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1. 发明申请

US20090270239A1 Black Complex Oxide Particles, Process for Producing the Same, Black Pastes, and Black Matrixes 审中-公开
标题翻译：黑色复合氧化物颗粒，其生产方法，黑色浆料和黑色矩阵
公开(公告)号：US20090270239A1
公开(公告)日：2009-10-29
申请号：US11887557
申请日：2006-03-27
申请人： Koichi Katsuyama , Takashi Nakashima , Hiroyuki Shimamura
发明人： Koichi Katsuyama , Takashi Nakashima , Hiroyuki Shimamura
IPC分类号： C03C8/14 , C04B14/30 , C04B14/34
CPC分类号： C09C1/0009 , C01G51/00 , C01P2002/54 , C01P2004/20 , C01P2004/41 , C01P2004/45 , C01P2004/51 , C01P2004/62 , C01P2006/12 , C01P2006/19 , C01P2006/40 , C01P2006/42 , C01P2006/62 , C01P2006/63 , C01P2006/64 , C08K3/22 , C08K7/00 , C09C1/00 , C09D7/61 , C09D7/67 , C09D7/68 , C09D7/69 , C09D11/037 , C09D17/007
摘要： The complex oxide particles of the present invention have a black hue, and contains 35 to 70% by weight of cobalt and 5 to 40% by weight of manganese. The molar ratio of cobalt to manganese Co/Mn is 0.5 to 14. The average particle diameter of primary particles is 0.05 to 0.3 μm. The particles have a shape of octahedral form. The particles are produced preferably through wet oxidation. No firing process is performed. The particles contain substantially no metal elements other than cobalt and manganese. The complex oxide particles of the present invention are suitably used as a black pigment for coating material, ink, toner, and rubbers or plastics.
摘要翻译：本发明的复合氧化物粒子具有黑色色调，含有35〜70重量％的钴和5〜40重量％的锰。钴与锰Co / Mn的摩尔比为0.5〜14。一次粒子的平均粒径为0.05〜0.3μm。颗粒具有八面体形状。优选通过湿氧化生产颗粒。不执行点火过程。颗粒基本上不含钴和锰以外的金属元素。本发明的复合氧化物粒子适合用作涂料，油墨，调色剂，橡胶或塑料的黑色颜料。

2. 发明申请

US20090269585A1 BLACK COMPLEX OXIDE PARTICLES 审中-公开
标题翻译：黑色复合氧化物颗粒
公开(公告)号：US20090269585A1
公开(公告)日：2009-10-29
申请号：US11909874
申请日：2006-03-27
申请人： Shoichi Fujiyasu , Koichi Katsuyama , Tomoyuki Hoshino , Masahiro Miwa , Hiroyuki Shimamura
发明人： Shoichi Fujiyasu , Koichi Katsuyama , Tomoyuki Hoshino , Masahiro Miwa , Hiroyuki Shimamura
IPC分类号： B32B1/00 , C09D1/00
CPC分类号： C01G51/006 , C01G51/00 , C01G53/00 , C01G53/006 , C01P2002/32 , C01P2002/52 , C01P2004/20 , C01P2004/62 , C01P2006/11 , C01P2006/12 , C01P2006/19 , C01P2006/40 , C01P2006/62 , C01P2006/63 , C01P2006/64 , C08K3/22 , C09C1/00 , C09C1/0009 , C09D5/24 , C09D7/61 , C09D7/68 , H01B1/08 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993
摘要： The complex oxide particles of the present invention are conductive and exhibit a black color. The particles contain cobalt in an amount of 40 to 65% by mass in terms of the metal element based on the whole particles and at least one kind or two or more kinds of metals selected from copper, nickel and molybdenum. The particles are preferably prepared in the following manner: an aqueous solution of mixed metal salts prepared from water-soluble salts, wherein the aqueous solution contains cobalt and one kind or two or more kinds of metal element selected from copper, nickel and molybdenum, is mixed and neutralized with an alkali hydroxide to obtain a metal hydroxide slurry; the resultant slurry of metal hydroxides is kept at a pH of 10 to 13 and oxidized at a temperature of higher than 40° C. and 60° C. or less to obtain a precursor slurry; the resultant precursor slurry is aged at 80 to 150° C.; and then, after solid-liquid separation, the resultant solid is heated at 400 to 700° C. for longer than 1 hour and 3 hours or less.
摘要翻译：本发明的复合氧化物粒子是导电性的，呈黑色。颗粒含有的金属元素相对于整个颗粒为40〜65质量％的钴和选自铜，镍和钼中的至少一种或两种以上的金属。颗粒优选以如下方式制备：由水溶性盐制备的混合金属盐的水溶液，其中所述水溶液含有钴和选自铜，镍和钼中的一种或两种或更多种金属元素，混合并用碱金属氢氧化物中和，得到金属氢氧化物浆料; 将所得的金属氢氧化物浆液保持在10〜13的pH，在高于40℃，60℃以下的温度下进行氧化，得到前体浆料; 所得前体浆料在80-150℃下老化; 然后在固液分离后，将所得固体在400-700℃下加热1小时以上3小时以下。

