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1. 发明申请

US20130079269A1 METHOD FOR PRODUCING HIGH CONCENTRATION OZONATED WATER AND DEVICE FOR PRODUCING HIGH CONCENTRATION OZONATED WATER 有权
标题翻译：生产高浓度臭氧水的方法及生产高浓度臭氧水的装置
公开(公告)号：US20130079269A1
公开(公告)日：2013-03-28
申请号：US13703139
申请日：2010-11-25
申请人： Kunihiko Koike , Sadaki Nakamura , Naohisa Makihira , Koichi Izumi , Goichi Inoue , Norikazu Hohshi , Takashi Minamihonoki
发明人： Kunihiko Koike , Sadaki Nakamura , Naohisa Makihira , Koichi Izumi , Goichi Inoue , Norikazu Hohshi , Takashi Minamihonoki
IPC分类号： C11D7/04 , C01B13/11
CPC分类号： C11D7/04 , C01B13/11 , C11D3/3947
摘要： The disclosed device and method produce high concentration ozonated water by connecting a high concentration ozone gas-supplying system that comprises an ozone gas-generating unit (1) for forming ozone gas, an ozone gas-concentrating unit (2) for concentrating the ozone gas formed, a concentrated ozone gas-pressurizing unit (3) for pressurizing the concentrated ozone gas output from the ozone gas-concentrating unit (2), and a cooling mechanism (13) for cooling the concentrated ozone gas-pressurizing unit (3), to an ozone gas-dissolving unit (4) to dissolve the high pressure, concentrated ozone gas in pure water and produce the high concentration ozonated water.
摘要翻译：所公开的装置和方法通过连接包括用于形成臭氧气体的臭氧气体发生单元（1）和用于浓缩臭氧气体的臭氧气体浓缩单元（2）的高浓度臭氧气体供应系统产生高浓度臭氧水形成有用于对从臭氧气体浓缩单元（2）输出的浓缩臭氧气体进行加压的浓缩臭氧气体加压单元（3）和用于冷却浓缩臭氧气体加压单元（3）的冷却机构（13）涉及将高压浓缩臭氧气体溶解在纯水中并产生高浓度臭氧化水的臭氧气体溶解单元（4）。

2. 发明授权

US09080131B2 Method for producing high concentration ozonated water and device for producing high concentration ozonated water 有权
标题翻译：高浓度臭氧水生产方法及高浓度臭氧水生产装置
公开(公告)号：US09080131B2
公开(公告)日：2015-07-14
申请号：US13703139
申请日：2010-11-25
申请人： Kunihiko Koike , Sadaki Nakamura , Naohisa Makihira , Koichi Izumi , Goichi Inoue , Norikazu Hohshi , Takashi Minamihonoki
发明人： Kunihiko Koike , Sadaki Nakamura , Naohisa Makihira , Koichi Izumi , Goichi Inoue , Norikazu Hohshi , Takashi Minamihonoki
IPC分类号： C11D7/04 , C01B13/11 , C11D3/39
CPC分类号： C11D7/04 , C01B13/11 , C11D3/3947
摘要： The disclosed device and method produce high concentration ozonated water by connecting a high concentration ozone gas-supplying system that comprises an ozone gas-generating unit (1) for forming ozone gas, an ozone gas-concentrating unit (2) for concentrating the ozone gas formed, a concentrated ozone gas-pressurizing unit (3) for pressurizing the concentrated ozone gas output from the ozone gas-concentrating unit (2), and a cooling mechanism (13) for cooling the concentrated ozone gas-pressurizing unit (3), to an ozone gas-dissolving unit (4) to dissolve the high pressure, concentrated ozone gas in pure water and produce the high concentration ozonated water.
摘要翻译：所公开的装置和方法通过连接包括用于形成臭氧气体的臭氧气体发生单元（1）和用于浓缩臭氧气体的臭氧气体浓缩单元（2）的高浓度臭氧气体供应系统产生高浓度臭氧水形成有用于对从臭氧气体浓缩单元（2）输出的浓缩臭氧气体进行加压的浓缩臭氧气体加压单元（3）和用于冷却浓缩臭氧气体加压单元（3）的冷却机构（13）涉及将高压浓缩臭氧气体溶解在纯水中并产生高浓度臭氧化水的臭氧气体溶解单元（4）。

