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1. 发明授权

US5599510A Catalytic wall reactors and use of catalytic wall reactors for methane coupling and hydrocarbon cracking reactions 失效
标题翻译：催化壁反应器和催化壁反应器用于甲烷偶联和烃裂解反应
公开(公告)号：US5599510A
公开(公告)日：1997-02-04
申请号：US447434
申请日：1995-05-23
申请人： Mark P. Kaminsky , George A. Huff, Jr. , Narasimhan Calamur , Michael J. Spangler
发明人： Mark P. Kaminsky , George A. Huff, Jr. , Narasimhan Calamur , Michael J. Spangler
IPC分类号： B01J8/00 , B01J15/00 , B01J19/24 , B01J23/10 , B01J23/14 , B01J35/04 , C07C2/84 , C07C4/04 , C07C4/06 , C07C5/32 , C07C5/48 , C10G57/00 , C07C2/00
CPC分类号： C10G57/00 , B01J15/005 , B01J19/2475 , B01J23/10 , B01J23/14 , B01J35/04 , B01J8/009 , C07C2/84 , C07C4/04 , C07C4/06 , C07C5/321 , C07C5/48 , B01J2219/00063 , B01J2219/00117 , B01J2219/00126 , B01J2219/00155 , C07C2521/02 , C07C2521/06 , C07C2523/02 , C07C2523/08 , C07C2523/10 , C07C2523/14 , Y10S585/91 , Y10S585/911 , Y10S585/943
摘要： Dual-flow chemical reactor cores containing catalytic heat-transfer walls comprising both a gas-impervious material and a suitable catalyst which allows oxidative coupling of methane into higher hydrocarbons, dual-flow reactors having these catalytic heat-transfer walls to control and facilitate simultaneously coupling of methane and cracking of hydrocarbon compounds in separate gas streams, and chemical processes which combine coupling of methane and cracking of hydrocarbon compounds to make olefins in a dual-flow reactor having catalytic heat-transfer walls.
摘要翻译：包含催化传热壁的双流化学反应堆核心，其包含不透气材料和允许甲烷氧化成高级烃的合适催化剂，具有这些催化传热壁的双流反应器控制并促进同时耦合的甲烷和烃化合物在分离的气流中的裂解，以及将甲烷的偶联和烃化合物的裂化结合在具有催化传热壁的双流反应器中制备烯烃的化学方法。

2. 发明授权

US5959156A Preparation of polyoxymethylene dimethyl ethers by catalytic conversion of dimethyl ether with formaldehyde formed by oxy-dehydrogenation of dimethyl ether 有权
标题翻译：通过二甲醚的氧化脱氢形成的二甲醚与甲醛的催化转化制备聚甲醛二甲醚
公开(公告)号：US5959156A
公开(公告)日：1999-09-28
申请号：US190359
申请日：1998-11-12
申请人： Gary P. Hagen , Michael J. Spangler
发明人： Gary P. Hagen , Michael J. Spangler
IPC分类号： C07C41/56 , C07C43/30 , C10L1/02 , C07C43/11
CPC分类号： C10L1/026 , C07C41/56 , C07C43/30 , Y02P20/127
摘要： A particularly useful process which includes the steps of providing a source of formaldehyde formed by conversion of dimethyl ether in the presence of a catalyst comprising silver as an essential catalyst component; and contacting the source of formaldehyde and a predominately dimethyl ether feedstream with a heterogeneous, condensation promoting catalyst capable of hydrating dimethyl ether under conditions of reaction sufficient to form an effluent comprising water, methanol, formaldehyde, dimethyl ether, and polyoxymethylene dimethyl ethers is disclosed. Unreacted dimethyl ether is recovered from the effluent and recycled to the formation of polyoxymethylene dimethyl ethers. The resulting dimethyl ether-free liquid mixture is heated in the presence of an acidic catalyst to convert at least the methanol and formaldehyde present to polyoxymethylene dimethyl ethers. Advantageously, methylal and higher polyoxymethylene dimethyl ethers are formed and separated in a catalytic distillation column. By including in the column an anion exchange resin, an essentially acid-free product is obtained which can be used directly as a blending component, or fractionated, as by further distillation, to provide more suitable components for blending into diesel fuel.
摘要翻译：一种特别有用的方法，其包括以下步骤：在包含银作为必需催化剂组分的催化剂存在下，通过转化二甲醚形成甲醛源; 并且公开了使甲醛源和主要是二甲醚进料流与能够在足以形成包含水，甲醇，甲醛，二甲醚和聚甲醛二甲醚的流出物的反应条件下使二甲醚水合的异相缩合促进催化剂。从流出物中回收未反应的二甲醚，再循环至形成聚甲醛二甲醚。将所得的无二甲醚液体混合物在酸性催化剂存在下加热至少将甲醇和甲醛转化为聚甲醛二甲醚。有利地，甲缩醛和更高级的聚甲醛二甲醚在催化蒸馏塔中形成并分离。通过在柱中包含阴离子交换树脂，获得基本上不含酸的产物，其可以直接用作共混组分，或通过进一步蒸馏分离，以提供更合适的用于混合到柴油中的组分。

