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    • 1. 发明授权
    • Oil/water/biocatalyst three phase separation process
    • 油/水/生物催化剂三相分离工艺
    • US5772901A
    • 1998-06-30
    • US640129
    • 1996-04-30
    • Li-Qun YuTodd A. MeyerBrian R. Folsom
    • Li-Qun YuTodd A. MeyerBrian R. Folsom
    • B01D17/00B01D17/038B01D35/06C10G32/00C10G33/06B01D21/26
    • C10G33/06B01D17/12
    • A method and an apparatus for separating a water/organic/solid emulsion, wherein the solid comprises particles having a length of about 50 .mu.m or less, are disclosed. The method comprises the steps of (1) directing the water/organic/solid emulsion from an emulsion source through a first hydrocyclone; (2) inverting the phase of the overflow emulsion from the first hydrocyclone; (3) directing the overflow emulsion through one or more subsequent hydrocyclones arranged in series; and (4) collecting the aqueous phase and the organic phase. The solid can be a biocatalyst, such as an intact bacterial, fungal or yeast cell. The organic phase is a liquid material substantially comprising carbon, which is substantially immiscible with water, such as petroleum. The apparatus of the present invention comprises a hydrocyclone series comprising two or more hydrocyclones connected in series, wherein the intake tube of the first hydrocyclone is connected by a line to an emulsion source; and a means for inverting the phase of the emulsion, interposed in the hydrocyclone series. The hydrocyclone series can comprise one or more de-oiling hydrocyclones, one or more dehydrating hydrocyclones or a combination thereof. The means for inverting the emulsion can be any means for sufficiently agitating the emulsion.
    • 公开了一种用于分离水/有机/固体乳液的方法和装置,其中所述固体包含长度为约50μm以下的颗粒。 该方法包括以下步骤:(1)将来自乳液源的水/有机/固体乳液通过第一水力旋流器引导; (2)从第一水力旋流器翻转溢流乳液的相位; (3)引导溢流乳液通过串联布置的一个或多个随后的水力旋流器; 和(4)收集水相和有机相。 固体可以是生物催化剂,例如完整的细菌,真菌或酵母细胞。 有机相是基本上包含碳的液体材料,其与水基本上不混溶,例如石油。 本发明的装置包括一个包括串联连接的两个或多个水力旋流器的水力旋流器系列,其中第一个水力旋流器的进气管通过一条管线连接到一个乳液源; 以及插入在水力旋流器系列中的用于颠倒乳液相的装置。 水力旋流器系列可以包括一种或多种去油水力旋流器,一种或多种脱水水力旋流器或其组合。 用于翻转乳液的方法可以是充分搅拌乳液的任何手段。