3. 发明授权

US08012241B2 Method and apparatus for condensing ozone gas 有权
标题翻译：用于冷凝臭氧气体的方法和装置
公开(公告)号：US08012241B2
公开(公告)日：2011-09-06
申请号：US12444649
申请日：2006-11-24
申请人： Kunihiko Koike , Sadaki Nakamura , Koichi Izumi , Goichi Inoue
发明人： Kunihiko Koike , Sadaki Nakamura , Koichi Izumi , Goichi Inoue
IPC分类号： C01B13/10 , B01D53/04
CPC分类号： C01B13/10
摘要： The present invention provides a method and an apparatus for condensing ozone arranged so as to efficiently take out the ozone gas of a predetermined concentration, although its construction is simple. The method for condensing the ozone gas comprises acting ozone-oxygen mixture gas on an adsorbing cylinder which is filled in its interior area with an adsorbent so as to selectively adsorb the ozone gas to an adsorbent and desorbing the selectively adsorbed ozone gas so as to condense and purify the ozone gas. The method further includes acting the ozone-oxygen mixture gas on the adsorbent in non-cooled state to selectively adsorb the ozone gas to the adsorbent and vacuuming the adsorbing cylinder on performing desorption-operation of the ozone gas to desorb the ozone gas from the adsorbent.
摘要翻译：本发明提供一种用于冷凝臭氧的方法和装置，其设置为有效地取出预定浓度的臭氧气体，尽管其结构简单。用于冷凝臭氧气体的方法包括在吸附筒上起作用的臭氧 - 氧混合气体，其中吸附剂填充在其内部区域中，以便选择性地将臭氧气体吸附到吸附剂上并且解吸选择性吸收的臭氧气体以便冷凝并净化臭氧气体。该方法还包括在非冷却状态下将臭氧 - 氧混合气体作用在吸附剂上，以选择性地将臭氧气体吸附到吸附剂上，并且对臭氧气体进行解吸操作以吸附臭氧气体从吸附剂中解吸吸附气缸。

4. 发明申请

US20100005961A1 METHOD AND APPARATUS FOR CONDENSING OZONE GAS 有权
标题翻译：浓缩臭氧气体的方法和装置
公开(公告)号：US20100005961A1
公开(公告)日：2010-01-14
申请号：US12444649
申请日：2006-11-24
申请人： Kunihiko Koike , Sadaki Nakamura , Koichi Izumi , Goichi Inoue
发明人： Kunihiko Koike , Sadaki Nakamura , Koichi Izumi , Goichi Inoue
IPC分类号： B01D53/047 , B01D53/02
CPC分类号： C01B13/10
摘要： The present invention provides a method and an apparatus for condensing ozone arranged so as to efficiently take out the ozone gas of a predetermined concentration, although its construction is simple. The method for condensing the ozone gas comprises acting ozone-oxygen mixture gas on an adsorbing cylinder which is filled in its interior area with an adsorbent so as to selectively adsorb the ozone gas to an adsorbent and desorbing the selectively adsorbed ozone gas so as to condense and purify the ozone gas. The method further includes acting the ozone-oxygen mixture gas on the adsorbent in non-cooled state to selectively adsorb the ozone gas to the adsorbent and vacuuming the adsorbing cylinder on performing desorption-operation of the ozone gas to desorb the ozone gas from the adsorbent.
摘要翻译：本发明提供一种用于冷凝臭氧的方法和装置，其设置为有效地取出预定浓度的臭氧气体，尽管其结构简单。用于冷凝臭氧气体的方法包括在吸附筒上加入臭氧 - 氧气混合气体，其中吸附剂填充在其内部区域中，以便选择性地将臭氧气体吸附到吸附剂上并解吸选择性吸附的臭氧气体以使其冷凝并净化臭氧气体。该方法还包括以非冷却状态将臭氧 - 氧气混合气体作用在吸附剂上，以选择性地将吸附臭氧气体吸附到吸附剂上，同时对臭氧气体进行解吸操作以吸附臭氧气体从吸附剂中解吸吸附气体。

