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1. 发明授权

US08586804B2 Synthesis of 1,1,3-trichloro-1-propene 有权
标题翻译：合成1,1,3-三氯-1-丙烯
公开(公告)号：US08586804B2
公开(公告)日：2013-11-19
申请号：US13278511
申请日：2011-10-21
申请人： Mario Joseph Nappa , Robert D. Lousenberg , Andrew Jackson
发明人： Mario Joseph Nappa , Robert D. Lousenberg , Andrew Jackson
IPC分类号： C07C17/25
CPC分类号： C07C17/25 , C07C21/04
摘要： Disclosed is a process for the dehydrochlorination of 1,1,1,3-tetrachloropropane comprising contacting 1,1,1,3,tetrachloropropane in the vapor phase in a reaction zone with a catalyst comprising iron, to produce a product mixture comprising 1,1,3-trichloro-1-propene; and recovering said 1,1,3-trichloro-1-propene from the product mixture produced. Also disclosed is a process for the dehydrochlorination of 1,1,1,3-tetrachloropropane comprising heating 1,1,1,3-tetrachloropropane in the liquid phase to produce a mixture comprising 1,1,3-trichloro-1-propene, cooling said mixture, separating hydrogen chloride from said mixture and recovering 1,1,3-trichloro-1-propene.
摘要翻译：公开了1,1,1,3-四氯丙烷的脱氯化氢的方法，包括使反应区中的气相中的1,1,1,3，四氯丙烷与包含铁的催化剂接触，以产生包含1， 1,3-三氯-1-丙烯; 并从所生产的产物混合物回收所述1,1,3-三氯-1-丙烯。还公开了1,1,1,3-四氯丙烷的脱氯化氢的方法，包括在液相中加热1,1,1,3-四氯丙烷以产生包含1,1,3-三氯-1-丙烯，冷却所述混合物，从所述混合物中分离出氯化氢并回收1,1,3-三氯-1-丙烯。

2. 发明申请

US20120172638A1 SYNTHESIS OF 1234YF BY SELECTIVE DEHYDROCHLORINATION OF 244BB 有权
标题翻译：通过244BB的选择性脱氢合成合成1234YF
公开(公告)号：US20120172638A1
公开(公告)日：2012-07-05
申请号：US13172987
申请日：2011-06-30
申请人： Mario Joseph Nappa , Robert D. Lousenberg , Andrew Jackson
发明人： Mario Joseph Nappa , Robert D. Lousenberg , Andrew Jackson
IPC分类号： C07C17/23 , C07C21/18
CPC分类号： C07C17/25 , B01J23/26 , B01J37/0036 , B01J37/038 , C07C21/18
摘要： Disclosed is a process for the manufacture of 2,3,3,3-tetrafluoropropene comprising: (a) contacting 1,1,1,2,tetrafluoro-2-chloropropane with a catalyst comprised of chromium (III) oxide, and at least 1% of an alkali metal, to produce a product mixture comprising 2,3,3,3-tetrafluoropropene; and (b) recovering said 2,3,3,3-tetrafluoropropene from the product mixture produced in step (a) above.
摘要翻译：公开了一种制备2,3,3,3-四氟丙烯的方法，其包括：（a）将1,1,1,2，四氟-2-氯丙烷与由氧化铬（III）组成的催化剂和至少 1％的碱金属，以制备包含2,3,3,3-四氟丙烯的产物混合物; 和（b）从上述步骤（a）中制备的产物混合物中回收所述2,3,3,3-四氟丙烯。

