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1. 发明授权

US5741876A Method of preparing powdered silicone resins 失效
标题翻译：粉状有机硅树脂的制备方法
公开(公告)号：US5741876A
公开(公告)日：1998-04-21
申请号：US774864
申请日：1996-12-23
申请人： Leslie Earl Carpenter, II , Jason Richard Cassiday , Leon Neal Cook , Linda Moy Madore , Theodore Arnold Oberhellman, III , Randall Gene Schmidt , Hongxi Zhang
发明人： Leslie Earl Carpenter, II , Jason Richard Cassiday , Leon Neal Cook , Linda Moy Madore , Theodore Arnold Oberhellman, III , Randall Gene Schmidt , Hongxi Zhang
IPC分类号： C08G77/04 , C08G77/06 , C08J3/12 , C08J3/16 , C08G77/00
CPC分类号： C08J3/122 , C08J3/16 , C08J2383/04
摘要： A method of obtaining fine-grained, free-flowing powdered silicone resins is disclosed. The powdered silicone resins contain very low or no residual aromatic solvents or other volatile organic compounds. The method includes the steps of (1) preparing a solution of an MQ silicone resin dissolved in a volatile liquid organosilicon solvent, such as hexamethyldisiloxane, and (2) spray-drying the solution obtained in step (1) to produce the silicone resin powder.
摘要翻译：公开了一种获得细粒状，自由流动的粉状有机硅树脂的方法。粉状有机硅树脂含有非常低的或没有残留的芳族溶剂或其他挥发性有机化合物。该方法包括以下步骤：（1）制备溶解在诸如六甲基二硅氧烷的挥发性液体有机硅溶剂中的MQ硅氧烷树脂的溶液，和（2）将步骤（1）中获得的溶液喷雾干燥以制备有机硅树脂粉末。

2. 发明授权

US5723521A Method of preparing solventless silicone resins that exhibit superior reconstitution and the resins so-produced 失效
标题翻译：制备表现出优异重构的无溶剂硅树脂的方法和如此制备的树脂
公开(公告)号：US5723521A
公开(公告)日：1998-03-03
申请号：US497736
申请日：1995-07-03
申请人： Leon Neal Cook , Richard Allen Hessick, Jr. , Hongxi Zhang , Randall Gene Schmidt
发明人： Leon Neal Cook , Richard Allen Hessick, Jr. , Hongxi Zhang , Randall Gene Schmidt
IPC分类号： C08G77/04 , C08G77/06 , C08J3/12 , C08J3/16 , C08K5/54
CPC分类号： C08J3/122 , C08J3/16 , C08J2383/04
摘要： Solventless silicone resins, which exhibit a high degree of reconstitution, are produced in forms such as powders and flakes. The degree of reconstitution is judged by the fact that silicone resin/fluid alloys produced therefrom exhibit only a minor shift in T.sub.g, the glass transition temperature, in comparison to analogous alloys produced from solvent dispersed (virgin) resin. Resin, and preferably virgin resin, is dispersed in a volatile liquid dispersant and blended with a nonvolatile silicone fluid. Thereafter, the volatile liquid dispersant is removed by means such as spray-drying or evaporation, resulting in the solventless resin forms of the invention.
摘要翻译：表现出高度重构的无溶剂硅树脂以粉末和薄片的形式生产。通过以下事实来判断重构程度：与由溶剂分散（原始）树脂制备的类似合金相比，由其生产的硅树脂/流体合金仅显示出Tg的微小偏移，玻璃化转变温度。树脂，优选原始树脂分散在挥发性液体分散剂中并与非挥发性硅氧烷流体共混。此后，通过喷雾干燥或蒸发等手段去除挥发性液体分散剂，得到本发明的无溶剂树脂形式。