5. 发明授权

US08945278B2 Method and apparatus for concentrating ozone gas 有权
标题翻译：浓缩臭氧气体的方法和设备
公开(公告)号：US08945278B2
公开(公告)日：2015-02-03
申请号：US13597822
申请日：2012-08-29
申请人： Naohisa Makihira , Sadaki Nakamura , Goichi Inoue , Kunihiko Koike
发明人： Naohisa Makihira , Sadaki Nakamura , Goichi Inoue , Kunihiko Koike
IPC分类号： B01D53/047 , C01B13/10
CPC分类号： B01D53/047 , B01D2253/106 , B01D2256/14 , B01D2259/40007 , B01D2259/40035 , B01D2259/402 , C01B13/10
摘要： A method of concentrating ozone gas including: causing ozone gas contained in ozone-oxygen mixture gas to be selectively adsorbed to adsorbents which are filled in a non-cooled state in at least two adsorbing cylinders arranged parallel to one another; desorbing the ozone gas from the adsorbents by subjecting a depressurizing process to each adsorbing cylinder during an ozone gas desorption operation; repeating an adsorption step and a desorption step alternately in the at least two adsorbing cylinders; and controlling the adsorbing cylinders, in such a way that one of the adsorbing cylinders is performing the adsorption step while another one of the adsorbing cylinders is performing the desorption step.
摘要翻译：一种浓缩臭氧气体的方法，包括：使包含在臭氧 - 氧气混合气体中的臭氧气体选择性地吸附在彼此平行布置的至少两个吸附气瓶中的非冷却状态的吸附剂上; 在臭氧气体解吸操作期间通过对每个吸附筒进行减压处理从吸附剂中解吸臭氧气体; 在所述至少两个吸附筒中交替地重复吸附步骤和解吸步骤; 并且以这样的方式控制所述吸附筒，使得所述吸附筒中的一个正在执行所述吸附步骤，而所述吸附缸中的另一个正在执行所述解吸附步骤。

6. 发明申请

US20130061750A1 METHOD AND APPARATUS FOR CONCENTRATING OZONE GAS 有权
标题翻译：浓缩臭氧气体的方法和装置
公开(公告)号：US20130061750A1
公开(公告)日：2013-03-14
申请号：US13597822
申请日：2012-08-29
申请人： Naohisa Makihira , Sadaki Nakamura , Goichi Inoue , Kunihiko Koike
发明人： Naohisa Makihira , Sadaki Nakamura , Goichi Inoue , Kunihiko Koike
IPC分类号： B01D53/047
CPC分类号： B01D53/047 , B01D2253/106 , B01D2256/14 , B01D2259/40007 , B01D2259/40035 , B01D2259/402 , C01B13/10
摘要： A method of concentrating ozone gas including: causing ozone gas contained in ozone-oxygen mixture gas to be selectively adsorbed to adsorbents which are filled in a non-cooled state in at least two adsorbing cylinders arranged parallel to one another; desorbing the ozone gas from the adsorbents by subjecting a depressurizing process to each adsorbing cylinder during an ozone gas desorption operation; repeating an adsorption step and a desorption step alternately in the at least two adsorbing cylinders; and controlling the adsorbing cylinders, in such a way that one of the adsorbing cylinders is performing the adsorption step while another one of the adsorbing cylinders is performing the desorption step.
摘要翻译：一种浓缩臭氧气体的方法，包括：使包含在臭氧 - 氧气混合气体中的臭氧气体选择性地吸附在彼此平行布置的至少两个吸附气瓶中的非冷却状态的吸附剂上; 在臭氧气体解吸操作期间通过对每个吸附筒进行减压处理从吸附剂中解吸臭氧气体; 在所述至少两个吸附筒中交替地重复吸附步骤和解吸步骤; 并且以这样的方式控制所述吸附筒，使得所述吸附筒中的一个正在执行所述吸附步骤，而所述吸附缸中的另一个正在执行所述解吸附步骤。