3. 发明授权

US5053578A Lower alkane conversion 失效
标题翻译：降低烷烃转化率
公开(公告)号：US5053578A
公开(公告)日：1991-10-01
申请号：US477318
申请日：1990-02-08
申请人： Glenn O. Michaels , Michael J. Spangler
发明人： Glenn O. Michaels , Michael J. Spangler
IPC分类号： B01J23/04 , B01J23/06 , B01J23/14 , B01J37/03 , C07C2/84
CPC分类号： B01J37/03 , B01J23/04 , B01J23/06 , B01J23/14 , C07C2/84 , C07C2521/04 , C07C2521/10 , C07C2523/02 , Y10S585/943
摘要： A method for converting a feedstock alkane containing from 1 to 3 carbon atoms to a higher molecular weight hydrocarbon comprising contacting a feedstock with an oxygen-containing gas in the presence of a catalytic composition is disclosed. The catalytic composition includes a Group IA metal, a Group IIA metal and a third component, the precursor of which is a sol such as an aqueous suspension of a metal such as aluminum, silicon, titanium, zinc, zirconium, cadmium or tin with which the other components of the composition are thoroughly dispersed.
摘要翻译：公开了一种将含有1至3个碳原子的原料烷烃转化为较高分子量烃的方法，包括在催化组合物存在下使原料与含氧气体接触。催化剂组合物包括IA族金属，IIA族金属和第三组分，其前体是诸如铝，硅，钛，锌，锆，镉或锡的金属的水性悬浮液的溶胶，其中组合物的其它组分被彻底分散。

4. 发明授权

US4814539A Conversion of a lower alkane 失效
标题翻译：低级烷烃的转化
公开(公告)号：US4814539A
公开(公告)日：1989-03-21
申请号：US706731
申请日：1985-02-28
申请人： James L. Jezl , Glenn O. Michaels , Michael J. Spangler , Mark L. Winzenburg
发明人： James L. Jezl , Glenn O. Michaels , Michael J. Spangler , Mark L. Winzenburg
IPC分类号： C07C2/84 , C07C2/02
CPC分类号： C07C2/84 , C07C2521/08 , C07C2523/06 , C07C2523/08 , C07C2523/14 , C07C2523/18 , C07C2523/22 , C07C2523/34
摘要： The catalyzed oxidative coupling of a lower molecular weight alkane to more valuable, higher molecular weight hydrocarbons and oxidative coupling catalysts for use therein are disclosed.
摘要翻译：公开了将低分子量烷烃催化氧化偶联到更有价值的较高分子量烃和用于其中的氧化偶联催化剂。