3. 发明授权

US5708098A Method of preparing solventless, thermoplastic silicone pellets and the pellets so-produced 失效
标题翻译：制备无溶剂，热塑性硅氧烷颗粒和如此制备的颗粒的方法
公开(公告)号：US5708098A
公开(公告)日：1998-01-13
申请号：US705106
申请日：1996-08-28
申请人： Leon Neal Cook , Richard Allen Hessick, Jr. , Kevin Edward Lupton , David Joseph Romenesko , Randall Gene Schmidt , Hongxi Zhang
发明人： Leon Neal Cook , Richard Allen Hessick, Jr. , Kevin Edward Lupton , David Joseph Romenesko , Randall Gene Schmidt , Hongxi Zhang
IPC分类号： B29B9/12 , B29C47/00 , C08J3/12 , C08J3/20 , C08L83/04 , C08F283/00
CPC分类号： C08J3/12 , B29B9/12 , B29C47/00 , B29C47/0011 , B29K2083/00 , C08J2383/04
摘要： Solventless, thermoplastic silicone pellets are prepared blending silicone resins (A) of the MQ-type and with predominantly linear silicone fluids (B), such as polydimethylsiloxane liquids and gums, to substantially homogeneity. The blends are heated to a predetermined compression-forming temperature, compression-formed to a densified mass and shaped into a pellet form. The composition of the pellets is balanced such that the pellets exhibit plastic flow at the predetermined compression-forming temperature and resist agglomeration at temperatures at or below a predetermined maximum storage temperature.
摘要翻译：制备无溶剂的热塑性硅氧烷颗粒，其将MQ型的有机硅树脂（A）和主要为直链的硅氧烷流体（B）如聚二甲基硅氧烷液体和树胶混合至基本均匀。将共混物加热至预定的压缩成形温度，压缩形成致密化块并成形为颗粒形式。颗粒的组成是平衡的，使得颗粒在预定的压缩成形温度下呈现塑性流动并且在等于或低于预定最大储存温度的温度下抵抗附聚。

4. 发明授权

US6124407A Silicone composition, method for the preparation thereof, and silicone elastomer 有权
标题翻译：硅酮组合物，其制备方法和硅氧烷弹性体
公开(公告)号：US6124407A
公开(公告)日：2000-09-26
申请号：US181211
申请日：1998-10-28
申请人： Yeong Joo Lee , Michael Dean Livingston , Hongxi Zhang , Randall Gene Schmidt
发明人： Yeong Joo Lee , Michael Dean Livingston , Hongxi Zhang , Randall Gene Schmidt
IPC分类号： C08L83/07 , C08L83/04 , C08L83/05 , H01L23/29 , C08G77/04 , C08G77/12 , C08G77/20
CPC分类号： H01L23/296 , C08L83/04 , C08G77/12 , C08G77/16 , C08G77/20 , H01L2924/0002 , H01L2924/09701
摘要： A silicone composition comprising (A) 100 parts by weight of a polydiorganosiloxane containing an average of at least two silicon-bonded alkenyl groups per molecule; (B) 75 to 150 parts by weight of an organopolysiloxane resin having a number-average molecular weight of from 2,000 to 5,000 and consisting essentially of R.sup.3.sub.2 R.sup.4 SiO.sub.1/2 units and SiO.sub.4/2 units wherein each R.sup.3 is independently selected from the group consisting of monovalent hydrocarbon and monovalent halogenated hydrocarbon groups free of aliphatic unsaturation, R.sup.4 is selected from the group consisting of R.sup.3 and alkenyl, the mole ratio of R.sup.3.sub.2 R.sup.4 SiO.sub.1/2 units to SiO.sub.4/2 units is from 0.6:1 to 1.1:1, and the resin contains an average of from 2.5 to 7.5 mole percent of alkenyl groups; (C) an organohydrogenpolysiloxane having an average of at least three silicon-bonded hydrogen atoms per molecule in an amount sufficient to provide from one to three silicon-bonded hydrogen atoms per alkenyl group in components (A) and (B) combined; (D) an adhesion promoter in an amount sufficient to effect adhesion of the composition to a substrate; and (E) a hydrosilylation catalyst in an amount sufficient to cure the composition.
摘要翻译：一种硅氧烷组合物，其包含（A）100重量份的每分子平均具有至少两个硅键合的烯基的聚二有机硅氧烷; （B）75〜150重量份的数均分子量为2,000〜5,000的有机聚硅氧烷树脂，其基本上由R32R4SiO + E，1/2 + EE单元和SiO 4/2单元构成，其中每个R 3为独立地选自单价烃和不含脂肪族不饱和键的一价卤代烃基，R4选自R3和烯基，R32R4SiO + E，fra1 / 2 + EE单元与SiO4 / 2单位为0.6:1至1.1:1，并且所述树脂含有平均2.5至7.5摩尔％的烯基; （C）每分子平均具有至少三个与硅键合的氢原子的有机氢聚硅氧烷，其量足以在组合物（A）和（B）中每个烯基上提供一至三个与硅键合的氢原子; （D）粘合促进剂，其量足以使组合物与基材粘合; 和（E）足以固化组合物的量的氢化硅烷化催化剂。