3. 发明授权

US08263817B2 Synthesis of 1234YF by selective dehydrochlorination of 244BB 有权
标题翻译：通过244BB的选择性脱氯化氢合成1234YF
公开(公告)号：US08263817B2
公开(公告)日：2012-09-11
申请号：US13172987
申请日：2011-06-30
申请人： Mario Joseph Nappa , Robert D. Lousenberg , Andrew Jackson
发明人： Mario Joseph Nappa , Robert D. Lousenberg , Andrew Jackson
IPC分类号： C07C17/25
CPC分类号： C07C17/25 , B01J23/26 , B01J37/0036 , B01J37/038 , C07C21/18
摘要： Disclosed is a process for the manufacture of 2,3,3,3-tetrafluoropropene comprising: (a) contacting 1,1,1,2,tetrafluoro-2-chloropropane with a catalyst comprised of chromium (III) oxide, and at least 1% of an alkali metal, to produce a product mixture comprising 2,3,3,3-tetrafluoropropene; and (b) recovering said 2,3,3,3-tetrafluoropropene from the product mixture produced in step (a) above.
摘要翻译：公开了一种制备2,3,3,3-四氟丙烯的方法，其包括：（a）将1,1,1,2，四氟-2-氯丙烷与由氧化铬（III）组成的催化剂和至少 1％的碱金属，以制备包含2,3,3,3-四氟丙烯的产物混合物; 和（b）从上述步骤（a）中制备的产物混合物中回收所述2,3,3,3-四氟丙烯。

4. 发明授权

US06730762B2 Linear copolymers of fluorocarbon-hydrocarbon monomers synthesized in carbon dioxide 失效
标题翻译：在二氧化碳中合成的碳氟烃单体的线性共聚物
公开(公告)号：US06730762B2
公开(公告)日：2004-05-04
申请号：US09773928
申请日：2001-02-02
申请人： Robert D. Lousenberg , Molly S. Shoichet
发明人： Robert D. Lousenberg , Molly S. Shoichet
IPC分类号： C08F11418
CPC分类号： C08F214/186 , C08F14/18 , Y02P20/544 , C08F2/04
摘要： Linear copolymers of fluorocarbon and hydrocarbon monomers. The present invention provides linear copolymers and terpolymers of fluorocarbon and hydrocarbon monomers, and particularly the invention provides a linear copolymers, of fluoromonomers, such as tetrafluoroethylene, chlorotrifluoroethylene, or vinylidene fluoride, with hydrocarbon monomers, such as vinyl acetate, acrylic acid ethyl acetate or tertiary butyl acrylate. The copolymers were synthesized by polymerization by a free radical mechanism in supercritical carbon dioxide and they are linear because of synthesis in carbon dioxide. The copolymer composition was controlled by the monomer feed concentration to have between 7 and 71 mol % TFE. Additionally, new and predominantly linear co- and terpolymers were prepared by hydrolysis and trans-esterification of the latter copolymers. Furthermore, neither surfactants nor dispersing agents are required to produce the linear copolymers, but may be used.
摘要翻译：碳氟化合物和烃单体的线性共聚物。本发明提供了碳氟化合物和烃单体的线型共聚物和三元共聚物，特别是本发明提供了氟单体如四氟乙烯，三氟氯乙烯或偏二氟乙烯的直链共聚物与烃单体如乙酸乙烯酯，丙烯酸乙酸乙酯或叔丁基丙烯酸酯。通过在超临界二氧化碳中的自由基机理聚合合成共聚物，由于在二氧化碳中合成，它们是线性的。共聚物组成由单体进料浓度控制，具有7至71mol％的TFE。另外，通过水解和后酯共聚制备新的和主要是线性的共聚物和三元共聚物。此外，不需要表面活性剂和分散剂来制造线性共聚物，而是可以使用。