5. 发明授权

US06437195B1 Preparation of polyoxymethylene dimethyl ethers by acid-activated catalytic conversion of methanol with formaldehyde formed by dehydrogenation of methanol 有权
公开(公告)号：US06437195B1
公开(公告)日：2002-08-20
申请号：US09903224
申请日：2001-07-11
申请人： Gary P. Hagen , Michael J. Spangler
发明人： Gary P. Hagen , Michael J. Spangler
IPC分类号： C07C4109
摘要： A particularly useful process which includes the steps of providing a feedstream comprising methanol, a soluble condensation promoting component capable of activating a heterogeneous acidic catalyst and a source of formaldehyde formed by conversion of methanol in the presence of a catalyst comprising copper and zinc, and heating this feedstream with the heterogeneous acidic catalyst in a catalytic distillation column to convert methanol and formaldehyde present to methylal and higher polyoxymethylene dimethyl ethers and to separate the methylal from the higher polyoxymethylene dimethyl ethers is disclosed. Advantageously, methylal and higher polyoxymethylene dimethyl ethers are formed and separated in a catalytic distillation column. By including within the column a section containing an anion exchange resin, an essentially acid-free product is obtained. Products can be used directly as a blending component, or fractionated, as by further distillation, to provide more suitable components for blending into fuel.

6. 发明授权

US6160186A Preparation of polyoxymethylene dimethyl ethers by catalytic conversion of dimethyl ether with formaldehyde formed by dehydrogenation of dimethyl ether 有权
标题翻译：通过二甲醚与二甲醚脱氢形成的甲醛的催化转化制备聚甲醛二甲醚
公开(公告)号：US6160186A
公开(公告)日：2000-12-12
申请号：US191399
申请日：1998-11-12
申请人： Gary P. Hagen , Michael J. Spangler
发明人： Gary P. Hagen , Michael J. Spangler
IPC分类号： C07C41/56 , C07C43/11
CPC分类号： C07C41/56 , Y02P20/127 , C07C43/30
摘要： A particularly useful process which includes the steps of providing a source of formaldehyde formed by conversion of dimethyl ether in the presence of a catalyst comprising copper and zinc; and contacting the source of formaldehyde and a predominately dimethyl ether feedstream with a heterogeneous, condensation promoting catalyst capable of hydrating dimethyl ether under conditions of reaction sufficient to form an effluent comprising water, methanol, formaldehyde, dimethyl ether, and polyoxymethylene dimethyl ethers is disclosed. Unreacted dimethyl ether is recovered from the effluent and recycled to the formation of polyoxymethylene dimethyl ethers. The resulting dimethyl ether-free liquid mixture is heated in the presence of an acidic catalyst to convert at least the methanol and formaldehyde present to polyoxymethylene dimethyl ethers. Advantageously, methylal and higher polyoxymethylene dimethyl ethers are formed and separated in a catalytic distillation column. By including in the column an anion exchange resin, an essentially acid-free product is obtained which can be used directly as a blending component, or fractionated, as by further distillation, to provide more suitable components for blending into diesel fuel.
摘要翻译：一种特别有用的方法，其包括在包含铜和锌的催化剂存在下提供通过二甲醚转化形成的甲醛源的步骤; 并且公开了使甲醛源和主要是二甲醚进料流与能够在足以形成包含水，甲醇，甲醛，二甲醚和聚甲醛二甲醚的流出物的反应条件下使二甲醚水合的异相缩合促进催化剂。从流出物中回收未反应的二甲醚，再循环至形成聚甲醛二甲醚。将所得的无二甲醚液体混合物在酸性催化剂存在下加热至少将甲醇和甲醛转化为聚甲醛二甲醚。有利地，甲缩醛和更高级的聚甲醛二甲醚在催化蒸馏塔中形成并分离。通过在柱中包含阴离子交换树脂，获得基本上不含酸的产品，其可以直接用作共混组分，或通过进一步蒸馏分离，以提供更合适的用于混合到柴油中的组分。

7. 发明授权

US4968655A Catalysts for conversion of a lower alkane 失效
标题翻译：用于转化低级烷烃的催化剂
公开(公告)号：US4968655A
公开(公告)日：1990-11-06
申请号：US314765
申请日：1987-02-23
申请人： James L. Jezl , Glenn O. Michaels , Michael J. Spangler , Mark L Winzenburg
发明人： James L. Jezl , Glenn O. Michaels , Michael J. Spangler , Mark L Winzenburg
IPC分类号： C07C2/84 , B01J21/08 , B01J23/14
CPC分类号： C07C2/84 , C07C2521/08 , C07C2523/06 , C07C2523/08 , C07C2523/14 , C07C2523/18 , C07C2523/22 , C07C2523/34
摘要： Catalysts containing a reducible compound on a silica-containing support are provided for the conversion of a lower molecular weight alkane to more valuable, higher molecular weight hydrocarbons.
摘要翻译：提供含有二氧化硅载体上的可还原化合物的催化剂用于将较低分子量的烷烃转化为更有价值的更高分子量的烃。