5. 发明授权

US5861450A Organic polymers modified with thermoplastic silicone blends 失效
标题翻译：用热塑性硅酮共混物改性的有机聚合物
公开(公告)号：US5861450A
公开(公告)日：1999-01-19
申请号：US705105
申请日：1996-08-28
申请人： Wei Chen , Kevin Edward Lupton , David Joseph Romenesko , Randall Gene Schmidt , Hongxi Zhang
发明人： Wei Chen , Kevin Edward Lupton , David Joseph Romenesko , Randall Gene Schmidt , Hongxi Zhang
IPC分类号： C08L23/00 , C08L23/02 , C08L33/06 , C08L39/02 , C08L67/02 , C08L75/04 , C08L77/00 , C08L83/04 , C08L101/00 , C08K5/24
CPC分类号： C08L23/02 , C08L101/00 , C08L23/06 , C08L77/00
摘要： An additive to improve the hydrophobicity of a thermoplastic resin wherein the additive is at least 0.3 parts by weight of a thermoplastic silicone blend, said thermoplastic silicone blend having:(A) an organosilicone resin of the empirical formula(R.sub.3 Sio.sub.1/2)a (R.sub.2 SiO.sub.2/2)b (RSiO.sub.3/2)c( SiO.sub.4/2)dwherein: a and d are positive numerical values and b and c are zero or positive numerical values with the provisos that a+b+c+d=1, 0.ltoreq.(b+c).ltoreq.0.2 and the ratio of a:(b+c+d) is between about 0.3 and 1.0; and R is a monovalent radical independently selected from the group consisting of hydrogen, hydroxyl, alkyl, alkenyl, alkoxy, oximo, aryl, epoxide, carboxyl, ether, polyether, amide and alkyl amino radicals, which R groups may be the same or different, with the proviso that at least sixty mole percent of said R radicals are methyl; and(B) a predominantly linear silicone fluid having the empirical formula(R'.sub.3 SiO.sub.1/2)x (R'.sub.2 SiO.sub.2/2)y (R'SiO.sub.3/2)zwherein: x and y are positive numerical values and z is 0 or a positive numerical value with the provisos that x+y+z=1, y/(x+y+z).gtoreq.0.8; and R' is a monovalent radical independently selected from the group consisting of hydroxyl and alkyl radicals, which R' groups may be the same or different, with the proviso that at least sixty mole percent of said R' radicals are methyl;said organosilicone resin (A) and said predominantly linear silicone fluid (B) being present in relative amounts such that said blends have a dynamic shear modulus (G*), measured at a frequency of 10 radians/sec, of at least 5.times.10.sup.7 dyne/cm.sup.2 at temperatures less than said predetermined maximum storage temperature.
摘要翻译：一种用于改善热塑性树脂的疏水性的添加剂，其中所述添加剂为至少0.3重量份的热塑性硅氧烷共混物，所述热塑性硅氧烷共混物具有：（A）经验式（R3Si1 / 2）a的有机硅氧烷树脂（R2SiO2 / 2）b（RSiO3 / 2）c（SiO4 / 2）d其中a和d为正数值，b和c为零或正数值，条件是a + b + c + d = /=(b+c) = 0.8; 并且R'是独立地选自羟基和烷基的一价基团，R'基团可以相同或不同，条件是至少60摩尔％的所述R'基团是甲基; 所述有机硅氧烷树脂（A）和所述主要线性硅氧烷流体（B）以相对的量存在，使得所述共混物的动态剪切模量（G *）以10弧度/秒的频率测量为至少5×10 7达因/ cm2，在低于所述预定最大存储温度的温度下。

