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1. 发明授权

US09821304B2 Process for the treatment of an ion exchange resin 有权
公开(公告)号：US09821304B2
公开(公告)日：2017-11-21
申请号：US14452101
申请日：2014-08-05
申请人： Lucite International UK Limited
发明人： Trevor Huw Morris
IPC分类号： B01J49/60 , B01J49/00 , C07C67/343 , C07C67/60 , B01J49/50 , B01J49/53
CPC分类号： B01J49/60 , B01J49/50 , B01J49/53 , C07C67/343 , C07C67/60 , Y02P20/582 , C07C69/54
摘要： A process for the reactivation of an acidic ion exchange resin is described. The invention relates to the treatment of an at least partially deactivated resin which has been deactivated by contact with an impure ethylenically unsaturated acid or ester containing target impurities. The reactivation includes the step of contacting the at least partially deactivated resin with an alcohol to thereby increase the activity thereof. The invention extends to reactivating a resin deactivated by contact with an impure ethylenically unsaturated acid, ester or nitrile containing target impurities by contacting the at least partially deactivated resin with an alcohol and a carboxylic acid to thereby increase the activity thereof. A reactivated resin and a process for preparing and purifying an ethylenically unsaturated acid or ester of the following formula: R1—C(═(CH2)m)—COOR2 are also described.

2. 发明申请

US20170036984A1 PROCESS FOR PRODUCTION OF A SILICA-SUPPORTED ALKALI METAL CATALYST 审中-公开
标题翻译：生产二氧化硅支持的碱金属催化剂的方法
公开(公告)号：US20170036984A1
公开(公告)日：2017-02-09
申请号：US15234751
申请日：2016-08-11
申请人： Lucite International UK Limited
发明人： Ian Andrew YORK , Trevor Huw Morris
IPC分类号： C07C51/353 , B01J23/92 , B01J38/48 , B01J35/00 , B01J35/10 , B01J23/04 , B01J21/08
CPC分类号： C07C51/353 , B01J21/08 , B01J23/04 , B01J23/92 , B01J35/0006 , B01J35/0013 , B01J35/1019 , B01J38/485 , B01J38/64 , G06F11/3632 , G06F11/3656 , Y02P20/584 , C07C57/04
摘要： A process for regenerating a silica-supported depleted alkali metal catalyst is described. The level of alkali metal on the depleted catalyst is at least 0.5 mol % and the silica support is a zero-gel. The process comprises the steps of contacting the silica supported depleted alkali metal catalyst with a solution of a salt of the alkali metal in a solvent system that has a polar organic solvent as the majority component. A re-impregnated catalyst prepared by the process of the invention any comprising a silica zero-gel support and a catalytic metal selected from an alkali metal in the range 0.5-5 mol % on the catalyst, wherein the surface area of the silica support is
摘要翻译：描述了二氧化硅负载的贫碱金属催化剂的再生方法。贫化催化剂上的碱金属含量至少为0.5mol％，二氧化硅载体为零凝胶。该方法包括以下步骤：使二氧化硅负载的贫碱金属催化剂与碱金属盐的溶液在具有极性有机溶剂作为主要组分的溶剂体系中接触。通过本发明方法制备的再浸渍催化剂，其任一种包括二氧化硅零凝胶载体和选自催化剂上0.5-5mol％范围的碱金属的催化金属，其中二氧化硅载体的表面积为还描述了<180m 2 / g。本发明适用于制备烯属不饱和酸或酯的方法，包括使式R 1 -CH 2 -COOR 3的链烷酸或酯与甲醛或合适的甲醛源接触。

3. 发明授权

US10221121B2 Process for production of a silica-supported alkali metal catalyst 有权
公开(公告)号：US10221121B2
公开(公告)日：2019-03-05
申请号：US15234751
申请日：2016-08-11
申请人： Lucite International UK Limited
发明人： Ian Andrew York , Trevor Huw Morris
IPC分类号： B01J21/08 , B01J23/04 , B01J23/92 , B01J35/00 , B01J35/10 , B01J38/48 , B01J38/64 , C07C57/04 , G06F11/36 , C07C51/353
摘要： A process for regenerating a silica-supported depleted alkali metal catalyst is described. The level of alkali metal on the depleted catalyst is at least 0.5 mol % and the silica support is a zero-gel. The process comprises the steps of contacting the silica supported depleted alkali metal catalyst with a solution of a salt of the alkali metal in a solvent system that has a polar organic solvent as the majority component. A re-impregnated catalyst prepared by the process of the invention any comprising a silica zero-gel support and a catalytic metal selected from an alkali metal in the range 0.5-5 mol % on the catalyst, wherein the surface area of the silica support is