7. 发明授权

US08404022B2 Method of concentrating ozone gas and apparatus therefor 有权
标题翻译：浓缩臭氧气体的方法及其设备
公开(公告)号：US08404022B2
公开(公告)日：2013-03-26
申请号：US13054999
申请日：2008-07-23
申请人： Kunihiko Koike , Sadaki Nakamura , Naohisa Makihira , Koichi Izumi , Shigenori Takatori
发明人： Kunihiko Koike , Sadaki Nakamura , Naohisa Makihira , Koichi Izumi , Shigenori Takatori
IPC分类号： B01D53/02
CPC分类号： C01B13/10
摘要： A method of concentrating ozone gas in which, although the apparatus configuration is simple, ozone gas of a predetermined concentration can be efficiently taken out, and an apparatus therefor are provided. In a method of concentrating ozone gas in which an ozone-oxygen mixture gas is acted in an adsorbing column that is filled with an adsorbent, to cause the adsorbent to selectively adsorb the ozone gas, and the selectively adsorbed ozone gas is desorbed, thereby concentrating and purifying the ozone gas, the ozone-oxygen mixture gas is acted on the adsorbent in a non-cooled state to cause the ozone gas to be selectively adsorbed to the adsorbent, the adsorbing column is vacuumed when performing an operation desorbing of the ozone gas, thereby desorbing the ozone gas from the adsorbent, and an initial amount of the leading out of the desorbed ozone gas is not recovered, thereby obtaining high-concentration ozone gas.
摘要翻译：浓缩臭氧气体的方法，其中尽管装置结构简单，但可以有效地取出预定浓度的臭氧气体，并提供其设备。在将填充有吸附剂的吸附塔中进行臭氧 - 氧气混合气体的臭氧气体浓缩的方法中，使吸附剂选择性吸附臭氧气体，并且将选择性吸附的臭氧气体解吸，净化臭氧气体时，臭氧 - 氧混合气体处于未冷却状态的吸附剂上，使臭氧气体选择性地吸附到吸附剂上，当对臭氧气体进行操作解吸时吸附塔被抽真空从而从吸附剂解吸臭氧气体，并且不能回收从解吸的臭氧气体中引出的初始量，从而获得高浓度的臭氧气体。

8. 发明申请

US20110123430A1 METHOD OF CONCENTRATING OZONE GAS AND APPARATUS THEREFOR 有权
标题翻译：浓缩臭氧及其装置的方法
公开(公告)号：US20110123430A1
公开(公告)日：2011-05-26
申请号：US13054999
申请日：2008-07-23
申请人： Kunihiko Koike , Sadaki Nakamura , Naohisa Makihira , Koichi Izumi , Shigenori Takatori
发明人： Kunihiko Koike , Sadaki Nakamura , Naohisa Makihira , Koichi Izumi , Shigenori Takatori
IPC分类号： C01B13/10
CPC分类号： C01B13/10
摘要： A method of concentrating ozone gas in which, although the apparatus configuration is simple, ozone gas of a predetermined concentration can be efficiently taken out, and an apparatus therefor are provided. In a method of concentrating ozone gas in which an ozone-oxygen mixture gas is acted in an adsorbing column that is filled with an adsorbent, to cause the adsorbent to selectively adsorb the ozone gas, and the selectively adsorbed ozone gas is desorbed, thereby concentrating and purifying the ozone gas, the ozone-oxygen mixture gas is acted on the adsorbent in a non-cooled state to cause the ozone gas to be selectively adsorbed to the adsorbent, the adsorbing column is vacuumed when performing an operation desorbing of the ozone gas, thereby desorbing the ozone gas from the adsorbent, and an initial amount of the leading out of the desorbed ozone gas is not recovered, thereby obtaining high-concentration ozone gas.
摘要翻译：浓缩臭氧气体的方法，其中尽管装置结构简单，但可以有效地取出预定浓度的臭氧气体，并提供其设备。在将填充有吸附剂的吸附塔中进行臭氧 - 氧气混合气体的臭氧气体浓缩的方法中，使吸附剂选择性吸附臭氧气体，并且将选择性吸附的臭氧气体解吸，净化臭氧气体时，臭氧 - 氧混合气体处于未冷却状态的吸附剂上，使臭氧气体选择性地吸附到吸附剂上，当对臭氧气体进行操作解吸时吸附塔被抽真空从而从吸附剂解吸臭氧气体，并且不能回收从解吸的臭氧气体中引出的初始量，从而获得高浓度的臭氧气体。