6. 发明授权

US5844031A Method of dispersing silicone compositions in organic thermoplastic materials 失效
标题翻译：将有机硅组合物分散在有机热塑性材料中的方法
公开(公告)号：US5844031A
公开(公告)日：1998-12-01
申请号：US704061
申请日：1996-08-28
申请人： Wei Chen , Hongxi Zhang , Kevin Edward Lupton , David Joseph Romenesko , Randall Gene Schmidt
发明人： Wei Chen , Hongxi Zhang , Kevin Edward Lupton , David Joseph Romenesko , Randall Gene Schmidt
IPC分类号： C08J3/07 , C08L23/00 , C08L83/04 , C08L101/00 , C08K5/24
CPC分类号： C08L83/04 , C08G77/12 , C08G77/14 , C08G77/16 , C08G77/18 , C08G77/20 , C08G77/26 , C08G77/46 , C08G77/70 , C08G77/80
摘要： A method of dispersing silicone compositions in organic thermoplastic materials is disclosed. The novel compositions produced by the method of the invention have a fine and relatively uniform dispersion or organosilicone in an organic thermoplastic. An organosilicone resin (A) and a predominantly linear silicone fluid (B) are first blended to substantial homogeneity to form an organosilicone alloy therefrom. The organosilicone alloy exhibits thermoplastic behavior and has a temperature-dependent complex viscosity .eta.*.sub.Si (T) associated therewith. Likewise the organic thermoplastic materials have a temperature-dependent complex viscosity, .eta.*.sub.OTP (T), associated therewith. The organic thermoplastic and the organosilicone alloy are thereafter mixed at a predetermined mixing temperature, T.sub.m, and a predetermined shear strain rate. The organic thermoplastic material and the organosilicone alloy are both in a flowable state at T.sub.m. The value of T.sub.m is selected to be about .+-.30.degree. C. of a temperature, T.sub.0, wherein the absolute value of {72*.sub.OTP (T.sub.0)-.eta.*.sub.Si (T.sub.0)} is at its lowest value, at the predetermined shear strain rate.
摘要翻译：公开了将有机硅组合物分散在有机热塑性材料中的方法。通过本发明的方法生产的新型组合物在有机热塑性塑料中具有精细且相对均匀的分散体或有机硅氧烷。首先将有机硅氧烷树脂（A）和主要为线性的硅氧烷流体（B）进行共混，从而形成有机硅氧烷合金。有机硅合金表现出热塑性，并具有与之相关的温度依赖性复数粘度ηa（T）。类似地，有机热塑性材料具有与之相关的温度依赖性复合物粘度eta * OTP（T）。然后将有机热塑性塑料和有机硅合金以预定的混合温度Tm和预定的剪切应变速率混合。有机热塑性材料和有机硅合金在Tm处于可流动状态。选择Tm的值为约+/- 30℃的温度T0，其中{72 * OTP（T0） - eta * Si（T0）}的绝对值处于其最低值，在预定的剪切应变速率。

