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1. 发明授权

US08754169B2 Method of preparing rubber comprising polymeric compositions and isoprene comprising interpolymers 失效
标题翻译：制备包含聚合物组合物和包含互聚物的异戊二烯的橡胶的方法
公开(公告)号：US08754169B2
公开(公告)日：2014-06-17
申请号：US13616809
申请日：2012-09-14
申请人： Mark N. Dedecker , James E. Hall , Daniel F. Graves
发明人： Mark N. Dedecker , James E. Hall , Daniel F. Graves
IPC分类号： C08F287/00 , C08L55/02 , C08L9/06
CPC分类号： C08F287/00
摘要： A method for forming a rubber-modified polymeric composition includes polymerizing vinyl aromatic monomer within a mixture including the vinyl aromatic monomer and an interpolymer having at least one block of polyisoprene, at lest one block of polystyrene, and at lest one block of polybutadiene to thereby form the rubber-modified polymeric composition, where the interpolymer includes an internal block of polyisoprene.
摘要翻译：形成橡胶改性聚合物组合物的方法包括在包含乙烯基芳族单体和互聚物的混合物中聚合乙烯基芳族单体，所述互聚物具有至少一个聚异戊二烯嵌段，至少一个聚苯乙烯嵌段，至少一个聚丁二烯嵌段形成橡胶改性的聚合物组合物，其中互聚物包括聚异戊二烯的内部嵌段。

2. 发明申请

US20130041105A1 METHOD OF PREPARING RUBBER COMPRISING POLYMERIC COMPOSITIONS AND ISOPRENE COMPRISING INTERPOLYMERS 失效
标题翻译：制备包含聚合物组合物的橡胶和包含嵌段共聚物的异丙酚的方法
公开(公告)号：US20130041105A1
公开(公告)日：2013-02-14
申请号：US13616809
申请日：2012-09-14
申请人： Mark N. DEDECKER , James E. Hall , Daniel F. Graves
发明人： Mark N. DEDECKER , James E. Hall , Daniel F. Graves
IPC分类号： C08L53/00 , C08L55/02
CPC分类号： C08F287/00
摘要： A process for preparing a rubber comprising polymeric composition, and the resulting compositions, and certain isoprene comprising interpolymers.
摘要翻译：一种制备包含聚合物组合物的橡胶的方法，以及所得组合物和包含互聚物的某些异戊二烯。

3. 发明申请

US20100113699A1 METHOD OF PREPARING RUBBER COMPRISING POLYMERIC COMPOSITIONS AND ISOPRENE COMPRISING INTERPOLYMERS 审中-公开
标题翻译：制备包含聚合物组合物的橡胶和包含嵌段共聚物的异丙酚的方法
公开(公告)号：US20100113699A1
公开(公告)日：2010-05-06
申请号：US12521616
申请日：2007-12-21
申请人： Mark N. Dedecker , James E. Hall , Daniel F. Graves
发明人： Mark N. Dedecker , James E. Hall , Daniel F. Graves
IPC分类号： C08L55/02 , C08L53/00 , C08L9/00
CPC分类号： C08F287/00
摘要： A process for preparing a rubber comprising polymeric composition, and the resulting compositions, and certain isoprene comprising interpolymers.
摘要翻译：一种制备包含聚合物组合物的橡胶的方法，以及所得组合物和包含互聚物的某些异戊二烯。

