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1. 发明申请

US20100160516A1 FLAME RETARDANT HALOGENATED PHENYL ETHER BLENDS 有权
标题翻译：阻燃剂HALOGENATED PHENYL ETHER BLENDS
公开(公告)号：US20100160516A1
公开(公告)日：2010-06-24
申请号：US12624497
申请日：2009-11-24
申请人： Larry D. Timberlake , James D. Siebecker
发明人： Larry D. Timberlake , James D. Siebecker
IPC分类号： C08K5/06 , C09K21/08
CPC分类号： C08K5/06 , C08K2201/014
摘要： A flame retardant blend comprises at least first and second halogenated non-polymeric phenyl ethers having the general formula (I): wherein each X is independently Cl or Br, each m is independently an integer of 1 to 5, each p is independently an integer of 1 to 4, n is an integer of 1 to 5 and wherein the values of n for the first and second ethers are different
摘要翻译：阻燃混合物包含至少具有通式（I）的第一和第二卤化非聚合苯基醚：其中每个X独立地为Cl或Br，每个m独立地为1至5的整数，每个p独立地为整数为1至4，n为1至5的整数，并且其中第一和第二醚的n值不同

2. 发明申请

US20120065297A1 FLAME RETARDANT HALOGENATED PHENYL ETHERS 有权
标题翻译：阻燃剂HALOGENATED PHENYL ETHERS
公开(公告)号：US20120065297A1
公开(公告)日：2012-03-15
申请号：US13248387
申请日：2011-09-29
申请人： Larry D. Timberlake , James D. Siebecker , Subramaniam Narayan
发明人： Larry D. Timberlake , James D. Siebecker , Subramaniam Narayan
IPC分类号： C08K5/136 , C08L55/02 , C08L69/00 , C07C43/29 , C08L67/00 , C08L79/00 , C08L63/00 , C08L25/06 , C08L23/02
CPC分类号： C07C43/29 , C08K5/06
摘要： A halogenated non-polymeric phenyl ether flame retardant is described having the general formula (I): wherein each X is independently Cl or Br, n is an integer of 1 or 2, and each p is independently an integer of 1 to 4, provided that, when each X is Cl, the total amount halogen in the ether is from about 50 to about 65 wt % and when each X is Br, the total amount halogen in the ether is from at least 70 wt % to about 79 wt % and wherein from about 30% to about 80%, for example from about 35% to about 75% of the halogenated ethers are fully halogenated the remainder being partially halogenated. The present flame retardant provides superior mechanical properties when incorporated into a polymer than similar flame retardants which contain a higher amount of fully halogenated species.
摘要翻译：描述了具有通式（I）的卤化非聚合苯基醚阻燃剂：其中每个X独立地为Cl或Br，n为1或2的整数，并且各p独立地为1至4的整数，当每个X为Cl时，醚中的卤素总量为约50至约65重量％，并且当每个X为Br时，醚中卤素的总量为至少70重量％至约79重量％并且其中约30％至约80％，例如约35％至约75％的卤代醚被完全卤化，其余部分被部分卤化。当掺入到聚合物中时，本发明的阻燃剂具有比含有更多量的完全卤化物质的类似阻燃剂优异的机械性能。

3. 发明授权

US07691954B2 Process for controlling the molecular weight of polymers of bromostyrenes 有权
标题翻译：控制溴苯乙烯聚合物分子量的方法
公开(公告)号：US07691954B2
公开(公告)日：2010-04-06
申请号：US12467682
申请日：2009-05-18
申请人： Wayne Meyer , Jennifer L. Bohan , Larry D. Timberlake , James D. Siebecker
发明人： Wayne Meyer , Jennifer L. Bohan , Larry D. Timberlake , James D. Siebecker
IPC分类号： C08F2/38 , C08F112/04
CPC分类号： C08F12/32 , C08F8/20 , C08F8/22 , C08F12/16 , C08F112/08 , C08F112/14 , C08F212/14 , C08F220/32 , C08K7/14 , C08L25/18 , C08L77/00 , C08F12/08 , C08L2666/06 , C08L2666/04
摘要： A controlled molecular weight polymer of styrene is provided having bromine substituted thereon. Control of molecular weight is achieved by the use of alpha-methyl styrene dimer as a chain transfer agent. The brominated polymer of styrene is useful as a flame retardant, particularly for polyamides giving improved properties including color retention after molding.
摘要翻译：提供苯乙烯的受控分子量聚合物，其上取代有溴。通过使用α-甲基苯乙烯二聚体作为链转移剂来实现分子量的控制。苯乙烯的溴化聚合物可用作阻燃剂，特别是用于聚酰胺，其具有改善的性能，包括成型后的保色性。

