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1. 发明授权

US5064436A Bone prosthetic material 失效
标题翻译：骨髓前体材料
公开(公告)号：US5064436A
公开(公告)日：1991-11-12
申请号：US373708
申请日：1989-07-03
申请人： Makoto Ogiso , Tetsuro Ogawa , Takeshi Ichitsuka , Masahide Inoue
发明人： Makoto Ogiso , Tetsuro Ogawa , Takeshi Ichitsuka , Masahide Inoue
IPC分类号： A61L27/00 , A61F2/00 , A61K6/033 , A61L27/12 , A61L27/56 , C04B38/00
CPC分类号： C04B38/009 , A61L27/12 , A61L27/56 , A61F2310/00293
摘要： A bone prosthetic material composed of calcium phosphate group granules which have open cells with an average pore size of 0.01-(10 .mu.m).sup.2 over a surface density of at least one per 10 .mu.m.sup.2. The prosthetic material is prepared by mixing organic inflammable particles with a calcium based powder, granulating and then firing the mixture.
摘要翻译：由具有平均孔径为0.011-（10μm）的开孔的磷酸钙颗粒组成的骨修复材料，其表面密度至少为每10平方米至少1个。通过将有机易燃颗粒与钙基粉末混合，制粒然后烧结混合物来制备假体材料。

2. 发明授权

US5240659A Process for producing shaped article of oriented calcium phosphate type compound 失效
标题翻译：用于生产定向磷酸钙型化合物成型制品的方法
公开(公告)号：US5240659A
公开(公告)日：1993-08-31
申请号：US857638
申请日：1992-03-24
申请人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita , Akihiko Yokoo
发明人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita , Akihiko Yokoo
IPC分类号： A61F2/00 , A61L27/12 , C04B35/447 , C04B35/634
CPC分类号： C04B35/447 , A61L27/12 , C04B35/634 , A61F2310/00293
摘要： An oriented shaped article of a calcium phosphate type compound is disclosed, in which at least two crystallographic axes of the primary particles of which the shaped article is composed each is oriented in one direction, respectively, in at least the surface of said article. A sinter of the oriented shaped article and a processes for producing the article and the sinter are also disclosed.
摘要翻译：公开了一种磷酸钙型化合物的取向成型制品，其中至少两个成型制品的一次颗粒的结晶轴分别在至少所述制品的表面上沿一个方向取向。还公开了定向成型制品的烧结体以及制造制品和烧结体的方法。

3. 发明授权

US06306297B1 Packing material for liquid chromatography and process for producing the same 失效
标题翻译：液相色谱的包装材料及其制备方法
公开(公告)号：US06306297B1
公开(公告)日：2001-10-23
申请号：US08371205
申请日：1995-01-11
申请人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita , Akihiko Yokoo , Katsumi Kawamura
发明人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita , Akihiko Yokoo , Katsumi Kawamura
IPC分类号： B01D1508
CPC分类号： B01J20/28059 , B01D15/3847 , B01J20/048 , B01J20/28004 , B01J20/28019 , B01J20/28078 , B01J20/282 , B01J20/286 , B01J20/3021 , B01J20/3064 , B01J20/3078 , B01J20/3092 , B01J20/3204 , B01J20/3208 , B01J20/3234 , B01J2220/54 , B01J2220/58
摘要： Column packing materials useful in applications such as liquid chromatography, as well as a process for producing such a packing material are described. A first aspect of the invention concerns a column packing material composed of a spherical substrate having a coating of a calcium phosphate based compound on the surface thereof. A second aspect of the invention concerns a packing material comprising porous calcium phosphate based granules having open pores with an average pore size of from 0.01 to 20 &mgr;m, said granules being composed of crystalline particles with an average size of from 0.1 to 10 &mgr;m. A third aspect of the invention concerns a spherical packing material for liquid chromatography comprising spherical particles of at least one material selected from the group consisting of Ca10(PO4)6(OH)2, Ca3(PO4)2, Ca2P2O7, Ca(PO3)2, Ca10(PO4)6F2 and Ca10(PO4)6Cl2, said packing material having a dense structure with a porosity of no more than 5%. A fourth aspect of the invention concerns a packing for liquid chromatography comprising particles having at least on the surface thereof a fluoroapatite represented by formula (I): Ca10(PO4)6(OH)2−2xF2x (I) wherein x is a number of from about 0.1 to 1.
摘要翻译：描述了可用于诸如液相色谱法的应用的柱状填料，以及用于生产这种包装材料的方法。本发明的第一方面涉及一种由包含磷酸钙基化合物的表面的球状基材构成的柱状填充材料。本发明的第二方面涉及包含多孔磷酸钙基颗粒的填充材料，该颗粒具有开孔，平均孔径为0.01至20μm，所述颗粒由平均尺寸为0.1至10μm的结晶颗粒组成。本发明的第三方面涉及一种用于液相色谱的球形包装材料，其包括至少一种选自Ca10（PO4）6（OH）2，Ca3（PO4）2，Ca2P2O7，Ca（PO3）2，Ca10（PO4）6F2和Ca10（PO4）6Cl2）组成的材料，所述包装材料具有致密结构孔隙率不超过5％。本发明的第四方面涉及用于液相色谱的填料，其包括至少在其表面上具有由式（I）表示的氟磷灰石的颗粒：其中x是数量从大约0.1到1。

