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1. 发明授权

US5747411A Supported catalysts which are suitable for ammonoxidation 失效
标题翻译：适用于氨氧化的载体催化剂
公开(公告)号：US5747411A
公开(公告)日：1998-05-05
申请号：US513740
申请日：1995-08-10
申请人： Lothar Karrer , Frank-Friedrich Pape , Ulrich Kohler , Rainer Becker , Peter Weidlich , Michael Hullmann , Heinz-Josef Kneuper
发明人： Lothar Karrer , Frank-Friedrich Pape , Ulrich Kohler , Rainer Becker , Peter Weidlich , Michael Hullmann , Heinz-Josef Kneuper
IPC分类号： B01J23/18 , B01J23/22 , B01J23/30 , C07B61/00 , C07C253/28 , C07C255/51 , C07C253/24
CPC分类号： C07C253/28 , B01J23/18 , B01J23/22
摘要： Supported catalysts which are suitable for ammonoxidation, comprising a) a spherical or approximately spherical support material which essentially comprises aluminum oxide, silicon dioxide, titanium dioxide and/or zirconium dioxide and whose bulk density is from 0.6 to 1.2 kg/l, and b) an active material which comprises, as essential components, vanadium and antimony in oxidic form.
摘要翻译：适用于氨氧化的载体催化剂包括a）球形或近似球形的载体材料，其主要包含氧化铝，二氧化硅，二氧化钛和/或二氧化锆，其堆积密度为0.6-1.2kg / l，和b）作为必需成分的以氧化物形式存在的钒和锑的活性物质。

2. 发明授权

US5952262A Preparation of aromatic or heteroaromatic nitriles 失效
标题翻译：芳香族或杂芳族腈的制备
公开(公告)号：US5952262A
公开(公告)日：1999-09-14
申请号：US723915
申请日：1996-09-30
申请人： Lothar Karrer , Frank-Friedrich Pape , Heinz-Josef Kneuper , Michael Hullmann
发明人： Lothar Karrer , Frank-Friedrich Pape , Heinz-Josef Kneuper , Michael Hullmann
IPC分类号： C07D213/84 , B01J23/18 , B01J23/22 , B01J23/847 , C07B61/00 , C07C253/24 , C07C253/28 , C07C255/32 , C07C255/49 , B01J23/16 , C07C253/12
CPC分类号： B01J23/8472 , B01J23/18 , B01J23/22 , C07C253/28
摘要： Preparation of aromatic or heteroaromatic nitrites of the formula I ##STR1## where X is nitrogen or C-R.sup.6 and all of the R substituents represent hydrogen, alkyl, halogen, nitro, amino or similar groups, provided at least one substituent is a cyano or alkylcyano group. The nitrites I are produced by reacting aromatic or heteroaromatic hydrocarbons of the formula II ##STR2## where X is nitrogen or C-R.sup.6, provided at least one substituent is C.sub.1 -C.sub.8 -alkyl, with ammonia and oxygen at 200 to 600.degree. C. under a pressure of 0.1 to 5 bar in the gas phase over a supported catalyst containing 0.5 to 20% by weight of vanadium oxide. The supported catalyst consists of from 2 to 30 particle fractions whose mean diameters differ by from 10 to 80% and the supporting carrier of the catalyst has a bulk density of 0.6 to 1.2 kg/liter.
摘要翻译：制备式I的芳族或杂芳族亚硝酸盐，其中X是氮或C-R6，所有R取代基代表氢，烷基，卤素，硝基，氨基或类似基团，提供至少一个取代基是氰基或烷基氰基。亚硝酸盐I通过使式II的芳族或杂芳族化合物（其中X是氮或C-R 6）提供，其中至少一个取代基是C 1 -C 8 - 烷基，氨和氧在200-600℃的压力下在含有0.5至20重量％氧化钒的负载型催化剂的气相中为0.1至5巴。载体催化剂由2至30个颗粒级分组成，其平均直径为10至80％，催化剂的载体载体的堆积密度为0.6至1.2kg /升。