4. 发明授权

US09504991B2 Process for production of a silica-supported alkali metal catalyst 有权
标题翻译：生产二氧化硅负载的碱金属催化剂的方法
公开(公告)号：US09504991B2
公开(公告)日：2016-11-29
申请号：US14432430
申请日：2013-10-01
申请人： Lucite International UK Limited
发明人： Ian Andrew York , Trevor Huw Morris
IPC分类号： B01J23/92 , B01J23/04 , B01J38/64 , C07C51/353 , B01J38/48 , G06F11/36
CPC分类号： C07C51/353 , B01J21/08 , B01J23/04 , B01J23/92 , B01J35/0006 , B01J35/0013 , B01J35/1019 , B01J38/485 , B01J38/64 , G06F11/3632 , G06F11/3656 , Y02P20/584 , C07C57/04
摘要： A process for regenerating a silica-supported depleted alkali metal catalyst is described. The level of alkali metal on the depleted catalyst is at least 0.5 mol % and the silica support is a zero-gel. The process comprises the steps of contacting the silica supported depleted alkali metal catalyst with a solution of a salt of the alkali metal in a solvent system that has a polar organic solvent as the majority component. A re-impregnated catalyst prepared by the process of the invention any comprising a silica zero-gel support and a catalytic metal selected from an alkali metal in the range 0.5-5 mol % on the catalyst, wherein the surface area of the silica support is
摘要翻译：描述了二氧化硅负载的贫碱金属催化剂的再生方法。贫化催化剂上的碱金属含量至少为0.5mol％，二氧化硅载体为零凝胶。该方法包括以下步骤：使二氧化硅负载的贫碱金属催化剂与碱金属盐的溶液在具有极性有机溶剂作为主要组分的溶剂体系中接触。通过本发明方法制备的再浸渍催化剂，其任一种包括二氧化硅零凝胶载体和选自催化剂上0.5-5mol％范围的碱金属的催化金属，其中二氧化硅载体的表面积为还描述了<180m 2 / g。本发明适用于制备烯属不饱和酸或酯的方法，包括使式R 1 -CH 2 -COOR 3的链烷酸或酯与甲醛或合适的甲醛源接触。

5. 发明申请

US20150238942A1 PROCESS FOR PRODUCTION OF A SILICA-SUPPORTED ALKALI METAL CATALYST 有权
标题翻译：生产二氧化硅支持的碱金属催化剂的方法
公开(公告)号：US20150238942A1
公开(公告)日：2015-08-27
申请号：US14432430
申请日：2013-10-01
申请人： LUCITE INTERNATIONAL UK LIMITED
发明人： Ian Andrew York , Trevor Huw Morris
IPC分类号： B01J23/92 , B01J38/64 , C07C51/353 , B01J23/04
CPC分类号： C07C51/353 , B01J21/08 , B01J23/04 , B01J23/92 , B01J35/0006 , B01J35/0013 , B01J35/1019 , B01J38/485 , B01J38/64 , G06F11/3632 , G06F11/3656 , Y02P20/584 , C07C57/04
摘要： A process for regenerating a silica-supported depleted alkali metal catalyst is described. The level of alkali metal on the depleted catalyst is at least 0.5 mol % and the silica support is a zero-gel. The process comprises the steps of contacting the silica supported depleted alkali metal catalyst with a solution of a salt of the alkali metal in a solvent system that has a polar organic solvent as the majority component. A re-impregnated catalyst prepared by the process of the invention any comprising a silicazero-gel support and a catalytic metal selected from an alkali metal in the range 0.5-5 mol % on the catalyst, wherein the surface area of the silica support is
摘要翻译：描述了二氧化硅负载的贫碱金属催化剂的再生方法。贫化催化剂上的碱金属含量至少为0.5mol％，二氧化硅载体为零凝胶。该方法包括以下步骤：使二氧化硅负载的贫碱金属催化剂与碱金属盐的溶液在具有极性有机溶剂作为主要组分的溶剂体系中接触。通过本发明的方法制备的再浸渍的催化剂，其任何包含硅氮烷凝胶载体和选自催化剂上0.5-5mol％范围的碱金属的催化金属，其中二氧化硅载体的表面积< 还描述了180m 2 / g。本发明适用于制备烯属不饱和酸或酯的方法，包括使式R 1 -CH 2 -COOR 3的链烷酸或酯与甲醛或合适的甲醛源接触。

6. 发明申请

US20140343176A1 PROCESS FOR THE TREATMENT OF AN ION EXCHANGE RESIN 有权
标题翻译：处理离子交换树脂的方法
公开(公告)号：US20140343176A1
公开(公告)日：2014-11-20
申请号：US14452101
申请日：2014-08-05
申请人： Lucite International UK Limited
发明人： Trevor Huw Morris
IPC分类号： B01J49/00
CPC分类号： B01J49/60 , B01J49/50 , B01J49/53 , C07C67/343 , C07C67/60 , Y02P20/582 , C07C69/54
摘要： A process for the reactivation of an acidic ion exchange resin is described. The invention relates to the treatment of an at least partially deactivated resin which has been deactivated by contact with an impure ethylenically unsaturated acid or ester containing target impurities. The reactivation includes the step of contacting the at least partially deactivated resin with an alcohol to thereby increase the activity thereof. The invention extends to reactivating a resin deactivated by contact with an impure ethylenically unsaturated acid, ester or nitrile containing target impurities by contacting the at least partially deactivated resin with an alcohol and a carboxylic acid to thereby increase the activity thereof. A reactivated resin and a process for preparing and purifying an ethylenically unsaturated acid or ester of the following formula: R1—C(═(CH2)m)—COOR2 are also described.
摘要翻译：描述了酸性离子交换树脂的再活化方法。本发明涉及至少部分失活的树脂的处理，其通过与不纯的烯属不饱和酸或含有目标杂质的酯接触而失活。再活化包括使至少部分失活的树脂与醇接触从而增加其活性的步骤。本发明通过使至少部分失活的树脂与醇和羧酸接触从而增加其活性，延长了通过与不纯的烯键式不饱和酸，含有目标杂质的酯或腈的接触来还原的树脂失活。还描述了再活化的树脂和制备和纯化下式的R 1 -C（=（CH 2）m）-COOR 2的烯属不饱和酸或酯的方法。

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