4. 发明授权

US5039408A Packing material for liquid chromatography 失效
标题翻译：液相色谱填充材料
公开(公告)号：US5039408A
公开(公告)日：1991-08-13
申请号：US461854
申请日：1990-01-08
申请人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita , Akihiko Yokoo , Katsumi Kawamura
发明人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita , Akihiko Yokoo , Katsumi Kawamura
IPC分类号： B01D15/08 , B01J20/04 , B01J20/32
CPC分类号： B01J20/28083 , B01J20/048 , B01J20/28004 , B01J20/28019 , B01J20/28085 , B01J20/282 , B01J20/286 , B01J20/3236 , B01J2220/54
摘要： Column packing materials useful in applications such as liquid chromatography, as well as a process for producing such a packing material are described. A first aspect of the invention concerns a column packing material composed of a spherical substrate having a coating of a calcium phosphate based compound on the surface thereof.A second aspect of the invention concerns a packing material comprising porous calcium phosphate based granules having open pores with an average pore size of from 0.01 to 20 .mu.m, said granules being composed of crystalline particles with an average size of from 0.1 to 10 .mu.m.A third aspect of the invention concerns a spherical packing material for liquid chromatography comprising spherical particles of at least one material selected from the group consisting of Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2, Ca.sub.3 (PO.sub.4).sub.2, Ca.sub.2 P.sub.2 O.sub.7, Ca(PO.sub.3).sub.2, Ca.sub.10 (PO.sub.4).sub.6 F.sub.2 and Ca.sub.10 (PO.sub.4).sub.6 Cl.sub.2, said packing material having a dense structure with a porosity of no more than 5%.A fourth aspect of the invention concerns a packing for liquid chromatography comprising particles having at least on the surface thereof a fluoroapatite represented by formula (I):Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2-2x F.sub.2x (I)wherein x is a number of from about 0.1 to 1.
摘要翻译：描述了可用于诸如液相色谱法的应用的柱状填料，以及用于生产这种包装材料的方法。本发明的第一方面涉及一种柱状填充材料，其由在其表面上具有磷酸钙基化合物的涂层的球形基材构成。本发明的第二方面涉及一种包含多孔磷酸钙基颗粒的包装材料，其具有平均孔径为0.01至20μm的开放孔，所述颗粒由平均尺寸为0.1-10μm的结晶颗粒组成。本发明的第三方面涉及一种用于液相色谱的球形包装材料，其包括选自Ca10（PO4）6（OH）2，Ca3（PO4）2，Ca2P2O7，Ca（PO3） 2，Ca10（PO4）6F2和Ca10（PO4）6Cl2，所述包装材料具有孔隙率不超过5％的致密结构。本发明的第四方面涉及一种用于液相色谱的填料，其包括至少在其表面上具有由式（I）表示的氟磷灰石的颗粒：Ca10（PO4）6（OH）2-2xF2x（I），其中x是约0.1至1。