3. 发明申请

US20080200726A1 Method For the Continuous Production of an Amine 有权
标题翻译：连续生产胺的方法
公开(公告)号：US20080200726A1
公开(公告)日：2008-08-21
申请号：US11993891
申请日：2006-06-21
申请人： Frank Haese , Joachim Wulff-Doring , Ulrich Kohler , Peter Gaa , Frank-Friedrich Pape , Johann-Peter Melder , Manfred Julius
发明人： Frank Haese , Joachim Wulff-Doring , Ulrich Kohler , Peter Gaa , Frank-Friedrich Pape , Johann-Peter Melder , Manfred Julius
IPC分类号： C07C211/44
CPC分类号： C07C209/18 , Y02P20/582 , C07C211/45
摘要： Processes comprising: providing an aromatic alcohol; and reacting the aromatic alcohol with ammonia at a temperature of 80 to 350° C. in the presence of hydrogen and a heterogeneous catalyst to form a crude reaction product comprising a corresponding primary aromatic amine, wherein the heterogeneous catalyst comprises a catalytically active composition which, prior to reduction with hydrogen, comprises 90 to 99.8% by weight of zirconium dioxide (ZrO2), 0.1 to 5.0% by weight of an oxygen-comprising compound of palladium, and 0.1 to 5.0% by weight of an oxygen-comprising compound of platinum.
摘要翻译：方法包括：提供芳族醇; 并在80至350℃的温度下在氢气和非均相催化剂存在下使芳族醇与氨反应形成包含相应的伯芳族胺的粗反应产物，其中非均相催化剂包含催化活性组合物，在用氢还原之前，包含90-99.8重量％的二氧化锆（ZrO 2/2），0.1-5.0重量％的含氧化合物的钯和0.1-5.0重量％的含氧化合物的铂。

4. 发明授权

US5955620A Dehydrogenation of 1,4-butanediol to .gamma.-butyrolactone 失效
标题翻译：将1,4-丁二醇脱氢成γ-丁内酯
公开(公告)号：US5955620A
公开(公告)日：1999-09-21
申请号：US923553
申请日：1997-09-04
申请人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
发明人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
IPC分类号： C07D307/33 , B01J23/72 , B01J23/78 , C07B61/00 , C07D315/00 , C07D307/32
CPC分类号： C07D315/00 , B01J23/78 , B01J23/72 , B01J35/0053 , B01J35/0066
摘要： A process for dehydrogenating 1,4-butanediol to .gamma.-butyrolactone in the gas phase in the presence of a copper-containing catalyst, wherein the catalyst contains 4-40% by weight of copper and 0-5% by weight of Na.sub.2 O, based on the total weight of the catalyst, on a carrier consisting of 80-100% by weight of SiO.sub.2 and 0-20% by weight of CaO.
摘要翻译：在含铜催化剂存在下，在气相中将1,4-丁二醇脱氢为γ-丁内酯的方法，其中催化剂含有4-40重量％的铜和0-5重量％的Na 2 O，基于在由80-100重量％的SiO 2和0-20重量％的CaO组成的载体上的催化剂的总重量。

5. 发明申请

US20090076306A1 PROCESS FOR CONTINUOUS PREPARATION OF A PRIMARY AROMATIC AMINE 审中-公开
标题翻译：连续制备主要芳香胺的方法
公开(公告)号：US20090076306A1
公开(公告)日：2009-03-19
申请号：US12159099
申请日：2006-12-21
申请人： Frank Haese , Joachim Wulff-Doring , Ulrich Kohler , Peter Gaa , Frank-Friedrich Pape , Johann-Peter Melder , Manfred Julius
发明人： Frank Haese , Joachim Wulff-Doring , Ulrich Kohler , Peter Gaa , Frank-Friedrich Pape , Johann-Peter Melder , Manfred Julius
IPC分类号： C07C209/00 , C07C211/46
CPC分类号： C07C209/18 , C07C211/45
摘要： A process for continuously preparing a primary aromatic amine by reacting a corresponding cycloaliphatic alcohol with ammonia in the presence of hydrogen at a temperature in the range from 80 to 350° C. in the presence of a heterogeneous catalyst, wherein the catalytically active composition of the catalyst, before its reduction with hydrogen, comprises from 90 to 99.8% by weight of zirconium dioxide (ZrO2), from 0.1 to 5.0% by weight of oxygen compounds of palladium and from 0.1 to 5.0% by weight of oxygen compounds of platinum.
摘要翻译：一种在多异性催化剂存在下，在80-350℃的温度下，在氢气存在下使相应的脂环族醇与氨反应连续制备伯芳香胺的方法，其中催化活性组合物催化剂在用氢还原之前包含90-99.8重量％的二氧化锆（ZrO 2），0.1-5.0重量％的氧化合物钯和0.1-5.0重量％的氧化合物铂。

