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1. 发明授权

US5036117A Heat-curable silicone compositions having improved bath life 失效
标题翻译：具有改善浴寿命的可热固化硅氧烷组合物
公开(公告)号：US5036117A
公开(公告)日：1991-07-30
申请号：US431352
申请日：1989-11-03
申请人： Kyuha Chung , Antony P. Wright , Ming-Hsiung Yeh
发明人： Kyuha Chung , Antony P. Wright , Ming-Hsiung Yeh
IPC分类号： B32B7/06 , B32B7/12 , C08F2/46 , C08K3/18 , C08K5/05 , C08K5/06 , C08K5/09 , C08K5/11 , C08L83/04 , C08L83/05 , C08L83/06 , C08L83/07 , C09D183/04 , C09D183/05 , C09D183/06 , C09D183/07 , C09J7/02
CPC分类号： C08L83/04 , C09D183/04 , C08G77/12 , C08G77/16 , C08G77/24
摘要： A curable organosilicon composition comprises a component having silicon-bonded hydrogen atoms, a component having silicon-bonded radicals reactive therewith, a curing catalyst, a catalyst-inhibitor and a bath life extender. The use of certain compounds, which are ineffective as a bath life extender in the absence of a catalyst inhibitor, effectively extend the room temperature bath life of a silicone coating composition containing a catalyst inhibitor. Being a substantial non-inhibitor for the catalyst the bath life extender component does not effect the cure time and/or cure temperature of the composition.This discovery has permitted the preparation of curable coating compositions which have a long bath life at room temperature and a rapid cure time at elevated temperatures which does not drift to longer intervals as the coating compositions ages over a typical production run.The room temperature cure times of the organopolysiloxane coating compositions of this invention are adequately long, and their cure times at elevated temperature are advantageously brief, that they are useful in fast-paced coating operations, such as adhesive release coating operations wherein the cured coating is further coated with an adhesive in-line, i.e., immediately after being cured.

2. 发明授权

US5108791A Heat-curable silicone compositions having improved bath life 失效
标题翻译：具有改善的浴寿命的可热固化的有机硅组合物
公开(公告)号：US5108791A
公开(公告)日：1992-04-28
申请号：US677938
申请日：1991-04-01
申请人： Kyuha Chung , Antony P. Wright , Ming-Hsiung Yeh
发明人： Kyuha Chung , Antony P. Wright , Ming-Hsiung Yeh
IPC分类号： C08L83/04 , C09D183/04
CPC分类号： C08L83/04 , C09D183/04
摘要： A curable organosilicon composition comprises a component having silicon-bonded hydrogen atoms, a component having silicon-bonded radicals reactive therewith, a curing catalyst, a catalyst-inhibitor and a bath life extender. The use of certain compounds, which are ineffective as a bath life extender in the absence of a catalyst inhibitor, effectively extend the room temperature bath life of a silicone coating composition containing a catalyst inhibitor. Being a substantial non-inhibitor for the catalyst the bath life extender component does not effect the cure time and/or cure temperature of the composition.This discovery has permitted the preparation of curable coating compositions which have a long bath life at room temperature and a rapid cure time at elevated temperatures which does not drift to longer intervals as the coating compositions ages over a typical production run.The room temperature cure times of the organopolysiloxane coating compositions of this invention are adequately long, and their cure times at elevated temperature are advantageously brief, that they are useful in fast-paced coating operations, such as adhesive release coating operations wherein the cured coating is further coated with an adhesive in-line, i.e., immediately after being cured.
摘要翻译：可固化的有机硅组合物包含具有与硅键合的氢原子的组分，具有与其反应的硅键合基团的组分，固化催化剂，催化剂抑制剂和浴寿命延长剂。在不存在催化剂抑制剂的情况下，使用无效作为浴寿命延长剂的某些化合物有效地延长了含有催化剂抑制剂的硅氧烷涂料组合物的室温浴寿命。作为催化剂的实质性非抑制剂，浴寿命延长剂组分不影响组合物的固化时间和/或固化温度。该发现允许制备在室温下具有长浴槽寿命和在高温下快速固化时间的可固化涂料组合物，其在涂料组合物比典型的生产流程老化时不会漂移到更长的间隔。本发明的有机聚硅氧烷涂料组合物的室温固化时间足够长，并且它们在升高的温度下的固化时间有利地是短暂的，它们可用于快速进行的涂布操作，例如粘合剂剥离涂覆操作，其中固化涂层为进一步用粘合剂在线涂布，即在固化后立即进行。