5. 发明授权

US4957674A Method for producing calcium phosphate-based material 失效
标题翻译：磷酸钙基材料的制造方法
公开(公告)号：US4957674A
公开(公告)日：1990-09-18
申请号：US192552
申请日：1988-05-11
申请人： Takeshi Ichitsuka , Yasuhiko Hirayama , Tetsuro Ogawa
发明人： Takeshi Ichitsuka , Yasuhiko Hirayama , Tetsuro Ogawa
IPC分类号： C04B35/64 , A61F2/00 , A61K6/033 , A61L27/12 , C01B25/32 , C01B25/42 , C01B25/44 , C01B25/455 , C04B35/447
CPC分类号： A61K6/033 , A61L27/12 , C01B25/327 , C01B25/42 , C01B25/44 , C01B25/455 , A61F2310/00293
摘要： A method for producing a calcium phosphate-based material comprising:(a) molding a calcium phosphate powder;(b) preliminarily calcining the resulting molding in a vacuum or under a reduced pressure until the relative density is 95% or more; and(c) firing the molding in air, an inert gas, or nitrogen gas.

6. 发明授权

US5651882A Packing material for liquid chromatography and process for producing the same 失效
标题翻译：液相色谱的包装材料及其制备方法
公开(公告)号：US5651882A
公开(公告)日：1997-07-29
申请号：US371378
申请日：1995-01-11
申请人： Takeshi Ichitsuka , Tetsuro Ogawa , Katsumi Kawamura , Akihiko Yokoo
发明人： Takeshi Ichitsuka , Tetsuro Ogawa , Katsumi Kawamura , Akihiko Yokoo
IPC分类号： B01D15/08 , B01J20/04 , B01J20/32
CPC分类号： B01J20/28059 , B01D15/3847 , B01J20/048 , B01J20/28004 , B01J20/28019 , B01J20/28078 , B01J20/282 , B01J20/286 , B01J20/3021 , B01J20/3028 , B01J20/3064 , B01J20/3078 , B01J20/3092 , B01J20/3204 , B01J20/3208 , B01J20/3234 , B01J2220/54 , B01J2220/58
摘要： Column packing materials useful in applications such as liquid chromatography, as well as a process for producing such a packing material are described. A first aspect of the invention concerns a column packing material composed of a spherical substrate having a coating of a calcium phosphate based compound on the surface thereof.A second aspect of the invention concerns a packing material comprising porous calcium phosphate based granules having open pores with an average pore size of from 0.01 to 20 .mu.m, said granules being composed of crystalline particles with an average size of from 0.1 to 10 .mu.m.A third aspect of the invention concerns a spherical packing material for liquid chromatography comprising spherical particles of at least one material selected from the group consisting of Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2, Ca.sub.3 (PO.sub.4).sub.2, Ca.sub.2 P.sub.2 O.sub.7, Ca(PO.sub.3).sub.2, Ca.sub.10 (PO.sub.4).sub.6 F.sub.2 and Ca.sub.10 (PO.sub.4).sub.6 Cl.sub.2, said packing material having a dense structure with a porosity of no more than 5%.A fourth aspect of the invention concerns a packing for liquid chromatography comprising particles having at least on the surface thereof a fluoroapatite represented by formula (I):Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2-2x F.sub.2x (I)wherein x is a number of from about 0.1 to 1.
摘要翻译：描述了可用于诸如液相色谱法的应用的柱状填料，以及用于生产这种包装材料的方法。本发明的第一方面涉及一种柱状填充材料，其由在其表面上具有磷酸钙基化合物的涂层的球形基材构成。本发明的第二方面涉及一种包含多孔磷酸钙基颗粒的包装材料，其具有平均孔径为0.01至20μm的开放孔，所述颗粒由平均尺寸为0.1-10μm的结晶颗粒组成。本发明的第三方面涉及一种用于液相色谱的球形包装材料，其包括选自Ca10（PO4）6（OH）2，Ca3（PO4）2，Ca2P2O7，Ca（PO3） 2，Ca10（PO4）6F2和Ca10（PO4）6Cl2，所述包装材料具有孔隙率不超过5％的致密结构。本发明的第四方面涉及一种用于液相色谱的填料，其包括至少在其表面上具有由式（I）表示的氟磷灰石的颗粒：Ca10（PO4）6（OH）2-2xF2x（I），其中x是约0.1至1。

