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1. 发明授权

US4124569A Process for the preparation of polyisocyanates containing urethane and biuret groups 失效
标题翻译：制备含氨基甲酸酯和缩二脲基团的多异氰酸酯的方法
公开(公告)号：US4124569A
公开(公告)日：1978-11-07
申请号：US832318
申请日：1977-09-12
申请人： Manfred Bock , Josef Pedain , Walter Uerdingen , Manfred Schonfelder
发明人： Manfred Bock , Josef Pedain , Walter Uerdingen , Manfred Schonfelder
IPC分类号： C08G18/00 , C07C67/00 , C07C239/00 , C07C269/02 , C07C273/18 , C07C275/48 , C07C275/62 , C08G18/78 , C08G18/80 , C08G18/79
CPC分类号： C07C273/1863 , C07C273/1872 , C08G18/7831 , C08G18/8041 , C08G18/8058
摘要： The present invention is concerned with a process for producing biuret polyisocyanates and the polyisocyanates so produced. These isocyanates are produced by the reaction of at least about a four fold molar excess of a diisocyanate having aliphatically bound isocyanate groups with amino alcohols having a particular structure at a temperature between about 90 and 200.degree. C. The amino alcohols contain at least three carbon atoms, have their hydroxyl and amino groups separated by at least two carbon atoms, and may contain urea, urethane, ether or amino bonds. The present invention is also concerned with a process for producing two component and one component moisture curing lacquers using the biuret polyisocyanates of the present invention and the lacquers so produced.
摘要翻译：本发明涉及制备缩二脲多异氰酸酯的方法和如此制备的多异氰酸酯。这些异氰酸酯是通过至少约四倍摩尔过量的具有脂肪族结合的异氰酸酯基团的二异氰酸酯与具有特定结构的氨基醇在约90-200℃之间的温度下进行的反应来制备的。氨基醇含有至少三个碳原子，其羟基和氨基被至少两个碳原子分开，并且可以含有脲，氨基甲酸酯，醚或氨基键。本发明还涉及使用本发明的缩二脲多异氰酸酯和如此制备的漆制备两组分和一种组分的湿固化漆的方法。

2. 发明授权

US4113705A Triisocyanates useful for the production of polyurethane resins 失效
标题翻译：可用于生产聚氨酯树脂的三异氰酸酯
公开(公告)号：US4113705A
公开(公告)日：1978-09-12
申请号：US778631
申请日：1977-03-17
申请人： Manfred Bock , Josef Pedain , Walter Uerdingen
发明人： Manfred Bock , Josef Pedain , Walter Uerdingen
IPC分类号： C08G18/00 , C07C67/00 , C07C241/00 , C07C265/00 , C07C265/14 , C08G18/73 , C08G18/75 , C09D175/00 , C07C119/045
CPC分类号： C08G18/757
摘要： This invention relates to new liquid cycloaliphatic triisocyanates and to their use as isocyanate components for the production of polyurethane resins by the known isocyanate polyaddition process.
摘要翻译：本发明涉及新的液体脂环族三异氰酸酯及其作为通过已知的异氰酸酯加聚方法生产聚氨酯树脂的异氰酸酯组分的用途。

3. 发明授权

US4045462A Bicyclic triisocyanates 失效
标题翻译：双环三异氰酸酯
公开(公告)号：US4045462A
公开(公告)日：1977-08-30
申请号：US674014
申请日：1976-04-05
申请人： Manfred Bock , Walter Uerdingen , Josef Pedain
发明人： Manfred Bock , Walter Uerdingen , Josef Pedain
IPC分类号： C08G18/00 , C07C67/00 , C07C241/00 , C07C255/45 , C07C263/10 , C07C265/00 , C07C265/08 , C07C265/10 , C07C265/14 , C08G18/72 , C08G18/73 , C08G18/75 , C08L75/04 , C09D175/00 , C07C119/045
CPC分类号： C07C265/00 , C08G18/758
摘要： The instant invention is directed to new liquid bicycloaliphatic triisocyanates and to the use thereof as the isocyanate component in the production of polyurethane plastics by the known isocyanate-polyaddition process. The new triisocyanates are particularly suitable for use as the isocyanate component in low-solvent, light-stable two-component polyurethane lacquers.
摘要翻译：本发明涉及新的液体双环脂族三异氰酸酯，以及通过已知的异氰酸酯加聚方法在聚氨酯塑料生产中作为异氰酸酯组分的用途。新的三异氰酸酯特别适合用作低溶剂，轻质双组分聚氨酯漆中的异氰酸酯组分。