5. 发明申请

US20100209600A1 NOVEL ALKYL PERFLUOROALKENE ETHERS 有权
标题翻译：新的阿尔茨海默病
公开(公告)号：US20100209600A1
公开(公告)日：2010-08-19
申请号：US12701802
申请日：2010-02-08
申请人： JOAN ELLEN BARTELT , Robert D. Lousenberg
发明人： JOAN ELLEN BARTELT , Robert D. Lousenberg
IPC分类号： B05D5/12 , C07C43/17 , C07C41/06 , B05D3/02 , B05D3/12 , C11D1/825 , C23G5/00
CPC分类号： C07C43/17 , C11D7/5018
摘要： Disclosed are compositions comprising a compound having the formula CF3(CF2)xCF═CFCF(OR)(CF2)yCF3, wherein R is CH3 or C2H5 or mixtures thereof, and wherein x and y are independently 0, 1, 2 or 3, and wherein x+y=1, 2 or 3. Also disclosed are unsaturated fluoroethers selected from the group consisting of CF3(CF2)xCF═CFCF(OR)(CF2)yCF3, CF3(CF2)xC(OR)═CFCF2(CF2)yCF3, CF3CF═CFCF(OR)(CF2)x(CF2)yCF3, CF3(CF2)xCF═C(OR)CF2(CF2)yCF3, and mixtures thereof, wherein R can be either CH3, C2H5 or mixtures thereof, and wherein x and y are independently 0, 1, 2 or 3, and wherein x+y=0, 1, 2 or 3. Also disclosed herein are novel methods of using a composition comprising at least one of the compounds described above as novel solvents, carrier fluids, dewatering agents, degreasing solvents or defluxing solvents.
摘要翻译：公开了包含式CF 3（CF 2）x CF = CFCF（OR）（CF 2）y CF 3的化合物，其中R是CH 3或C 2 H 5或其混合物的组合物，其中x和y独立地是0,1,2或3，还公开了选自CF 3（CF 2）xCF≡CFCF（OR）（CF 2）y CF 3，CF 3（CF 2）x C（OR）= CFCF 2（CF 2））的不饱和氟醚， y CF 3，CF 3 CF = CFCF（OR）（CF 2）x（CF 2）y CF 3，CF 3（CF 2）x CF = C（OR）CF 2（CF 2）y CF 3及其混合物，其中R可以是CH 3，C 2 H 5或其混合物，其中x和y独立地为0,1,2或3，并且其中x + y = 0,1,2或3.本文还公开了使用包含至少一种上述化合物作为新溶剂的组合物的新方法载体流体，脱水剂，脱脂溶剂或去油溶剂。

6. 发明授权

US08399713B2 Alkyl perfluoroalkene ethers 有权
标题翻译：烷基全氟烯烃醚
公开(公告)号：US08399713B2
公开(公告)日：2013-03-19
申请号：US12701802
申请日：2010-02-08
申请人： Joan Ellen Bartelt , Robert D. Lousenberg
发明人： Joan Ellen Bartelt , Robert D. Lousenberg
IPC分类号： C07C43/17 , C07C41/06 , B05D5/12 , C11D1/825 , C23G5/00
CPC分类号： C07C43/17 , C11D7/5018
摘要： Disclosed are compositions comprising a compound having the formula CF3(CF2)xCF═CFCF(OR)(CF2)yCF3, wherein R is CH3 or C2H5 or mixtures thereof, and wherein x and y are independently 0, 1, 2 or 3, and wherein x+y=1, 2 or 3. Also disclosed are unsaturated fluoroethers selected from the group consisting of CF3(CF2)xCF═CFCF(OR)(CF2)yCF3, CF3(CF2)xC(OR)═CFCF2(CF2)yCF3, CF3CF═CFCF(OR)(CF2)x(CF2)yCF3, CF3(CF2)xCF═C(OR)CF2(CF2)yCF3, and mixtures thereof, wherein R can be either CH3, C2H5 or mixtures thereof, and wherein x and y are independently 0, 1, 2 or 3, and wherein x+y=0, 1, 2 or 3. Also disclosed herein are novel methods of using a composition comprising at least one of the compounds described above as novel solvents, carrier fluids, dewatering agents, degreasing solvents or defluxing solvents.
摘要翻译：公开了包含式CF 3（CF 2）x CF = CFCF（OR）（CF 2）y CF 3的化合物，其中R是CH 3或C 2 H 5或其混合物的组合物，其中x和y独立地是0,1,2或3，还公开了选自CF 3（CF 2）xCF≡CFCF（OR）（CF 2）y CF 3，CF 3（CF 2）x C（OR）= CFCF 2（CF 2））的不饱和氟醚， y CF 3，CF 3 CF = CFCF（OR）（CF 2）x（CF 2）y CF 3，CF 3（CF 2）x CF = C（OR）CF 2（CF 2）y CF 3及其混合物，其中R可以是CH 3，C 2 H 5或其混合物，其中x和y独立地为0,1,2或3，并且其中x + y = 0,1,2或3.本文还公开了使用包含至少一种上述化合物作为新溶剂的组合物的新方法载体流体，脱水剂，脱脂溶剂或去油溶剂。