3. 发明授权

US5087716A Novel synthesis of difunctional halo organo noncarbon group IV main group element amides 失效
标题翻译：双官能卤代有机非芳族IV族主要元素酰胺的合成
公开(公告)号：US5087716A
公开(公告)日：1992-02-11
申请号：US607194
申请日：1990-12-24
申请人： Antony P. Wright , Padmakumari J. Varaprath
发明人： Antony P. Wright , Padmakumari J. Varaprath
IPC分类号： C07F7/12 , C07F7/22 , C07F7/30 , C07F9/06 , C07F9/26 , C07F9/44 , C07F9/46 , C07F9/535 , C07F19/00 , D21H19/32 , G03F7/075
CPC分类号： G03F7/0755 , C07F19/005 , C07F7/123 , C07F7/2216 , C07F7/30 , C07F9/065 , C07F9/26 , C07F9/4465 , C07F9/46 , C07F9/535 , D21H19/32
摘要： Difunctional halo silicon amide compounds are prepared by cleaving the nitrogen-silicon bond in a nitrogen-silicon heterocycle with a reactive halide. The reaction is straight forward with no intermediates or byproducts. The halo functionality is capable of capping any SiOH group. When the other functionality is an acrylamide, the capped entity may be polymerized or crosslinked by free radical initiators of the acrylamide functionality thereby producing useful products such as paper release coatings and photoresists.
摘要翻译：通过用反应性卤化物裂解氮 - 硅杂环中的氮 - 硅键来制备二官能卤代硅酰胺化合物。反应是直接的，没有中间体或副产物。卤素官能团能够覆盖任何SiOH基团。当其它官能团是丙烯酰胺时，封端的实体可以由丙烯酰胺官能团的自由基引发剂聚合或交联，从而产生有用的产物，例如剥离涂层和光致抗蚀剂。

4. 发明授权

US5082958A Novel synthesis of difunctional halo organo noncarbon group IV main group element amides 失效
标题翻译：多功能HALO ORGANO NONCARBON第四组主要组件元素的新合成
公开(公告)号：US5082958A
公开(公告)日：1992-01-21
申请号：US467868
申请日：1990-01-22
申请人： Antony P. Wright , Padmakumari J. Varaprath
发明人： Antony P. Wright , Padmakumari J. Varaprath
IPC分类号： C07F7/12 , C07F7/22 , C07F7/30 , C07F9/06 , C07F9/26 , C07F9/44 , C07F9/46 , C07F9/535 , C07F19/00 , D21H19/32 , G03F7/075
CPC分类号： G03F7/0755 , C07F19/005 , C07F7/123 , C07F7/2216 , C07F7/30 , C07F9/065 , C07F9/26 , C07F9/4465 , C07F9/46 , C07F9/535 , D21H19/32
摘要： Difunctional halo silicon amide compounds are prepared by cleaving the nitrogen-silicon bond in a nitrogen-silicon heterocycle with a reactive halide. The reaction is straight forward with no intermediates or byproducts. The halo functionality is capable of capping any SiOH group. When the other functionality is an acrylamide, the capped entity may be polymerized or crosslinked by free radical initiators of the acrylamide functionality thereby producing useful products such as paper release coatings and photoresists.