4. 发明申请

US20090227753A1 PROCESS FOR CONTROLLING THE MOLECULAR WEIGHT OF POLYMERS OF BROMOSTYRENES 有权
标题翻译：用于控制BROMOSRENES聚合物分子量的方法
公开(公告)号：US20090227753A1
公开(公告)日：2009-09-10
申请号：US12467682
申请日：2009-05-18
申请人： Wayne MEYER , Jennifer L. Bohan , Larry D. Timberlake , James D. Siebecker
发明人： Wayne MEYER , Jennifer L. Bohan , Larry D. Timberlake , James D. Siebecker
IPC分类号： C08F12/16
CPC分类号： C08F12/32 , C08F8/20 , C08F8/22 , C08F12/16 , C08F112/08 , C08F112/14 , C08F212/14 , C08F220/32 , C08K7/14 , C08L25/18 , C08L77/00 , C08F12/08 , C08L2666/06 , C08L2666/04
摘要： A controlled molecular weight polymer of styrene is provided having bromine substituted thereon. Control of molecular weight is achieved by the use of alpha-methyl styrene dimer as a chain transfer agent. The brominated polymer of styrene is useful as a flame retardant, particularly for polyamides giving improved properties including color retention after molding.
摘要翻译：提供苯乙烯的受控分子量聚合物，其上取代有溴。通过使用α-甲基苯乙烯二聚体作为链转移剂来实现分子量的控制。苯乙烯的溴化聚合物可用作阻燃剂，特别是用于聚酰胺，其具有改善的性能，包括成型后的保色性。

5. 发明授权

US08158038B2 Flame retardant halogenated polymer compositions 有权
标题翻译：阻燃卤化聚合物组合物
公开(公告)号：US08158038B2
公开(公告)日：2012-04-17
申请号：US12909923
申请日：2010-10-22
申请人： Larry D. Timberlake , James D. Siebecker
发明人： Larry D. Timberlake , James D. Siebecker
IPC分类号： C09K21/00
CPC分类号： C09K21/08 , C07C43/29 , C08K5/0066 , C08K5/06
摘要： A halogenated aryl ether oligomer is formed by halogenation of an aryl ether oligomer and is useful as a flame retardant for flammable macromolecular materials. Typically, the halogenated aryl ether oligomer comprises the following repeating monomeric units: wherein R is hydrogen or alkyl, especially C1 to C4 alkyl, Hal is halogen, m is at least 1, n is 0 to 3 and x is at least 2.
摘要翻译：通过芳基醚低聚物的卤化形成卤代芳基醚低聚物，并且可用作易燃大分子材料的阻燃剂。通常，卤代芳基醚低聚物包含以下重复单体单元：其中R是氢或烷基，特别是C1至C4烷基，Hal是卤素，m是至少1，n是0-3，x是至少2。

6. 发明申请

US20090221754A1 POLYMER COMPOSITIONS OF BROMOSTYRENES HAVING CONTROLLED MOLECULAR WEIGHT 有权
标题翻译：具有控制分子量的硼烷的聚合物组合物
公开(公告)号：US20090221754A1
公开(公告)日：2009-09-03
申请号：US12467667
申请日：2009-05-18
申请人： Wayne Meyer , Jennifer L. Bohan , Larry D. Timberlake , James D. Siebecker
发明人： Wayne Meyer , Jennifer L. Bohan , Larry D. Timberlake , James D. Siebecker
IPC分类号： C08L77/00
CPC分类号： C08F12/32 , C08F8/20 , C08F8/22 , C08F12/16 , C08F112/08 , C08F112/14 , C08F212/14 , C08F220/32 , C08K7/14 , C08L25/18 , C08L77/00 , C08F12/08 , C08L2666/06 , C08L2666/04
摘要： A controlled molecular weight polymer of styrene is provided having bromine substituted thereon. Control of molecular weight is achieved by the use of alphα-methyl styrene dimer as a chain transfer agent. The brominated polymer of styrene is useful as a flame retardant, particularly for polyamides giving improved properties including color retention after molding.
摘要翻译：提供苯乙烯的受控分子量聚合物，其上取代有溴。通过使用α-甲基苯乙烯二聚体作为链转移剂来实现分子量的控制。苯乙烯的溴化聚合物可用作阻燃剂，特别是用于聚酰胺，其具有改善的性能，包括成型后的保色性。

7. 发明申请

US20080015394A1 Process for higher purity decabromodiphenyl oxide 审中-公开
标题翻译：高纯度十溴二苯醚的工艺
公开(公告)号：US20080015394A1
公开(公告)日：2008-01-17
申请号：US11827172
申请日：2007-07-10
申请人： Steven Bakeis , David W. Bartley , Stephen B. Falloon , Timothy T. Lawlor , David C. Sanders , James D. Siebecker , Larry D. Timberlake
发明人： Steven Bakeis , David W. Bartley , Stephen B. Falloon , Timothy T. Lawlor , David C. Sanders , James D. Siebecker , Larry D. Timberlake
IPC分类号： C07C41/00
CPC分类号： C07C41/22 , C07C43/29
摘要： A process for substantially perbrominating diphenyl ether comprising the steps of: (A) adding the diphenyl ether to a mixture of: (i) a greater than 400 percent excess of the stoichiometric amount of bromine; and (ii) a catalytically effective amount of a Lewis acid catalyst; (B) heating said mixture to an elevated temperature during the addition; and (C) continuing the reaction at an elevated temperature after addition of the aromatic compound has been completed.
摘要翻译：包括以下步骤的基本上每二溴二苯醚的方法：（A）将二苯醚加入到以下混合物中：（i）大于400％过量的化学计量量的溴; 和（ii）催化有效量的路易斯酸催化剂; （B）在添加期间将所述混合物加热至升高的温度; 和（C）在加入芳族化合物之后在升高的温度下继续反应已经完成。