7. 发明授权

US5134009A Shaped article of oriented calcium phosphate type compounds, sinter thereof and processes for producing same 失效
标题翻译：面向磷酸钙型化合物的成型品及其制造方法及其制造方法
公开(公告)号：US5134009A
公开(公告)日：1992-07-28
申请号：US407009
申请日：1989-09-14
申请人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita , Akihiko Yokoo
发明人： Takeshi Ichitsuka , Tetsuro Ogawa , Masaya Sumita , Akihiko Yokoo
IPC分类号： A61L27/00 , A61F2/00 , A61L27/12 , C04B35/447 , C04B35/634 , C04B35/636 , C04B35/638
CPC分类号： C04B35/63416 , A61L27/12 , C04B35/447 , C04B35/634 , C04B35/63424 , C04B35/6365 , C04B35/638 , A61F2310/00293 , Y10T428/24058 , Y10T428/24124 , Y10T428/249921 , Y10T428/2927 , Y10T428/2929
摘要： An oriented shaped article of a calcium phosphate type compound is disclosed, in which at least two crystallographic axes of the primary particles of which the shaped article is composed each is oriented in one direction, respectively, in at least the surface of said article. A sinter of the oriented shaped article and a processes for producing the article and the sinter are also disclosed.

8. 发明授权

US5651884A Packing material for liquid chromatography 失效
标题翻译：液相色谱填充材料
公开(公告)号：US5651884A
公开(公告)日：1997-07-29
申请号：US469731
申请日：1995-06-06
申请人： Takeshi Ichitsuka , Tetsuro Ogawa , Katsumi Kawamura , Masaya Sumita , Akihiko Yokoo
发明人： Takeshi Ichitsuka , Tetsuro Ogawa , Katsumi Kawamura , Masaya Sumita , Akihiko Yokoo
IPC分类号： B01D15/08 , B01J20/04 , B01J20/32
CPC分类号： B01J20/28059 , B01D15/3847 , B01J20/048 , B01J20/28004 , B01J20/28019 , B01J20/28078 , B01J20/282 , B01J20/286 , B01J20/3021 , B01J20/3028 , B01J20/3064 , B01J20/3078 , B01J20/3092 , B01J20/3204 , B01J20/3208 , B01J20/3234 , B01J2220/54 , B01J2220/58
摘要： Column packing materials useful in applications such as liquid chromatography, as well as a process for producing such a packing material are described. A first aspect of the invention concerns a column packing material composed of a spherical substrate having a coating of a calcium phosphate based compound on the surface thereof.A second aspect of the invention concerns a packing material comprising porous calcium phosphate based granules having open pores with an average pore size of from 0.01 to 20 .mu.m, said granules being composed of crystalline particles with an average size of from 0.1 to 10 .mu.m.A third aspect of the invention concerns a spherical packing material for liquid chromatography comprising spherical particles of at least one material selected from the group consisting of Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2, Ca.sub.3 (PO.sub.4).sub.2, Ca.sub.2 P.sub.2 O.sub.7, Ca(PO.sub.3).sub.2, Ca.sub.10 (PO.sub.4).sub.6 F.sub.2 and Ca.sub.10 (PO.sub.4).sub.6 Cl.sub.2, said packing material having a dense stricture with a porosity of no more than 5%.A fourth aspect of the invention concerns a packing for liquid chromatography comprising particles having at least on the surface thereof a fluoroapatite represented by formula (I):Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2-2x F.sub.2x (I)wherein x is a number of from about 0.1 to 1.
摘要翻译：描述了可用于诸如液相色谱法的应用的柱状填料，以及用于生产这种包装材料的方法。本发明的第一方面涉及一种柱状填充材料，其由在其表面上具有磷酸钙基化合物的涂层的球形基材构成。本发明的第二方面涉及一种包含多孔磷酸钙基颗粒的包装材料，其具有平均孔径为0.01至20μm的开放孔，所述颗粒由平均尺寸为0.1-10μm的结晶颗粒组成。本发明的第三方面涉及一种用于液相色谱的球形包装材料，其包括选自Ca10（PO4）6（OH）2，Ca3（PO4）2，Ca2P2O7，Ca（PO3） 2，Ca10（PO4）6F2和Ca10（PO4）6Cl2，所述包装材料具有密度不大于5％的密度。本发明的第四方面涉及一种用于液相色谱的填料，其包括至少在其表面上具有由式（I）表示的氟磷灰石的颗粒：Ca10（PO4）6（OH）2-2xF2x（I），其中x是约0.1至1。