4. 发明授权

US09376508B2 Polymers and use thereof in preparation of high impact polymeric compositions 有权
标题翻译：聚合物及其在制备高冲击聚合物组合物中的用途
公开(公告)号：US09376508B2
公开(公告)日：2016-06-28
申请号：US13124230
申请日：2009-10-13
申请人： Zengquan Qin , Jason T. Poulton , Mark N. DeDecker , James E. Hall
发明人： Zengquan Qin , Jason T. Poulton , Mark N. DeDecker , James E. Hall
IPC分类号： C08F279/02 , C08F287/00 , C08L25/12 , C08C19/44 , C08F297/04 , C08F236/06
CPC分类号： C08C19/44 , C08F236/06 , C08F297/04 , C08F2438/00 , C08F230/08 , C08F216/1416 , C08F212/08
摘要： Terminally functionalized polymers that are living or pseudo-living polymers reacted with certain allyl glycidyl ethers, or certain allylhalosilanes or combinations thereof, and a process for preparing the terminally functionalized polymers. Rubber-modified polymeric compositions comprising the terminally functionalized polymers.
摘要翻译：作为活性或假活性聚合物的终端官能化聚合物与某些烯丙基缩水甘油醚或某些烯丙基卤硅烷或其组合反应，以及制备末端官能化聚合物的方法。包含末端官能化聚合物的橡胶改性聚合物组合物。

5. 发明申请

US20110263794A1 New Polymers And Use Thereof In Preparation Of High Impact Polymeric Compositions 有权
标题翻译：新型高分子聚合物及其制备方法
公开(公告)号：US20110263794A1
公开(公告)日：2011-10-27
申请号：US13124230
申请日：2009-10-13
申请人： Zengquan Qin , Jason T. Poulton , Mark N. DeDecker , James E. Hall
发明人： Zengquan Qin , Jason T. Poulton , Mark N. DeDecker , James E. Hall
IPC分类号： C08L25/12 , C08F287/00 , C08F279/02
CPC分类号： C08C19/44 , C08F236/06 , C08F297/04 , C08F2438/00 , C08F230/08 , C08F216/1416 , C08F212/08
摘要： Terminally functionalized polymers that are living or pseudo-living polymers reacted with certain allyl glycidyl ethers, or certain allylhalosilanes or combinations thereof, and a process for preparing the terminally functionalized polymers. Rubber-modified polymeric compositions comprising the terminally functionalized polymers.
摘要翻译：作为活性或假活性聚合物的终端官能化聚合物与某些烯丙基缩水甘油醚或某些烯丙基卤硅烷或其组合反应，以及制备末端官能化聚合物的方法。包含末端官能化聚合物的橡胶改性聚合物组合物。

6. 发明授权

US5089558A Thermoformable blends of multiblock polymer compositions with polystyrene 失效
标题翻译：多嵌段聚合物组合物与聚苯乙烯的可热成型共混物
公开(公告)号：US5089558A
公开(公告)日：1992-02-18
申请号：US646485
申请日：1991-01-28
申请人： James E. Hall , Daniel F. Graves
发明人： James E. Hall , Daniel F. Graves
IPC分类号： C08L25/02 , C08L53/02
CPC分类号： C08L25/02 , C08L53/02 , C08L2205/02
摘要： A polymer composition for use in making thermoformed products which comprises a blend of: (1) 20 to 75% by weight of a polyvinylaromatic resin, (2) 20 to 75% by weight of S.sub.1 -(B/S.sub.2).sub.n type block copolymer wherein S.sub.1 and S.sub.2 are vinylaromatic block polymers, B is a diene block polymer, (B/S.sub.2) represents a tapered or non-tapered block copolymer and the S.sub.1 block is 5 to 20% by weight of the block copolymer, (S.sub.1 +S.sub.2) is 65 to 95% by weight of the block copolymer, and the total block styrene content of the block copolymer ranges between 35 and 80% by weight, and (3) 0.5 to 10% by weight a diene-vinylaromatic block copolymer (B'-S') containing 10-60% by weight of the vinylaromatic polymer block.
摘要翻译：一种用于制造热成型产品的聚合物组合物，其包含以下混合物：（1）20至75重量％的聚乙烯基芳族树脂，（2）20至75重量％的S1-（B / S2）n型嵌段共聚物其中S1和S2是乙烯基芳族嵌段聚合物，B是二烯嵌段聚合物，（B / S2）表示锥形或非渐变嵌段共聚物，S1嵌段是嵌段共聚物的5〜20重量％（S1 + S2 ）为嵌段共聚物的65〜95重量％，嵌段共聚物的总嵌段苯乙烯含量为35〜80重量％，（3）0.5〜10重量％的二烯 - 乙烯基芳族嵌段共聚物（B '-S'），其含有10-60重量％的乙烯基芳族聚合物嵌段。