7. 发明授权

US5684192A Substituted trifluorostyrene monomeric compositions 失效
标题翻译：取代的三氟苯乙烯单体组合物
公开(公告)号：US5684192A
公开(公告)日：1997-11-04
申请号：US575349
申请日：1995-12-20
申请人： Charles Stone , Alfred E. Steck , Robert D. Lousenberg
发明人： Charles Stone , Alfred E. Steck , Robert D. Lousenberg
IPC分类号： B01D61/42 , B01D69/02 , B01D69/12 , B01D71/28 , B01D71/32 , C07C309/86 , C08F8/00 , C08F12/30 , C08F14/18 , C08F114/18 , C08F212/14 , C08F214/18 , C08J5/22 , C08L27/12 , G01N27/40 , G01N27/407 , H01M2/16 , H01M8/02 , H01M8/10 , C07C317/14
CPC分类号： G01N27/40 , B01D69/02 , B01D69/12 , B01D71/28 , B01D71/32 , C07C309/86 , C08F12/30 , C08F14/185 , C08F212/14 , C08F8/12 , C08J5/225 , G01N27/4073 , G01N27/4074 , H01M2/1653 , H01M8/1023 , H01M8/1039 , C08F2800/10 , C08F2800/20 , C08J2327/12
摘要： Sulfonyl fluoride substituted .alpha.,.beta.,.beta.-trifluorostyrene monomers are disclosed. The monomers are incorporated into polymeric compositions which are conveniently hydrolyzed to produce polymeric compositions which include ion-exchange moieties. The resulting compositions which include ion-exchange moieties are particularly suitable for use as solid polymer electrolytes in electrochemical applications, such as, for example, electrochemical fuel cells.
摘要翻译：公开了磺酰氟取代的α，β，β-三氟苯乙烯单体。将单体引入聚合物组合物中，其中方便地水解以产生包括离子交换部分的聚合物组合物。包括离子交换部分的所得组合物特别适合用作电化学应用中的固体聚合物电解质，例如电化学燃料电池。

8. 发明授权

US08486295B2 Alkyl perfluoroalkene ethers and uses thereof 有权
标题翻译：烷基全氟烯烃醚及其用途
公开(公告)号：US08486295B2
公开(公告)日：2013-07-16
申请号：US13170646
申请日：2011-06-28
申请人： Joan Ellen Bartelt , Robert D. Lousenberg
发明人： Joan Ellen Bartelt , Robert D. Lousenberg
IPC分类号： C09K5/04
CPC分类号： C09K5/10
摘要： Disclosed are methods of transferring heat comprising providing a device, using a heat-transfer fluid to transfer heat to or from the device, wherein the heat-transfer fluid compositions comprise at least one unsaturated fluoroether having the formula CF3(CF2)xCF═CFCF(OR)(CF2)yCF3, CF3(CF2)xC(OR)═CFCF2(CF2)yCF3, CF3CF═CFCF(OR)(CF2)x(CF2)yCF3, CF3(CF2)xCF═C(OR)CF2(CF2)yCF3, or mixtures thereof, wherein R can be either CH3, C2H5 or mixtures thereof, and wherein x and y are independently 0, 1, 2 or 3, and wherein x+y=0, 1, 2 or 3.
摘要翻译：公开了传递热量的方法，包括提供装置，使用传热流体将热量传递到装置或从设备传递热量，其中传热流体组合物包含至少一种具有式CF 3（CF 2）x CF = CFCF的不饱和氟醚（CF 2）x CF = C（OR）CF 2（CF 2）x CF（OR）= CFCF 2（CF 2）y CF 3，CF 3 CF = CFCF（OR））yCF 3或其混合物，其中R可以是CH 3，C 2 H 5或其混合物，并且其中x和y独立地为0,1,2或3，并且其中x + y = 0,1,2或3。