9. 再颁专利

USRE35340E Packing material for liquid chromatography 失效
标题翻译：液相色谱填充材料
公开(公告)号：USRE35340E
公开(公告)日：1996-10-01
申请号：US105850
申请日：1993-08-13
申请人： Takeshi Ichitsuka , Tetsuro Ogawa , Katsumi Kawamura , Masaya Sumita , Akihiko Yokoo
发明人： Takeshi Ichitsuka , Tetsuro Ogawa , Katsumi Kawamura , Masaya Sumita , Akihiko Yokoo
IPC分类号： B01J20/04 , B01D15/08
CPC分类号： G01N30/482 , B01J20/048 , B01J20/103 , B01J20/28004 , B01J20/28019 , B01J20/28054 , B01J20/28078 , B01J20/28095 , B01J20/282 , B01J20/283 , B01J20/3021 , B01J20/3078 , B01J20/3204 , B01J20/3236 , B01J2220/54
摘要： Column packing materials useful in applications such as liquid chromatography, as well as a process for producing such a packing material are described. A first aspect of the invention concerns a column packing material composed of a spherical substrate having a coating of a calcium phosphate based compound on the surface thereof.A second aspect of the invention concerns a packing material comprising porous calcium phosphate based granules having open pores with an average pore size of from 0.01 to 20 .mu.m, said granules being composed of crystalline particles with an average size of from 0.1 to 10 .mu.m.A third aspect of the invention concerns a spherical packing material for liquid chromatography comprising spherical particles of at least one material selected from the group consisting of Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2, Ca.sub.3 (PO.sub.4).sub.2, Ca.sub.2 P.sub.2 O.sub.7, Ca(PO.sub.3).sub.2, Ca.sub.10 (PO.sub.4).sub.6 F.sub.2 and Ca.sub.10 (PO.sub.4).sub.6 Cl.sub.2, said packing material having a dense structure with a porosity of no more than 5%.A fourth aspect of the invention concerns a packing for liquid chromatography comprising particles having at least on the surface thereof a fluoroapatite represented by formula (I):Ca.sub.10 (PO.sub.4).sub.6 (OH).sub.2-2x F.sub.2x (I)wherein x is a number of from about 0.1 to 1.
摘要翻译：描述了可用于诸如液相色谱法的应用的柱状填料，以及用于生产这种包装材料的方法。本发明的第一方面涉及一种柱状填充材料，其由在其表面上具有磷酸钙基化合物的涂层的球形基材构成。本发明的第二方面涉及一种包含多孔磷酸钙基颗粒的包装材料，其具有平均孔径为0.01至20μm的开放孔，所述颗粒由平均尺寸为0.1-10μm的结晶颗粒组成。本发明的第三方面涉及一种用于液相色谱的球形包装材料，其包括选自Ca10（PO4）6（OH）2，Ca3（PO4）2，Ca2P2O7，Ca（PO3） 2，Ca10（PO4）6F2和Ca10（PO4）6Cl2，所述包装材料具有孔隙率不超过5％的致密结构。本发明的第四方面涉及一种用于液相色谱的填料，其包括至少在其表面上具有由式（I）表示的氟磷灰石的颗粒：Ca10（PO4）6（OH）2-2xF2x（I），其中x是约0.1至1。

10. 再颁专利

USRE34037E Support for biomedical implant device 失效
公开(公告)号：USRE34037E
公开(公告)日：1992-08-18
申请号：US642582
申请日：1991-01-17
申请人： Masahide Inoue , Takeshi Ichitsuka , Yasuhiko Hirayama , Shozo Koshikawa , Tateki Kitaoka , Nobuo Nakabayashi , Tatsumichi Takeda , Osamu Minoo
发明人： Masahide Inoue , Takeshi Ichitsuka , Yasuhiko Hirayama , Shozo Koshikawa , Tateki Kitaoka , Nobuo Nakabayashi , Tatsumichi Takeda , Osamu Minoo
IPC分类号： A61M25/02 , A61F2/00 , A61L27/12 , A61L29/02
CPC分类号： A61L29/02 , A61L27/12 , A61F2310/00293
摘要： A support for a biomedical implant device in which the support has a surface layer composed of a biocompatible calcium phosphate material such as sintered hydroxyapatite with a porosity of 50-60% and pore size of 0.5-500 micrometers. Preferably, the surface layer is formed with projections or recesses of a few hundred micrometers size.

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