4. 发明授权

US4324879A Process for the preparation of polyisocyanates containing isocyanurate groups and the use thereof 失效
标题翻译：制备含有异氰脲酸酯基团的多异氰酸酯的方法及其用途
公开(公告)号：US4324879A
公开(公告)日：1982-04-13
申请号：US151005
申请日：1980-05-19
申请人： Manfred Bock , Josef Pedain , Walter Uerdingen
发明人： Manfred Bock , Josef Pedain , Walter Uerdingen
IPC分类号： C07D251/34 , C08G18/00 , C08G18/79 , C08G18/80 , C08G18/20
CPC分类号： C07D251/34 , C08G18/792 , C08G18/8061 , C08G2150/20
摘要： The present invention is concerned with an improved process for the production of partially trimerized hexamethylene diisocyanate which yields isocyanurate isocyanates which have low viscosity and low monomer contents by the use of a quaternary ammonium hydroxide catalyst which is hydroxyalkyl substituted at its N atom.
摘要翻译：本发明涉及制备部分三聚的六亚甲基二异氰酸酯的改进方法，其通过使用在其N原子上被羟烷基取代的季铵氢氧化物催化剂得到具有低粘度和低单体含量的异氰脲酸酯异氰酸酯。

5. 发明授权

US4296230A Polyurethane coatings produced from (1) a polyisocyanate mixture of polyisocyanates from the diphenol methane series and a polyhydroxy polyether containing at least one tertiary amine nitrogen with (2) a polyol in a two component coating system 失效
标题翻译：由（1）来自二酚系列的多异氰酸酯的多异氰酸酯混合物和含有至少一种叔胺氮的多羟基聚醚与（2）多元醇在双组分涂布体系中的多异氰酸酯混合物
公开(公告)号：US4296230A
公开(公告)日：1981-10-20
申请号：US938165
申请日：1978-08-30
申请人： Josef Pedain , Walter Uerdingen , Hans-Jurgen Muller
发明人： Josef Pedain , Walter Uerdingen , Hans-Jurgen Muller
IPC分类号： C08G18/00 , C08G18/10 , C08G18/50 , C08G18/72 , C08G18/76 , C09D5/46 , C09D175/00
CPC分类号： C08G18/7664 , C08G18/10 , C08G18/5021 , Y10T428/31551
摘要： The present invention relates to a process for the production of coatings by coating substrates of any type with a coating composition of which the binder consists essentially of a mixture of:(a) a polyisocyanate component and(b) at least one organic polyhydroxyl compound, distinguished by the fact that the polyisocyanate component(a) is a reaction product obtained from:(i) a polyisocyanate mixture which, in addition to from about 20 to 80%, by weight, of 2,4'-diisocyanato diphenyl methane, contains a total of from about 80 to 20%, by weight, of 2,2'-diisocyanato diphenyl methane, 4,4'-diisocyanato diphenyl methane and, optionally, higher nuclear polyisocyanates of the diphenyl methane series and(ii) a polyhydroxy polyether containing at least one tertiary amine nitrogen atom and having an average molecular weight of from about 500 to 10,000 or a polyhydroxy polyether mixture containing at least one such polyhydroxy polyether and having an average molecular weight of from about 500 to 10,000.components (i) and (ii) having been reacted in an NCO:OH equivalent ratio of from about 300:1 to 10:1 to form a reaction product containing free isocyanate groups and urethane groups.
摘要翻译：本发明涉及一种通过用涂料组合物涂覆任何类型的基材来生产涂料的方法，其中粘合剂基本上由下列混合物组成：（a）多异氰酸酯组分和（b）至少一种有机多羟基化合物，其特征在于多异氰酸酯组分（a）是由以下物质获得的反应产物：（i）多异氰酸酯混合物，除了约20至80重量％的2,4'-二异氰酸酯二苯基甲烷外，总共约80至20重量％的2,2'-二异氰酸根合二苯基甲烷，4,4'-二异氰酸根合二苯基甲烷和任选的二苯基甲烷系列的较高核多异氰酸酯和（ii）多羟基聚醚含有至少一个叔胺氮原子并且具有约500至10,000的平均分子量或包含至少一种这样的多羟基聚醚并且平均分子量为约50的多羟基聚醚混合物 0到10,000。组分（i）和（ii）以约300:1至10:1的NCO:OH当量比反应形成含有游离异氰酸酯基团和氨基甲酸酯基团的反应产物。