5. 发明授权

US4732996A Treatment of alkoxysilanes 失效
标题翻译：烷氧基硅烷的处理
公开(公告)号：US4732996A
公开(公告)日：1988-03-22
申请号：US13742
申请日：1987-02-10
申请人： Kenneth W. Moorhead , Kirsten L. Reading , David J. Rengering , Antony P. Wright
发明人： Kenneth W. Moorhead , Kirsten L. Reading , David J. Rengering , Antony P. Wright
IPC分类号： C07F7/04 , C07F7/08 , C07F7/20 , C07F7/18
CPC分类号： C07F7/20
摘要： A process in which the residual chloride impurities in crude alkoxysilanes with atmospheric boiling points below 130.degree. C. are reduced in order to render the resultant alkoxysilanes more suitable as a starting intermediate for the preparation of other chemical compounds and for use in electronics applications is described. The essence of the process is contacting the alkoxysilane with an alkaline metal compound using superatmospheric pressure to achieve a treatment temperature of greater than 130.degree. C.

6. 发明授权

US5481046A Telechelic telomers of chlorotrifluoroethylene 失效
标题翻译：三氟氯乙烯的电视派对
公开(公告)号：US5481046A
公开(公告)日：1996-01-02
申请号：US270843
申请日：1994-07-05
申请人： Richard D. Chambers , Martin P. Greenhall , Antony P. Wright
发明人： Richard D. Chambers , Martin P. Greenhall , Antony P. Wright
IPC分类号： C08F2/00 , C07C19/16 , C07C43/12 , C08F2/38 , C08F14/24 , C08F214/24 , C07C41/00 , C07C19/07
CPC分类号： C07C43/123 , C07C19/16
摘要： Iodine terminated liquid telechelic telomers of chlorotrifluoroethylene (CTFE) containing an average of more than 1 CTFE unit per molecule are novel compounds. The telomers can be prepared by a photochemically initiated reaction between liquified CTFE and either elemental iodine or the telogen ICF.sub.2 CFClI at temperatures below about 50.degree. C.
摘要翻译：每分子平均含有超过1个CTFE单位的碘三氟乙烯（CTFE）的碘终止液体遥爪调聚物是新化合物。可以通过在低于约50℃的温度下在液化的CTFE和元素碘或前体基因ICF2CF1I之间的光化学引发反应来制备调聚物。

7. 发明授权

US5260350A Radiation curable acryloxyfunctional silicone coating composition 失效
标题翻译：辐射固化丙烯酰氧基官能有机硅涂料组合物
公开(公告)号：US5260350A
公开(公告)日：1993-11-09
申请号：US839007
申请日：1992-02-14
申请人： Antony P. Wright
发明人： Antony P. Wright
IPC分类号： C08F2/44 , C08F2/46 , C08F20/10 , C08F20/20 , C08F220/20 , C08F290/00 , C08F290/06 , C08F292/00 , C08F299/08 , C08L33/04 , C08L83/07 , C09D4/00 , C09D4/02 , C09D4/06 , C09D183/08 , C09D183/10 , B32B9/04 , C08G77/04 , C08G77/26
CPC分类号： C09D4/06 , C09D183/08 , C09D183/10 , Y10T428/31507 , Y10T428/31663 , Y10T428/31667 , Y10T428/31786 , Y10T428/31855
摘要： The present invention relates to a silicone coating composition which, when cured on a solid substrate either by ultraviolet or electron beam radiation, provides a transparent abrasion resistant coating firmly adhered thereon. The silicon coating is prepared by reacting at least one multifunctional acrylate monomer with an amino-organofunctional silane, mixing the modified silane with at least one acrylic monomer and thereafter adding colloidal silica.
摘要翻译：本发明涉及一种硅氧烷涂料组合物，其通过紫外线或电子束辐射固化在固体基质上时，提供牢固粘附在其上的透明耐磨涂层。硅涂层通过使至少一种多官能丙烯酸酯单体与氨基 - 有机官能硅烷反应制备，将改性硅烷与至少一种丙烯酸单体混合，然后加入胶体二氧化硅。