7. 发明申请

US20130284265A1 WAVELENGTH CONVERSION PERYLENE DIESTER CHROMOPHORES AND LUMINESCENT FILMS 有权
标题翻译：波长转换周期性染料和发光膜
公开(公告)号：US20130284265A1
公开(公告)日：2013-10-31
申请号：US13978370
申请日：2012-01-04
申请人： Zongcheng Jiang , Rachwal Bogumila , Hongxi Zhang , Peng Wang , Michiharu Yamamoto , Shuangxi Wang
发明人： Zongcheng Jiang , Rachwal Bogumila , Hongxi Zhang , Peng Wang , Michiharu Yamamoto , Shuangxi Wang
IPC分类号： H01L31/0216
CPC分类号： H01L31/02168 , C09B3/14 , C09K11/06 , C09K2211/1011 , H01L51/0055 , Y02E10/52
摘要： This invention is related to novel perylene diester derivatives represented by the general formula (I) or general formula (II) as described herein. The derivatives are useful in various applications, such as luminescent dyes for optical light collection systems, fluorescence-based solar collectors, fluorescence-activated displays, and/or single-molecule spectroscopy. The invention also relates to a luminescent medium, such as a luminescent film, that can significantly enhance the solar harvesting efficiency of thin film CdS/CdTe or CIGS solar cells. The luminescent medium comprises an optically transparent polymer matrix and at least one luminescent dye that comprises a perylene diester derivative. Over 16% of an efficiency enhancement to a CdS/CdTe solar cell and over 12% of an efficiency enhancement to a CIGS solar cell can be achieved.
摘要翻译：本发明涉及由本文所述的通式（I）或通式（II）表示的新型苝二酯衍生物。该衍生物可用于各种应用，例如用于光学收集系统的发光染料，基于荧光的太阳能收集器，荧光激活显示器和/或单分子光谱学。本发明还涉及可以显着提高薄膜CdS / CdTe或CIGS太阳能电池的太阳能收集效率的发光介质，例如发光膜。发光介质包括光学透明的聚合物基质和包含苝二酯衍生物的至少一种发光染料。可以实现对CdS / CdTe太阳能电池的超过16％的效率增强和对CIGS太阳能电池的效率提高的超过12％。

8. 发明授权

US07658111B2 Sensors with high temperature piezoelectric ceramics 失效
标题翻译：高温压电陶瓷传感器
公开(公告)号：US07658111B2
公开(公告)日：2010-02-09
申请号：US11941785
申请日：2007-11-16
申请人： Hongxi Zhang
发明人： Hongxi Zhang
IPC分类号： G01L9/08
CPC分类号： G01L23/10 , C01G29/006 , C01G33/006 , C01G35/006 , C01G39/006 , C01G41/006 , C01G49/009 , C01P2002/50 , C01P2006/32 , C01P2006/40 , C04B35/495 , C04B2235/3208 , C04B2235/3251 , C04B2235/3256 , C04B2235/3258 , C04B2235/3298 , C04B2235/76 , C04B2235/77 , C04B2235/81 , G01P15/0907 , H01L41/1132 , H01L41/187
摘要： A piezoelectric sensor includes a ceramic material that has the formula of [Bi2O2][Am−1BmO3m+1], where m=2, A is mono-, di-, or tri-valent ions or a combination of them, B is transition element such as Fe3+, Ti4+, Nb5+, Ta5+, W6+, Mo6+ or a combination of them. The ceramics have high Curie temperature of 900˜940° C. The sensors claimed in the present invention utilize [Bi2O2][Am−1BmO3m+1] ceramics parts as sensing elements in various shapes and dimensions and can be used to sense force, acceleration, and pressure at very high temperatures of 600˜800° C.
摘要翻译：压电传感器包括具有[Bi 2 O 2] [Am-1BmO 3m + 1]式的陶瓷材料，其中m = 2，A是一价，二价或三价离子或它们的组合，B是转变元素如Fe3 +，Ti4 +，Nb5 +，Ta5 +，W6 +，Mo6 +或它们的组合。陶瓷具有高的居里温度为900〜940℃。本发明所要求的传感器利用[Bi 2 O 2] [Am-1BmO 3m + 1]陶瓷部件作为各种形状和尺寸的传感元件，并且可用于感测力，加速度，并在600〜800℃的非常高的温度下进行压力

