R1R2R3R4X-或N + R5R6R7R8Y-的离子液体作为电解质，并且使用添加到离子液体中的金属盐由于金属源或金属阳极用作金属源，其中R 1至R 8中的任一个独立地表示可以被选自OH，Cl，Br的基团取代的氢，烷基，环烷基，芳基或芳烷基，F，I，苯基，NH2，CN，NO2，COOR9，CHO，COR9或OR9，R5至R8中的至少一个为脂肪烷基链，R5至R8中的一个或多个可为（聚）氧化烯基团，其中亚烷基是C1-C4亚烷基，氧化烯单元的总数可以是1至50个氧化烯单元，并且R 1至R 8中的至少一个是C 1至C 4烷基链，R 9是烷基或环烷基， X-是具有N-酰基磺酰亚胺阴离子（-CO-N-SO 2 - ）官能团的阴离子，Y-是与N + R5R相容的阴离子 6R7R8铵阳离子，如卤化物阴离子，羧酸根阴离子，硫酸盐（有机和无机硫酸盐），磺酸盐，碳酸盐，硝酸盐，亚硝酸盐，硫氰酸盐，氢氧化物或磺酰亚胺阴离子。

9. 发明申请

US20090178972A1 Use of an Adsorbent for the Removal of Liquid, Gaseous and/or Dissolved Constituents From a Process Stream 有权
标题翻译：使用吸附剂从工艺流中去除液体，气态和/或溶解的成分
公开(公告)号：US20090178972A1
公开(公告)日：2009-07-16
申请号：US12280918
申请日：2007-03-05
申请人： Dirk Thomas Meijer , Cornelis Johannes Govardus Van Strien
发明人： Dirk Thomas Meijer , Cornelis Johannes Govardus Van Strien
IPC分类号： C02F9/00 , C02F1/26 , C02F1/28 , B01D11/04 , B01D15/00
CPC分类号： B01D11/04 , B01D15/00 , B01J20/18 , B01J20/20 , B01J20/26 , B01J20/261 , B01J20/267 , B01J20/28052 , B01J20/28078 , B01J20/28097 , C02F1/26 , C02F1/28 , C02F1/281 , C02F1/283 , C02F1/285 , C02F1/288 , C02F9/00
摘要： A method for removing liquid, gaseous and/or dissolved constituents from an aqueous stream includes contacting the aqueous stream with a porous material and then contacting the aqueous stream with an adsorbent material. The porous material includes pores having an average diameter of approximately 0.01 μm to approximately 50 μm and an extraction liquid immobilized within at least a portion of the pores.
摘要翻译：从水流中除去液体，气态和/或溶解成分的方法包括使含水物流与多孔材料接触，然后使含水物流与吸附材料接触。多孔材料包括平均直径为约0.01μm至约50μm的孔和固定在至少一部分孔内的萃取液。

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