8. 发明授权

US4783552A Bis(2-methoxyisopropyl) maleate 失效
标题翻译：双（2-甲氧基异丙基）马来酸酯
公开(公告)号：US4783552A
公开(公告)日：1988-11-08
申请号：US769228
申请日：1985-08-26
申请人： Peter Y. K. Lo , LeRoy E. Thayer , Antony P. Wright
发明人： Peter Y. K. Lo , LeRoy E. Thayer , Antony P. Wright
IPC分类号： C07C69/60 , C07F7/08 , C07F9/18 , C08K5/11 , C08L83/00 , C08L83/04 , C08L83/05 , C08L83/06 , C08L83/07 , C09J7/02 , D21H19/32
CPC分类号： D21H19/32 , C08L83/04 , C08G77/12 , C08G77/16 , C08G77/20 , C08G77/24 , C08G77/26
摘要： Organosilicon compositions which cure by way of a metal-catalyzed reaction of silicon-bonded hydroxyl radicals and/or silicon-bonded olefinic hydrocarbon radicals with silicon-bonded hydrogen atoms are stabilized for hours at room temperature by the incorporation of a hydrocarbonoxyalkyl maleate. However, the stabilized compositions are rapidly curable at low elevated temperature. Liquid organopolysiloxane compositions of this invention are particularly useful for coating operations, particularly paper coating operations to prepare an adhesive-releasing layer.
摘要翻译：通过硅键合的羟基自由基和/或硅键合的烯烃基团与硅键合的氢原子的金属催化反应固化的有机硅组合物通过引入马来酸烷氧基烷基酯在室温下稳定数小时。然而，稳定的组合物可在低升高的温度下快速固化。本发明的液体有机基聚硅氧烷组合物特别可用于涂布操作，特别是用于制备粘合剂释放层的纸张涂布操作。

9. 发明授权

US4758631A Method of preparing allyl-terminated polyisobutylene 失效
标题翻译：制备烯丙基封端的聚异丁烯的方法
公开(公告)号：US4758631A
公开(公告)日：1988-07-19
申请号：US919529
申请日：1986-10-16
申请人： Joseph P. Kennedy , Donald R. Weyenberg , Lech Wilczek , Antony P. Wright
发明人： Joseph P. Kennedy , Donald R. Weyenberg , Lech Wilczek , Antony P. Wright
IPC分类号： C08F8/02 , C08F2/38 , C08F8/42 , C08F10/10 , C08F210/10 , C08F275/00
CPC分类号： C08F210/10 , C08F10/10 , C08F8/02 , C08F8/26 , C08K5/5403 , C08F2810/30 , C08F2810/40
摘要： The invention relates to a method of preparing allyl-terminated polyisobutylene (PIB) by allylation with allyltrimethylsilane of tertiary chloro-capped PIB by electrophilic substitution. The synthesis begins with the BCl.sub.3, catalyzed mono- or oligo-tertiary chloride "inifer" initiated polymerization of isobutylene, followed in the same reaction vessel by the addition of hexane, allyltrimethylsilane, and TiCl.sub.4.
摘要翻译：本发明涉及通过亲电取代与叔氯基封端的PIB的烯丙基三甲基硅烷烯化反应制备烯丙基封端的聚异丁烯（PIB）的方法。合成开始于BCl 3，催化的单或低三氯化钛“异构体”引发的异丁烯的聚合，然后通过加入己烷，烯丙基三甲基硅烷和TiCl 4在相同的反应容器中。

10. 发明授权

US4861907A Process for synthesis of acylamino silicon compounds 失效
标题翻译：合成酰基氨基硅化合物的方法
公开(公告)号：US4861907A
公开(公告)日：1989-08-29
申请号：US335612
申请日：1989-04-10
申请人： Antony P. Wright , David J. Bunge
发明人： Antony P. Wright , David J. Bunge
IPC分类号： C07F7/10 , C07F7/08 , C08G77/38 , C08G77/388
CPC分类号： C07F7/0889 , C07F7/0801 , C08G77/388
摘要： Organosilicon compounds containing at least one acylamino-substituted hydrocarbon radical are prepared by reacting an organosilicon compound containing at least one amino-substituted hydrocarbon radical with an acyl halide in a nonaqueous solvent in the presence of an aqueous alkaline material and an additive that facilitates the transfer of the alkaline material into the nonaqueous phase.

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