6. 发明授权

US5663438A Preparation of cyclic amines 失效
标题翻译：环胺的制备
公开(公告)号：US5663438A
公开(公告)日：1997-09-02
申请号：US516147
申请日：1995-08-17
申请人： Ulrich Kohler , Frank-Friedrich Pape , Matthias Irgang , Joachim Wulff-Doring , Michael Hesse , Peter Polanek
发明人： Ulrich Kohler , Frank-Friedrich Pape , Matthias Irgang , Joachim Wulff-Doring , Michael Hesse , Peter Polanek
IPC分类号： B01J23/40 , B01J23/42 , B01J23/58 , B01J23/63 , C07B61/00 , C07C209/16 , C07C209/68 , C07C211/45
CPC分类号： C07C209/68 , C07C209/16
摘要： A process for the preparation of a phenyl amine which may be substituted by alkyl or cycloalkyl in which the corresponding cyolohexylamine is reduced at temperatures of 150.degree. to 300.degree. C. and pressures of 0.01 to 50 bar in the presence of a heterogeneous dehydrogenation catalyst consisting essentially of palladium or a palladium/platinum mixture supported on carrier consisting of the oxides of rare earth metals and and metals of Group IVb of the Periodic Table of Elements, with the proviso that the palladium/platinum mixture may also be supported on an alumina carrier. The cyclohexylamine reactant can be advantageously prepared by reacting the corresponding phenol with ammonia and hydrogen at 100.degree. to 250.degree. C. in the presence of the same heterogeneous catalyst as a preliminary step to provide a two stage process using the same catalyst in both stages.
摘要翻译：制备苯基胺的方法，其可以被烷基或环烷基取代，其中相应的环己胺在150-300℃的温度和0.01至50巴的压力下在存在非均相脱氢催化剂的条件下还原，基本上由负载在由稀土金属的氧化物构成的载体上的钯或钯/铂混合物和元素周期表IVb族金属组成，条件是钯/铂混合物也可以负载在氧化铝载体上。环己胺反应物可以有利地通过在相同的非均相催化剂的存在下在100-250℃下使相应的苯酚与氨和氢反应来制备，以提供在两个阶段中使用相同催化剂的两阶段方法。

7. 发明授权

US6093677A Catalyst for dehydrogenating 1,4-butanediol to .gamma.-butyrolactone 有权
标题翻译：将1,4-丁二醇脱氢为γ-丁内酯的催化剂
公开(公告)号：US6093677A
公开(公告)日：2000-07-25
申请号：US323919
申请日：1999-06-02
申请人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
发明人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
IPC分类号： C07D307/33 , B01J23/72 , B01J23/78 , C07B61/00 , C07D315/00 , B01J23/70
CPC分类号： C07D315/00 , B01J23/78 , B01J23/72 , B01J35/0053 , B01J35/0066
摘要： A process for dehydrogenating 1,4-butanediol to .gamma.-butyrolactone in the gas phase in the presence of a copper-containing catalyst, wherein the catalyst contains 4-40% by weight of copper and 0-5% by weight of Na.sub.2 O, based on the total weight of the catalyst, on a carrier consisting of 80-100% by weight of SiO.sub.2 and 0-20% by weight of CaO.
摘要翻译：在含铜催化剂存在下，在气相中将1,4-丁二醇脱氢为γ-丁内酯的方法，其中催化剂含有4-40重量％的铜和0-5重量％的Na 2 O，基于在由80-100重量％的SiO 2和0-20重量％的CaO组成的载体上的催化剂的总重量。

8. 发明授权

US09345988B2 Devices and method for continuous distillative separation of a mixture containing one or more alkanolamine(s) 有权
标题翻译：用于连续蒸馏分离含有一种或多种链烷醇胺的混合物的装置和方法
公开(公告)号：US09345988B2
公开(公告)日：2016-05-24
申请号：US14057017
申请日：2013-10-18
申请人： Willi Schmidt , Gerd Kaibel , Elke Geiβler , Wolfgang Reif , Manfred Julius , Frank-Friedrich Pape
发明人： Willi Schmidt , Gerd Kaibel , Elke Geiβler , Wolfgang Reif , Manfred Julius , Frank-Friedrich Pape
IPC分类号： B01D3/32 , B01D3/14 , B01D3/42 , C07C213/04 , C07C213/10
CPC分类号： B01D3/32 , B01D3/14 , B01D3/42 , C07C213/04 , C07C213/10 , Y02P20/582 , C07C215/08 , C07C215/10
摘要： Apparatus and processes for continuous distillative separation of a mixture comprising one or more alkanolamine(s) are described. The separation is performed in one or more dividing wall column(s) and the alkanolamine or the alkanolamines is/are withdrawn as a side draw stream or side draw streams (side fraction(s)).
摘要翻译：描述了包含一种或多种链烷醇胺的混合物的连续蒸馏分离的装置和方法。分离在一个或多个分隔壁柱中进行，并且链烷醇胺或链烷醇胺作为侧馏分流或侧馏分流（侧馏分）排出。