8. 发明授权

US08357738B2 Flame retardant halogenated phenyl ether blends 有权
标题翻译：阻燃卤化苯基醚共混物
公开(公告)号：US08357738B2
公开(公告)日：2013-01-22
申请号：US12624497
申请日：2009-11-24
申请人： Larry D. Timberlake , James D. Siebecker
发明人： Larry D. Timberlake , James D. Siebecker
IPC分类号： C08K5/06
CPC分类号： C08K5/06 , C08K2201/014
摘要： A flame retardant blend comprises at least first and second halogenated non-polymeric phenyl ethers having the general formula (I): wherein each X is independently Cl or Br, each m is independently an integer of 1 to 5, each p is independently an integer of 1 to 4, n is an integer of 1 to 5 and wherein the values of n for the first and second ethers are different.
摘要翻译：阻燃混合物包含至少具有通式（I）的第一和第二卤化非聚合苯基醚：其中每个X独立地为Cl或Br，每个m独立地为1至5的整数，每个p独立地为整数为1至4，n为1至5的整数，并且其中第一和第二醚的n值不同。

9. 发明授权

US07691947B2 Polymer compositions of bromostyrenes having controlled molecular weight 有权
标题翻译：具有受控分子量的溴苯乙烯的聚合物组成
公开(公告)号：US07691947B2
公开(公告)日：2010-04-06
申请号：US12467667
申请日：2009-05-18
申请人： Wayne Meyer , Jennifer L. Bohan , Larry D. Timberlake , James D. Siebecker
发明人： Wayne Meyer , Jennifer L. Bohan , Larry D. Timberlake , James D. Siebecker
IPC分类号： C08L25/18 , C08L77/00 , C08F2/38
CPC分类号： C08F12/32 , C08F8/20 , C08F8/22 , C08F12/16 , C08F112/08 , C08F112/14 , C08F212/14 , C08F220/32 , C08K7/14 , C08L25/18 , C08L77/00 , C08F12/08 , C08L2666/06 , C08L2666/04
摘要： A controlled molecular weight polymer of styrene is provided having bromine substituted thereon. Control of molecular weight is achieved by the use of alpha-methyl styrene dimer as a chain transfer agent. The brominated polymer of styrene is useful as a flame retardant, particularly for polyamides giving improved properties including color retention after molding.
摘要翻译：提供苯乙烯的受控分子量聚合物，其上取代有溴。通过使用α-甲基苯乙烯二聚体作为链转移剂来实现分子量的控制。苯乙烯的溴化聚合物可用作阻燃剂，特别是用于聚酰胺，其具有改善的性能，包括成型后的保色性。

10. 发明授权

US08362127B2 Flame retardant halogenated phenyl ethers 有权
标题翻译：阻燃卤化苯基醚
公开(公告)号：US08362127B2
公开(公告)日：2013-01-29
申请号：US13248387
申请日：2011-09-29
申请人： Larry D. Timberlake , James D. Siebecker , Subramaniam Narayan
发明人： Larry D. Timberlake , James D. Siebecker , Subramaniam Narayan
IPC分类号： C08K5/06
CPC分类号： C07C43/29 , C08K5/06
摘要： A halogenated non-polymeric phenyl ether flame retardant is described having the general formula (I): wherein each X is independently Cl or Br, n is an integer of 1 or 2, and each p is independently an integer of 1 to 4, provided that, when each X is Cl, the total amount halogen in the ether is from about 50 to about 65 wt % and when each X is Br, the total amount halogen in the ether is from at least 70 wt % to about 79 wt % and wherein from about 30% to about 80%, for example from about 35% to about 75% of the halogenated ethers are fully halogenated the remainder being partially halogenated. The present flame retardant provides superior mechanical properties when incorporated into a polymer than similar flame retardants which contain a higher amount of fully halogenated species.
摘要翻译：描述了具有通式（I）的卤化非聚合苯基醚阻燃剂：其中每个X独立地为Cl或Br，n为1或2的整数，并且各p独立地为1至4的整数，当每个X为Cl时，醚中的卤素总量为约50至约65重量％，并且当每个X为Br时，醚中卤素的总量为至少70重量％至约79重量％并且其中约30％至约80％，例如约35％至约75％的卤代醚被完全卤化，其余部分被部分卤化。当掺入到聚合物中时，本发明的阻燃剂具有比含有更多量的完全卤化物质的类似阻燃剂优异的机械性能。

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