8. 发明授权

US4754093A Conversion of a lower alkane 失效
标题翻译：低级烷烃的转化
公开(公告)号：US4754093A
公开(公告)日：1988-06-28
申请号：US706660
申请日：1985-02-28
申请人： James L. Jezl , Glenn O. Michaels , Michael J. Spangler
发明人： James L. Jezl , Glenn O. Michaels , Michael J. Spangler
IPC分类号： C07C2/84 , C07C2/00
CPC分类号： C07C2/84 , Y10S585/943
摘要： The catalyzed oxidative coupling of a lower molecular weight alkane to move valuable, higher molecular weight hydrocarbons is disclosed.
摘要翻译：公开了低分子量烷烃催化的氧化偶联以移动有价值的较高分子量烃。

9. 发明授权

US06292076B1 Circuit interrupter with improved DIN rail mounting adaptor 有权
标题翻译：具有改进的DIN导轨安装适配器的断路器
公开(公告)号：US06292076B1
公开(公告)日：2001-09-18
申请号：US09385611
申请日：1999-08-30
申请人： Dean B. DeGrazia , Erik R. Bogdon , Michael J. Spangler , Gary R. Funk , Roger W. Helms , David C. Turner
发明人： Dean B. DeGrazia , Erik R. Bogdon , Michael J. Spangler , Gary R. Funk , Roger W. Helms , David C. Turner
IPC分类号： H01H902
CPC分类号： H02B1/052 , H02B1/0523
摘要： A DIN rail adapter for a circuit interrupter including a backplate having two guide members and two substantially planar stabilizing tab. The backplate further includes a first spring attachment region. A slider is slideably disposed between the guide members and the stabilizing tabs, and includes a second spring attachment region. A spring is disposed between the first and second spring attachment regions for biasing the slider in a first direction.
摘要翻译：一种用于断路器的DIN导轨适配器，其包括具有两个导向构件和两个基本上平面的稳定翼片的背板。背板还包括第一弹簧附接区域。滑动件可滑动地设置在引导构件和稳定翼片之间，并且包括第二弹簧附接区域。弹簧设置在第一和第二弹簧附接区域之间，用于沿第一方向偏置滑块。

10. 发明授权

US5478370A Method for producing synthesis gas 失效
标题翻译：合成气的制造方法
公开(公告)号：US5478370A
公开(公告)日：1995-12-26
申请号：US269699
申请日：1994-07-01
申请人： Michael J. Spangler
发明人： Michael J. Spangler
IPC分类号： C01B3/48 , C01B3/16 , C01B3/38 , C01B3/26
CPC分类号： C01B3/384 , C01B2203/0233 , C01B2203/0238 , C01B2203/0415 , C01B2203/0475 , C01B2203/06 , C01B2203/061 , C01B2203/062 , C01B2203/0838 , C01B2203/0894 , C01B2203/1011 , C01B2203/1052 , C01B2203/1064 , C01B2203/1241
摘要： The invention provides an improved method for producing synthesis gas from lower alkanes which utilizes molten baths as reactors. A molten metal oxide bath delivers oxygen to a feed stream containing lower alkanes and enhances oxidation of the lower alkanes to produce carbon dioxide and a molten elemental metal. In a molten metal bath, the metal is regenerated to metal oxide by contact with a regenerant such as air. Heat evolved in the molten baths is transferred to an endothermic reactor where a portion of the carbon dioxide is converted to a mixture of carbon oxides and hydrogen.
摘要翻译：本发明提供了一种利用熔池作为反应器从低级烷烃生产合成气的改进方法。熔融金属氧化物浴将氧气输送到含有低级烷烃的进料流，并增强低级烷烃的氧化以产生二氧化碳和熔融元素金属。在熔融金属浴中，金属通过与再生剂例如空气接触而再生成金属氧化物。在熔融浴中放出的热量转移到吸热反应器中，其中一部分二氧化碳转化为碳氧化物和氢气的混合物。

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