7. 发明授权

US06242536B1 Process for preparation of block copolymers in mixed alkane/cycloalkane solvents 失效
标题翻译：在混合烷烃/环烷烃溶剂中制备嵌段共聚物的方法
公开(公告)号：US06242536B1
公开(公告)日：2001-06-05
申请号：US08988925
申请日：1997-12-11
申请人： James E. Hall , Daniel F. Graves , Hideo Takeichi
发明人： James E. Hall , Daniel F. Graves , Hideo Takeichi
IPC分类号： C08F29300
CPC分类号： C08F297/04
摘要： The dispersibility of the initial polystyrene block in forming a S-B-S type of copolymer is improved by first preparing a small block of homopolydiene such as homopolybutadiene as a dispersing agent. Onto this small block of homopolybutadiene, the first block of polystyrene is formed and affixed and thereby made dispersible in a mixture of alkanes and 15 to 60% by weight of cycloalkanes, preferably hexane and cyclohexane. After the preparation of the dispersing agent and the first styrene block, the remaining monomer charges to the reactor are fed in aliphatic hydrocarbon diluents, preferably hexane or technical hexane, thereby greatly reducing the final percentage of cycloalkanes including cyclohexane in the reactor to less than 25% of total dispersing medium. The block copolymers produced according to the present process display a narrow molecular weight distribution and improved tensile strength over block copolymers produced in the absence of the additional cycloalkanes in the solvent system.
摘要翻译：初始聚苯乙烯嵌段在形成S-B-S型共聚物中的分散性通过首先制备均聚二烯如小聚丁二烯作为分散剂的小块来改善。在该小块均聚丁二烯上，形成第一块聚苯乙烯并固化，从而使其分散在烷烃和15至60重量％的环烷烃，优选己烷和环己烷的混合物中。在分散剂和第一苯乙烯嵌段的制备之后，向脂肪烃稀释剂（优选己烷或工业己烷）中将进料到反应器中的剩余单体进料进料，从而大大降低反应器中包括环己烷在内的环烷烃的最终百分比至小于25 总分散介质的百分比。根据本发明制备的嵌段共聚物在溶剂体系中不存在另外的环烷烃时产生的嵌段共聚物显示窄的分子量分布和改进的拉伸强度。

8. 发明授权

US5385994A 2,5-substituted tetrahydrofurans as anionic initiator modifiers 失效
标题翻译： 2,5-取代的四氢呋喃作为阴离子引发剂改性剂
公开(公告)号：US5385994A
公开(公告)日：1995-01-31
申请号：US139667
申请日：1993-10-22
申请人： Daniel F. Graves , James E. Hall , William J. Shuttleworth
发明人： Daniel F. Graves , James E. Hall , William J. Shuttleworth
IPC分类号： C07D307/06 , C08F4/42 , C08F4/48 , C08F12/04 , C08F297/04
CPC分类号： C08F297/04 , C08F12/04
摘要： A method for improving the initiation efficiency during the anionic polymerization of 15 to 100 percent weight of a vinyl aromatic hydrocarbon monomers and 0 to 85 percent by weight of a conjugated diene monomer by conducting the polymerization in the presence of a catalytically effective amount of: (a) an organolithium initiator and (b) a 2,5-substituted tetrahydrofuran modifier having the structural formula: ##STR1## wherein R.sub.1 and R.sub.1 ' are independently H or an alkyl group containing 1 to 4 carbon atoms and R.sub.2 and R.sub.2 ' are alkyl group containing 1 to 4 carbon atoms.
摘要翻译：通过在催化有效量的存在下进行聚合，提高阴离子聚合中的引发效率的方法：15-100重量％的乙烯基芳族烃单体和0至85重量％的共轭二烯单体， a）有机锂引发剂和（b）具有以下结构式的2,5-取代的四氢呋喃改性剂：其中R1和R1'独立地是H或含有1至4个碳原子的烷基，R2和R2'是烷基含有1至4个碳原子的基团。