9. 发明申请

US20110282104A1 NOVEL ALKYL PERFLUOROALKENE ETHERS 审中-公开
标题翻译：新的阿尔茨海默病
公开(公告)号：US20110282104A1
公开(公告)日：2011-11-17
申请号：US13187637
申请日：2011-07-21
申请人： JOAN ELLEN BARTELT , Robert D. Lousenberg
发明人： JOAN ELLEN BARTELT , Robert D. Lousenberg
IPC分类号： C07C41/06
CPC分类号： C07C43/17 , C11D7/5018
摘要： Disclosed are compositions comprising a compound having the formula CF3(CF2)xCF═CFCF(OR)(CF2)yCF3, wherein R is CH3 or C2H5or mixtures thereof, and wherein x and y are independently 0, 1, 2 or 3, and wherein x+y=1, 2 or 3. Also disclosed are unsaturated fluoroethers selected from the group consisting of CF3(CF2)xCF═CFCF(OR)(CF2)yCF3, CF3(CF2)xC(OR)═CFCF2(CF2)yCF3, CF3CF═CFCF(OR)(CF2)x(CF2)yCF3, CF3(CF2)xCF═C(OR)CF2(CF2)yCF3, and mixtures thereof, wherein R can be either CH3, C2H5 or mixtures thereof, and wherein x and y are independently 0, 1, 2 or 3, and wherein x+y=0, 1, 2 or 3. Also disclosed herein are novel methods of making a composition comprising at least one of the compounds described.
摘要翻译：公开了包含式CF 3（CF 2）x CF = CFCF（OR）（CF 2）y CF 3的化合物，其中R为CH 3或C 2 H 5或其混合物的组合物，其中x和y独立地为0,1,2或3，还公开了选自CF 3（CF 2）xCF≡CFCF（OR）（CF 2）y CF 3，CF 3（CF 2）x C（OR）= CFCF 2（CF 2）y CF 3）的不饱和氟代醚，CF 3CF≡CFCF（OR）（CF 2）x（CF 2）y CF 3，CF 3（CF 2）x CF = C（OR）CF 2（CF 2）y CF 3及其混合物，其中R可以是CH 3，C 2 H 5或其混合物， x和y独立地为0,1,2或3，并且其中x + y = 0,1,2或3.本文还公开了制备包含至少一种所述化合物的组合物的新方法。

10. 发明授权

US08058319B2 Process to prepare fluoropolymer dispersions and membranes 失效
标题翻译：氟聚合物分散体和膜的制备方法
公开(公告)号：US08058319B2
公开(公告)日：2011-11-15
申请号：US11750391
申请日：2007-05-18
申请人： Robert D. Lousenberg
发明人： Robert D. Lousenberg
IPC分类号： C08J5/20
CPC分类号： C08J5/2237 , C08J3/091 , C08J2327/18 , H01M8/1023 , H01M8/1039 , H01M8/1058 , H01M8/1072 , H01M2300/0082 , Y02P70/56
摘要： Described is a process to prepare fluoropolymer organic-liquid dispersions containing a homogeneous mixture of reacted and unreacted sulfonyl halide groups. The dispersions are useful in the preparation of crosslinked membranes.
摘要翻译：描述了制备含有反应和未反应的磺酰卤基团的均匀混合物的含氟聚合物有机 - 液体分散体的方法。分散体可用于制备交联膜。

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