6. 发明授权

US4137389A Low-molecular weight acrylate resins and a process for their production 失效
标题翻译：低分子量丙烯酸酯树脂及其制备方法
公开(公告)号：US4137389A
公开(公告)日：1979-01-30
申请号：US871248
申请日：1978-01-23
申请人： Frank Wingler , Josef Pedain , Walter Uerdingen
发明人： Frank Wingler , Josef Pedain , Walter Uerdingen
IPC分类号： C08F2/02 , C08F220/12 , C08J3/09 , C08F2/00 , C08F4/38 , C08F16/12
CPC分类号： C08J3/095 , C08F2/02 , C08F220/12 , C08K5/06 , C08J2333/06
摘要： A process for the production of a crosslinkable low-molecular weight acrylic resin containing hydroxyl-groups and having a low-molecular consistency factor by the radical bulk copolymerization of(A) 0 to 30 parts by weight of a hydroxyalkyl ester of acrylic acid or methacrylic acid or mixtures thereof;(B) 0 to 60 parts by wt. of styrene or a substituted styrene or methyl methacrylate or mixtures thereof;(C) 10 to 90 parts by weight of an acrylic acid ester or of a methacrylic acid ester with 2 to 12 carbon atoms in the alcohol radical or mixtures thereof;(D) 0 to 30 parts by weight of an .alpha.,.beta.-monoolefinically saturated mono- or di-carboxylic acid with 3 to 5 carbon atoms or of a maleic acid semiester or mixtures thereof or reaction products thereof with a monoglycidyl compound, in the presence of 10 to 70 parts by weight of a monoallyl ether of an at least trihydric alcohol,The sum of the parts by weight of all the monomers A - E amounting to 100,Wherein the indicated quantity of monomer E is initially introduced and, at temperatures above 100.degree. C, monomers A to D together with 0.5 to 6% by weight, based on A to D, of an initiator with a half-life period at 100 to 160.degree. C of 0.01 to 100 minutes, are introduced over a period of 1 to 6 hours and polymerized, at least 98% by weight of the monomers A to D and from 36 to 95% by weight of monomer E being converted. Acrylate resins of this type are eminently suitable for the production of readily processible binder mixtures which although low in viscosity, have a very high solids content.
摘要翻译：一种通过（A）0-30重量份的丙烯酸或甲基丙烯酸羟烷基酯的自由基本体共聚生产含羟基并具有低分子稠度因子的可交联的低分子量丙烯酸树脂的方法酸或其混合物; （B）0〜60重量份。的苯乙烯或取代的苯乙烯或甲基丙烯酸甲酯或其混合物; （C）10至90重量份的丙烯酸酯或醇基中具有2至12个碳原子的甲基丙烯酸酯或其混合物; （D）0至30重量份具有3至5个碳原子的α，β-单烯烃饱和的单羧酸或二羧酸或马来酸半酯或其混合物或其与单缩水甘油基化合物的反应产物，在存在10至70重量份的至少三元醇的单烯丙基醚，所有单体A-E的重量份数为100，由于初始引入了单体E的指示数量，并且在温度高于100℃，单体A至D和基于A至D的0.5至6重量％的引发剂，其在100至160℃下的半衰期为0.01至100分钟的引发剂通过时间为1至6小时并聚合，至少98重量％的单体A至D和36至95重量％的单体E被转化。这种类型的丙烯酸酯树脂非常适用于生产易于加工的粘合剂混合物，尽管粘度低，但固体含量非常高。