9. 发明授权

US5746841A Process for passivating treatment of piping system for high-purity gas 失效
标题翻译：高纯度气体管道系统钝化处理工艺
公开(公告)号：US5746841A
公开(公告)日：1998-05-05
申请号：US612644
申请日：1996-03-08
申请人： Kunihiko Koike , Goichi Inoue
发明人： Kunihiko Koike , Goichi Inoue
IPC分类号： C21D1/76 , C23C8/14 , F16L58/00 , H01L21/205 , H01L21/302 , H01L21/3065 , C23C8/12
CPC分类号： C23C8/14 , F16L58/00
摘要： A high-concentration ozone gas having a concentration of at least 50 VOL % of ozone in the ozone-oxygen system is acted within the temperature range of a normal temperature to 60.degree. C. on an ultrapurity-gas piping system for use in a semiconductor manufacturing apparatus and the like or on a metal component part for use in an ultrahigh-vacuum apparatus to form a passivation film on the interior metal surface thereof.
摘要翻译：在臭氧 - 氧气系统中具有至少50vol％的臭氧浓度的高浓度臭氧气体在用于半导体的超纯气体管道系统中在常温至60℃的温度范围内起作用制造装置等，或者在用于超高真空装置的金属部件上，在其内部金属表面上形成钝化膜。

10. 发明授权

US06344130B1 Method for continuously generating highly concentrated ozone gas 有权
标题翻译：连续生成高浓度臭氧气体的方法
公开(公告)号：US06344130B1
公开(公告)日：2002-02-05
申请号：US09443346
申请日：1999-11-19
申请人： Kunihiko Koike , Goichi Inoue , Tatsuo Fukuda
发明人： Kunihiko Koike , Goichi Inoue , Tatsuo Fukuda
IPC分类号： C25C100
CPC分类号： C01B13/10 , B01D53/0462 , B01D53/0476 , B01D53/053 , B01D2253/106 , B01D2256/14 , B01D2257/106 , B01D2259/40062 , B01D2259/40088 , B01D2259/403
摘要： A method for generating highly concentrated ozone gas by adsorbing ozone gas generated by an ozonizer with an absorbent within an adsorption column and then separating highly concentrated ozone gas from the adsorption column. Three adsorption columns are arranged in parallel. Each of the adsorption columns is controlled to repeat four steps of an ozone gas adsorbing step, a stabilizing and pressurizing step, an ozone gas desorbing step and a cooling down step. Each of the ozone gas adsorbing step and the ozone gas desorbing step has operation time set twice the operation time of each of the stabilizing and pressurizing step and the cooling down step. An ozone gas concentrating unit comprises three adsorption columns which are set to operate one after another by ⅓ cycle lag. Highly concentrated ozone gas separated at the desorbing step of each adsorption column is once stored in an ozone gas storage vessel.
摘要翻译：一种利用吸附塔吸附臭氧发生器产生的臭氧气体吸附高浓度臭氧气体的方法，然后从吸附塔中分离出高浓度的臭氧气体。三个吸附柱平行布置。控制每个吸附塔重复臭氧气体吸附步骤，稳定和加压步骤，臭氧气体解吸步骤和冷却步骤的四个步骤。每个臭氧气体吸附步骤和臭氧气体解吸步骤的操作时间设定为稳定和加压步骤和冷却步骤中的每一个的操作时间的两倍。臭氧气体浓缩单元包括三个吸附塔，这些吸附塔被设置成一个接一个地循环运行1个循环滞后。在每个吸附塔的解吸步骤分离的高浓度臭氧气体一次储存在臭氧气体储存容器中。

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