9. 发明授权

US07897690B2 Rubber composition containing functionalized polymer nanoparticles 有权
标题翻译：含有官能化聚合物纳米粒子的橡胶组合物
公开(公告)号：US07897690B2
公开(公告)日：2011-03-01
申请号：US12504255
申请日：2009-07-16
申请人： Xiaorong Wang , James E. Hall , Georg G. A. Böhm , Chenchy Jeffrey Lin
发明人： Xiaorong Wang , James E. Hall , Georg G. A. Böhm , Chenchy Jeffrey Lin
IPC分类号： C08F279/00
CPC分类号： B82Y30/00 , C08F279/02 , C08F222/06
摘要： A polymer nanoparticle is provided. The nanoparticle includes an inner layer having alkenylbenzene monomer units. The nanoparticle further includes an outer layer having monomer units selected from conjugated dienes, alkylenes, alkenylbenzenes, and mixtures thereof. The nanoparticle has at least one functional group associated with the outer layer. Applications of use as additives for rubber, including the rubber compositions, are also provided.
摘要翻译：提供聚合物纳米颗粒。纳米颗粒包括具有烯基苯单体单元的内层。纳米颗粒还包括具有选自共轭二烯，亚烷基，链烯基苯及其混合物的单体单元的外层。纳米颗粒具有与外层相关联的至少一个官能团。还提供了用作橡胶添加剂的应用，包括橡胶组合物。

10. 发明授权

US07737218B2 Method for generating free radical capable polymers using tin or silicon halide compounds 失效
标题翻译：使用锡或卤化硅化合物生成可自由基聚合物的方法
公开(公告)号：US07737218B2
公开(公告)日：2010-06-15
申请号：US11618059
申请日：2006-12-29
申请人： James E. Hall , David F. Lawson
发明人： James E. Hall , David F. Lawson
IPC分类号： C08L83/00 , C08L51/08 , C08L51/00 , C08L61/04 , C08L53/00 , C08F293/00 , C08F36/00 , C08F8/18 , C08F8/00 , C08F2/38 , C08C19/44 , C08G63/48 , C08K5/00
CPC分类号： C08F8/42
摘要： Provided is a method comprising reacting the anionic living end of a polymer with a compound selected from the group consisting of tin halides and silicon halides to produced a polymer with a homolytically cleavable group containing a Sn—C bond or a Si—C bond. An engineered plastic may then be produced by adding the polymer containing a homolytically cleavable group containing a Sn—C bond or a Si—C bond to a solvent comprising at least one vinyl monomer; (b) optionally adding at least one additional inert solvent; (c) optionally adding additives selected from the group consisting of extender oils, modifiers, and antioxidants; and (d) initiating polymerization of the at least one vinyl monomer by the use of an initiator and/or heat, wherein a free radical is produced from the polymer containing a homolytically cleavable group containing a Sn—C bond or a Si—C bond.
摘要翻译：提供了一种方法，其包括使聚合物的阴离子活性端与选自卤化锡和卤化硅的化合物反应，以制备具有含Sn-C键或Si-C键的均聚裂解基团的聚合物。然后可以通过将含有含有Sn-C键或Si-C键的均聚裂解基团的聚合物加入到包含至少一种乙烯基单体的溶剂中来制备工程塑料; （b）任选地加入至少一种另外的惰性溶剂; （c）任选地添加选自由增量油，改性剂和抗氧化剂组成的组的添加剂; 和（d）通过使用引发剂和/或加热引发至少一种乙烯基单体的聚合，其中由含有Sn-C键或Si-C键的均聚裂解基团的聚合物产生自由基。

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