7. 发明授权

US5055345A Multilayer composite material 失效
标题翻译：多层复合材料
公开(公告)号：US5055345A
公开(公告)日：1991-10-08
申请号：US482425
申请日：1990-02-20
申请人： Joachim Wank , Walter Uerdingen , Lutz Schrader , Werner Waldenrath
发明人： Joachim Wank , Walter Uerdingen , Lutz Schrader , Werner Waldenrath
IPC分类号： B32B7/02 , B32B7/12 , B32B27/08 , B32B27/20 , B32B27/40 , B42D25/00
CPC分类号： B32B27/08 , B42D25/00 , B42D25/47 , B42D2033/04 , B42D2033/20 , B42D2033/30 , B42D25/45 , Y10S428/90 , Y10S428/916 , Y10T428/1438 , Y10T428/1462 , Y10T428/24967 , Y10T428/31507 , Y10T428/31551
摘要： A 0.3 to 2 mm thick multilayer composite material comprising the following layers:1st layer: 0.01 to 0.3 mm thick highly transparent thermoplastic2nd layer: 5 to 50 .mu.m thick decorative ink layer and/or 5 to 50 .mu.m thick adhesive layer3rd layer: 0.05 to 0.5 mm thick thermoplastic containing 0.1 to 30% by weight pigment4th layer: 0.05 to 0.8 mm thick highly elastic plastic containing up to 30% by weight pigment5th layer: 0.05 to 0.5 mm thick thermoplastic containing 0.1 to 30% by weight pigment6th layer: 5 to 50 .mu.m decorative ink layer and/or 5 to 50 .mu.m thick adhesive layer7th layer: 0.01 to 0.3 mm thick highly transparent thermoplastic is disclosedlayers 3 and 5 being optional.
摘要翻译：含有以下层的0.3〜2mm厚的多层复合材料：第1层：0.01〜0.3mm厚的高透明热塑性第2层：5〜50μm厚的装饰油墨层和/或5〜50μm厚的粘合层第3层：含有0.1〜30重量％颜料的0.05〜0.5mm厚的热塑性第4层：含有高达30重量％颜料的0.05〜0.8mm厚的高弹性塑料第5层：含有0.1〜30重量％的0.05〜0.5mm厚的热塑性颜料第6层：5〜50μm的装饰油墨层和/或5〜50μm厚的粘合剂层第7层：0.01〜0.3mm厚的高透明性的热塑性塑料是公开的层3和5。

8. 发明授权

US4812589A Polyhydroxyl compounds containing a sulfonic acid ester group 失效
标题翻译：含有磺酸酯基的多羟基化合物
公开(公告)号：US4812589A
公开(公告)日：1989-03-14
申请号：US908435
申请日：1986-09-17
申请人： Klaus Prater , Walter Uerdingen , Heinrich Heine , Dieter Freitag
发明人： Klaus Prater , Walter Uerdingen , Heinrich Heine , Dieter Freitag
IPC分类号： C08G18/00 , C07C67/00 , C07C301/00 , C07C303/10 , C07C303/26 , C07C309/63 , C07C309/65 , C08G18/30 , C08G18/38 , C07C143/68
CPC分类号： C08G18/3855 , C07C309/00
摘要： The invention relates to a process for the production of sulphonic acid ester group-containing polyhydroxyl compounds having an average hydroxyl functionality of from 1.5 to 4, comprising reacting(a) paraffin sulphochlorides which are obtained by sulphochlorination of paraffins containing from 10 to 18 carbon atoms or of industrial mixtures of these paraffins, with unreacted paraffins and/or with chloroparaffins, having saponifiable chlorine content, based on the total weight of component (a), of from 5 to 15% with(b) an alcohol which is at least trihydric and which contains primary and/or secondary hydroxyl groups within the molecular weight range of from 92 to 250 or with mixtures of polyhydric alcohols having a molecular weight in the range of from 62 to 250 with an average hydroxyl functionality of from 2.5 to 5in the presence of hydrogen chloride acceptors while maintaining an equivalent ratio of hydroxyl groups to sulphochloride groups of at least 2:1 with the optional removal of sulphochloride group-free paraffin and/or chloroparaffin and excess alcohol from the reaction mixture after the reaction.
摘要翻译：本发明涉及一种具有平均羟基官能度为1.5至4的含磺酸酯基的多羟基化合物的制备方法，包括使（a）通过使含有10至18个碳原子的链烷烃的亚氯化得到的链烷烃氯化物或这些链烷烃的工业混合物与未反应的烷烃和/或与氯代烷烃的有机物混合物，其组分（a）的可皂化氯含量为5至15％，（b）至少三元醇并且其在92至250的分子量范围内含有伯和/或仲羟基，或者在分子量范围为62-250的多元醇与平均羟基官能度为2.5至5的混合物中氯化氢受体的存在，同时保持至少2:1的羟基与硫酰氯基团的当量比，并且可选地除去的不含亚磺酰基的无石蜡和/或氯代石蜡和过量的醇从反应混合物中反应。

