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1. 发明授权

US06765107B2 Method for manufacturing phosphonate esters 失效
标题翻译：膦酸酯的制备方法
公开(公告)号：US06765107B2
公开(公告)日：2004-07-20
申请号：US09979077
申请日：2002-07-30
申请人： Li-Biao Han , Farzad Mirzaei , Masato Tanaka
发明人： Li-Biao Han , Farzad Mirzaei , Masato Tanaka
IPC分类号： C07F940
CPC分类号： C07F9/657181 , C07F9/4015
摘要： The present invention relates to a new manufacturing method for phosphonate esters, which have utility as a carbon-carbon binding formation agent, as well as a synthesis intermediate for biologically active substances such as medical drugs and agri-chemicals. Specifically the present invention relates to a new industrially advantageous manufacturing method for phosphonate esters in which the phosphonate esters of the subject can be efficiently obtained with a high yield rate through a simple operation while having barely any side reaction or sub-product. More specifically, the present invention pertains to a manufacturing method for phosphonate esters in which secondary phosphonate esters and alkene compounds are reacted in a transition metal catalyst. In addition the present invention relates to a new manufacturing method for allylphosphonate esters in which secondary cyclic phosphonate esters and 1,3-diene compounds are reacted in a palladium catalyst.
摘要翻译：本发明涉及一种可用作碳 - 碳结合形成剂的膦酸酯的新制备方法，以及用于生物活性物质如医药和农药的合成中间体。具体而言，本发明涉及一种新的工业上有利的膦酸酯的制造方法，其中通过简单的操作，几乎没有任何副反应或副产物，可以以高产率有效地获得受试者的膦酸酯。更具体地说，本发明涉及膦酸酯的制备方法，其中次膦酸酯和烯烃化合物在过渡金属催化剂中反应。此外，本发明涉及烯丙基膦酸酯的新制备方法，其中二次环状膦酸酯和1,3-二烯化合物在钯催化剂中反应。

2. 发明授权

US07166737B2 Method for manufacturing phosphonate esters 失效
标题翻译：膦酸酯的制备方法
公开(公告)号：US07166737B2
公开(公告)日：2007-01-23
申请号：US10853312
申请日：2004-05-26
申请人： Li-Biao Han , Farzad Mirzaei , Masato Tanaka
发明人： Li-Biao Han , Farzad Mirzaei , Masato Tanaka
IPC分类号： C07F9/655
CPC分类号： C07F9/657181 , C07F9/4015
摘要： The present invention relates to a new manufacturing method for phosphonate esters, which have utility as a carbon-carbon binding formation agent, as well as a synthesis intermediate for biologically active substances such as medical drugs and agri-chemicals.Specifically the present invention relates to a new industrially advantageous manufacturing method for phosphonate esters in which the phosphonate esters of the subject can be efficiently obtained with a high yield rate through a simple operation while having barely any side reaction or sub-product.More specifically, the present invention pertains to a manufacturing method for phosphonate esters in which secondary phosphonate esters and alkene compounds are reacted in a transition metal catalyst. In addition the present invention relates to a new manufacturing method for allylphosphonate esters in which secondary cyclic phosphonate esters and 1,3-diene compounds are reacted in a palladium catalyst.
摘要翻译：本发明涉及一种可用作碳 - 碳结合形成剂的膦酸酯的新制备方法，以及用于生物活性物质如医药和农药的合成中间体。具体而言，本发明涉及一种新的工业上有利的膦酸酯的制造方法，其中通过简单的操作，几乎没有任何副反应或副产物，可以以高产率有效地获得受试者的膦酸酯。更具体地说，本发明涉及膦酸酯的制备方法，其中次膦酸酯和烯烃化合物在过渡金属催化剂中反应。此外，本发明涉及烯丙基膦酸酯的新制备方法，其中二次环状膦酸酯和1,3-二烯化合物在钯催化剂中反应。

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