9. 发明申请

US20160108310A1 WAVELENGTH CONVERSION FILMS WITH MULTIPLE PHOTOSTABLE ORGANIC CHROMOPHORES 审中-公开
标题翻译：波长变换膜与多种可见光有机色素
公开(公告)号：US20160108310A1
公开(公告)日：2016-04-21
申请号：US14768959
申请日：2014-03-25
申请人： Tao GU , Hongxi ZHANG , Weiping LIN , Wan-Yun HSIEH , Michiharu YAMAMOTO , NITTO DENKO CORPORATION
发明人： Tao Gu , Hongxi Zhang , Weiping Lin , Wan-Yun Hsieh , Michiharu Yamamoto
IPC分类号： C09K11/06 , H01L31/055
CPC分类号： C09K11/06 , A01G9/1438 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , C09K2211/1029 , C09K2211/1051 , C09K2211/1059 , H01L31/055 , Y02A40/252 , Y02B10/12 , Y02E10/52 , Y02P60/124
摘要： Described herein are wavelength conversion films which utilize photostable organic chromophores. In some embodiments, wavelength conversion films and chromophores exhibit improved photostability. In some embodiments, a wavelength conversion film comprising luminescent compounds is useful for improving the solar harvesting efficiency of solar cells, solar panels, or photovoltaic devices. In some embodiments, a wavelength conversion film comprising multiple luminescent compounds is useful for greenhouse roofs. Some embodiments provide an improved solar light wavelength profile for improved plant nutrition and/or growth.
摘要翻译：这里描述了利用光稳定有机发色团的波长转换膜。在一些实施方案中，波长转换膜和发色团表现出改善的光稳定性。在一些实施例中，包含发光化合物的波长转换膜可用于改善太阳能电池，太阳能电池板或光伏器件的太阳能收集效率。在一些实施例中，包含多种发光化合物的波长转换膜可用于温室屋顶。一些实施例提供改进的太阳光波长分布，用于改善植物营养和/或生长。

10. 发明授权

US09287419B2 Wavelength conversion perylene diester chromophores and luminescent films 有权
标题翻译：波长转换苝二酯发色团和发光膜
公开(公告)号：US09287419B2
公开(公告)日：2016-03-15
申请号：US13978370
申请日：2012-01-04
申请人： Zongcheng Jiang , Bogumila Rachwal , Hongxi Zhang , Peng Wang , Michiharu Yamamoto , Shuangxi Wang
发明人： Zongcheng Jiang , Bogumila Rachwal , Hongxi Zhang , Peng Wang , Michiharu Yamamoto , Shuangxi Wang
IPC分类号： H01L51/00 , H01L31/0216 , C09B3/14 , C09K11/06
CPC分类号： H01L31/02168 , C09B3/14 , C09K11/06 , C09K2211/1011 , H01L51/0055 , Y02E10/52
摘要： This invention is related to novel perylene diester derivatives represented by the general formula (I) or general formula (II) as described herein. The derivatives are useful in various applications, such as luminescent dyes for optical light collection systems, fluorescence-based solar collectors, fluorescence-activated displays, and/or single-molecule spectroscopy. The invention also relates to a luminescent medium, such as a luminescent film, that can significantly enhance the solar harvesting efficiency of thin film CdS/CdTe or CIGS solar cells. The luminescent medium comprises an optically transparent polymer matrix and at least one luminescent dye that comprises a perylene diester derivative. Over 16% of an efficiency enhancement to a CdS/CdTe solar cell and over 12% of an efficiency enhancement to a CIGS solar cell can be achieved.
摘要翻译：本发明涉及由本文所述的通式（I）或通式（II）表示的新型苝二酯衍生物。该衍生物可用于各种应用，例如用于光学收集系统的发光染料，基于荧光的太阳能收集器，荧光激活显示器和/或单分子光谱学。本发明还涉及可以显着提高薄膜CdS / CdTe或CIGS太阳能电池的太阳能收集效率的发光介质，例如发光膜。发光介质包括光学透明的聚合物基质和包含苝二酯衍生物的至少一种发光染料。可以实现对CdS / CdTe太阳能电池的超过16％的效率增强和对CIGS太阳能电池的效率提高的超过12％。

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