9. 发明授权

US4666980A Transparent moulding compositions 失效
标题翻译：透明成型组合物
公开(公告)号：US4666980A
公开(公告)日：1987-05-19
申请号：US748864
申请日：1985-06-26
申请人： Christian Lindner , Karl-Heinz Ott , Walter Uerdingen , Hans-Eberhard Braese , Hans-Jurgen Kress
发明人： Christian Lindner , Karl-Heinz Ott , Walter Uerdingen , Hans-Eberhard Braese , Hans-Jurgen Kress
IPC分类号： C08L33/12 , C08F279/00 , C08F279/02 , C08L7/00 , C08L21/00 , C08L25/14 , C08L33/00 , C08L33/02 , C08L33/04 , C08L51/00 , C08L51/02 , C08L51/04 , C08L55/02 , C08F265/06
CPC分类号： C08L51/003 , C08L25/14 , C08L51/04 , C08L55/02
摘要： This invention provides thermoplastic moulding moulding compositions with good dimensional stability under heat and transparency consisting of particular graft polymers and optionally thermoplastic polymer resins.
摘要翻译：本发明提供在特定的接枝聚合物和任选的热塑性聚合物树脂的热和透明度下具有良好尺寸稳定性的热塑性模塑组合物。

10. 发明授权

US4404379A Cycloaminals and a process for their preparation 失效
标题翻译：环状物及其制备方法
公开(公告)号：US4404379A
公开(公告)日：1983-09-13
申请号：US935439
申请日：1978-08-21
申请人： Manfred Hajek , Kuno Wagner , Walter Uerdingen , Wolfgang Wellner
发明人： Manfred Hajek , Kuno Wagner , Walter Uerdingen , Wolfgang Wellner
IPC分类号： C07D233/02 , C07D239/04 , C08G18/80
CPC分类号： C07D239/04 , C07D233/02 , C08G18/808
摘要： The present invention is concerned with a new class of compounds prepared by reacting cyclic aminals of the formula ##STR1## with polyisocyanates of the formula R.sub.5 (NCO).sub.m+n to yield ##STR2## and with this process for obtaining said compounds, as well as the use of such compounds in polyurethane chemistry. If such compounds are free of isocyanates (n=0) they are useful as latent cross-linkers or hardeners activatable by heat or moisture. If such compounds carry free isocyanate groups (n=1 or 2) there are useful as synthetic resin precursors. In the above formulaem represents an integer of from 1 to 3, andn represents 0, 1 or 2, and the sum of m+n is 2 or 3,R.sub.1 represents an aliphatic hydrocarbon group which is optionally cyano-substituted and which has from 1 to 6 carbon atoms, a cycloaliphatic hydrocarbon group having from 5-10 carbon atoms or an araliphatic hydrocarbon group having from 7-10 carbon atoms;R.sub.2 represents a divalent aliphatic hydrocarbon group having from 2 to 6 carbon atoms, at least two carbon atoms being situated between the two nitrogen atoms;R.sub.3 and R.sub.4 are identical or different and represent hydrogen, aliphatic hydrocarbon groups having from 1 to 18 carbon atoms, cycloaliphatic hydrocarbon groups having from 5 to 10 carbon atoms or aromatic hydrocarbon groups having from 6 to 10 carbon atoms, or the two groups R.sub.3 and R.sub.4 together with the carbon atom of the heterocyclic ring may also form a 5-membered or 6-membered cycloaliphatic ring; andR.sub.5 represents an (m+n)-valent group such as that which can be obtained by the removal of m+n isocyanate groups from an (m+n)-valent polyisocyanate.
摘要翻译：本发明涉及通过使式“IMAGE”的环状胺与式R 5（NCO）m + n的多异氰酸酯反应得到新一类化合物，得到所述化合物的方法作为这种化合物在聚氨酯化学中的应用。如果这些化合物不含异氰酸酯（n = 0），它们可用作潜热的交联剂或通过热或湿气活化的硬化剂。如果这些化合物带有游离异氰酸酯基团（n = 1或2），则可用作合成树脂前体。在上式中，m表示1〜3的整数，n表示0,1或2，m + n的和为2或3，R1表示任意氰基取代的脂肪族烃基， 1至6个碳原子，具有5-10个碳原子的脂环族烃基或具有7-10个碳原子的芳脂族烃基; R2表示具有2至6个碳原子的二价脂族烃基，至少两个碳原子位于两个氮原子之间; R3和R4相同或不同，表示氢，具有1至18个碳原子的脂族烃基，具有5至10个碳原子的脂环族烃基或具有6至10个碳原子的芳族烃基，或两个基团R3和 R4与杂环的碳原子一起也可以形成5元或6元脂环族环; 并且R 5表示可以通过从（m + n）价多异氰酸酯除去m + n个异氰酸酯基团而得到的（m + n）价基团。

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