9. 发明申请

US20110180151A1 METHOD FOR SAFELY PREVENTING BACKFLOWING IN THE CONVEYING OF A FLUID 有权
标题翻译：用于在流体输送中更好地防止回流的方法
公开(公告)号：US20110180151A1
公开(公告)日：2011-07-28
申请号：US13001467
申请日：2009-06-16
申请人： Franz Borgel , Alfred Krause , Mirko Kreitschmann , Anton Meier , Frank-Friedrich Pape , Wolfgang Reif , Michael Salla
发明人： Franz Borgel , Alfred Krause , Mirko Kreitschmann , Anton Meier , Frank-Friedrich Pape , Wolfgang Reif , Michael Salla
IPC分类号： F15D1/00
CPC分类号： F17D1/14 , F16K15/00 , Y10T137/0396
摘要： A method for reliably avoiding backflow in the transport of a liquid under pressure via a transport pipe (1), in which a shut-off device (2) with differential pressure switching is arranged, into a container (3) which is under pressure and which comprises the liquid to be transported and/or another liquid is proposed, wherein a pressure accumulator (4) which is filled with the liquid to be transported up to a certain level and above the liquid level, in direct contact with the liquid to be transported, with an inert gas is arranged in the transport pipe (1) upstream from the shut-off device (2) in the transport direction, the inert gas being provided in the pressure accumulator (4) under an excess pressure and in an amount relative to the container (3) to be filled which are designed so that, in the case of a drop in the pressure in the transport pipe (1), the inert gas ensures a positive pressure difference in the transport pipe (1) to the container (3) over a period which is at least as long as the reaction time of the shut-off device (2) and the shut-off device (2) has an emptying pipe (6) with emptying valve (7).
摘要翻译：一种用于可靠地避免在压力下输送液体的回流的方法，该输送管（1）具有压差切换的切断装置（2），其中所述输送管（1）设置在处于压力下的容器（3）中，其包括待运输的液体和/或另一种液体，其中填充有待运输的液体达到一定水平并高于液面的压力蓄积器（4）与液体直接接触在输送方向上从切断装置（2）的上游配置有惰性气体输送的惰性气体，惰性气体在过压压力下设置在蓄压器（4）中，相对于被填充的容器（3），其被设计成使得在输送管（1）中的压力下降的情况下，惰性气体确保输送管（1）中的正压差容器（3）至少在一段时间内只要关闭装置（2）和切断装置（2）的反应时间具有排空阀（7）的排空管（6）。

10. 发明申请

US20110168542A1 DEVICES AND METHOD FOR CONTINUOUS DISTILLATIVE SEPARATION OF A MIXTURE CONTAINING ONE OR MORE ALKANOLAMINE(S) 失效
标题翻译：含有一种或多种烷基胺的混合物的连续分离的装置和方法（S）
公开(公告)号：US20110168542A1
公开(公告)日：2011-07-14
申请号：US13119511
申请日：2009-09-16
申请人： Willi Schmidt , Gerd Kaibel , Elke Geissler , Wolfgang Reif , Manfred Julius , Frank-Friedrich Pape
发明人： Willi Schmidt , Gerd Kaibel , Elke Geissler , Wolfgang Reif , Manfred Julius , Frank-Friedrich Pape
IPC分类号： B01D3/14
CPC分类号： B01D3/32 , B01D3/14 , B01D3/42 , C07C213/04 , C07C213/10 , Y02P20/582 , C07C215/08 , C07C215/10
摘要： Apparatus and processes for continuous distillative separation of a mixture comprising one or more alkanolamine(s), wherein the separation is performed in one or more dividing wall column(s) and the alkanolamine or the alkanolamines is/are withdrawn as a side draw stream or side draw streams (side fraction(s)).
摘要翻译：将包含一种或多种烷醇胺的混合物的连续蒸馏分离的装置和方法，其中在一个或多个分隔壁塔和链烷醇胺或链烷醇胺中进行分离作为侧馏分流或侧馏分流（侧馏分）。

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