3. 发明授权

US07465495B2 Composite black oxide particle, method for producing same, black coating material and black matrix 失效
标题翻译：复合黑色氧化物颗粒，其制造方法，黑色涂料和黑色矩阵
公开(公告)号：US07465495B2
公开(公告)日：2008-12-16
申请号：US10576125
申请日：2004-10-14
申请人： Shoichi Fujiyasu , Tomio Hayashi , Koichi Katsuyama , Hiroyuki Shimamura
发明人： Shoichi Fujiyasu , Tomio Hayashi , Koichi Katsuyama , Hiroyuki Shimamura
IPC分类号： B32B5/16
CPC分类号： C01G51/006 , C01P2002/32 , C01P2004/32 , C01P2004/45 , C01P2004/62 , C01P2004/80 , C01P2004/82 , C01P2004/84 , C01P2006/12 , C01P2006/19 , C01P2006/60 , C01P2006/62 , C01P2006/63 , C01P2006/64 , C09C1/0081 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993
摘要： Disclosed is a composite black oxide particle which is composed of oxide of cobalt, copper and manganese. The copper/cobalt molar ratio is 0.1-0.5, and the manganese/cobalt molar ratio is 0.2-1.0. The composite black oxide particle further contains silicon, and the silicon content to the total oxide particle is 0.1-3 mass %. The surface of the composite black oxide particle is coated with aluminum oxide. The Al content in the surface coating to the entire particle is 0.05-3 mass %.
摘要翻译：公开了由钴，铜和锰的氧化物构成的复合黑氧化物粒子。铜/钴摩尔比为0.1-0.5，锰/钴摩尔比为0.2-1.0。复合黑色氧化物粒子还含有硅，与氧化物总量的硅含量为0.1〜3质量％。复合黑色氧化物颗粒的表面涂覆有氧化铝。表面涂覆到整个颗粒的Al含量为0.05-3质量％。

4. 发明申请

US20070128438A1 Composite black oxide particle, method for producing same, black coating material and black matrix 失效
标题翻译：复合黑色氧化物颗粒，其制造方法，黑色涂料和黑色矩阵
公开(公告)号：US20070128438A1
公开(公告)日：2007-06-07
申请号：US10576125
申请日：2004-10-14
申请人： Shoichi Fujiyasu , Tomio Hayashi , Koichi Katsuyama , Hiroyuki Shimamura
发明人： Shoichi Fujiyasu , Tomio Hayashi , Koichi Katsuyama , Hiroyuki Shimamura
IPC分类号： B32B1/00 , B32B18/00 , B32B15/02 , C04B14/00
CPC分类号： C01G51/006 , C01P2002/32 , C01P2004/32 , C01P2004/45 , C01P2004/62 , C01P2004/80 , C01P2004/82 , C01P2004/84 , C01P2006/12 , C01P2006/19 , C01P2006/60 , C01P2006/62 , C01P2006/63 , C01P2006/64 , C09C1/0081 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993
摘要： Disclosed is a composite black oxide particle which is composed of oxide of cobalt, copper and manganese. The copper/cobalt molar ratio is 0.1-0.5, and the manganese/cobalt molar ratio is 0.2-1.0. The composite black oxide particle further contains silicon, and the silicon content to the total oxide particle is 0.1-3 mass %. The surface of the composite black oxide particle is coated with aluminum oxide. The Al content in the surface coating to the entire particle is 0.05-3 mass %.
摘要翻译：公开了由钴，铜和锰的氧化物构成的复合黑氧化物粒子。铜/钴摩尔比为0.1-0.5，锰/钴摩尔比为0.2-1.0。复合黑色氧化物粒子还含有硅，与氧化物总量的硅含量为0.1〜3质量％。复合黑色氧化物颗粒的表面涂覆有氧化铝。表面涂覆到整个颗粒的Al含量为0.05-3质量％。

5. 发明授权

US6120576A Method for preparing nickel fine powder 失效
标题翻译：镍微粉制备方法
公开(公告)号：US6120576A
公开(公告)日：2000-09-19
申请号：US112361
申请日：1998-07-09
申请人： Yoshiharu Toshima , Takayuki Araki , Takao Hayashi , Hiroyuki Shimamura
发明人： Yoshiharu Toshima , Takayuki Araki , Takao Hayashi , Hiroyuki Shimamura
IPC分类号： B22F1/00 , B22F9/24
CPC分类号： C22B23/0453 , B22F1/0014 , B22F9/24 , B22F2998/00
摘要： A method for preparing nickel fine powder is herein disclosed, which comprises the steps of mixing an aqueous sodium hydroxide solution comprising, on the basis of the total weight of the sodium hydroxide present in the aqueous solution, 75 to 85% by weight of liquid caustic soda as specified in JIS K 1203 and 25 to 15% by weight, in total, of at least one of sodium hydroxide as specified in JIS K 8576 and solid caustic soda as specified in JIS K 1202, with an aqueous solution of nickel sulfate to form nickel hydroxide, then reducing the resulting nickel hydroxide with hydrazine and recovering nickel fine powder produced. The nickel fine powder prepared by the method has an average particle size of the primary particles ranging from 0.1 to 0.9 .mu.m, a D.sub.90 value of not more than 2.1 .mu.m and a tap density of not less than 3.5 g/cc. The nickel fine powder has a low degree of aggregation, a narrow particle size distribution and a high tap density and therefore, the powder is quite suitably used as a material for producing an internal electrode for a laminated ceramic condenser.
摘要翻译：本文公开了一种制备镍微粉的方法，其包括以下步骤：将氢氧化钠水溶液混合，所述氢氧化钠水溶液基于存在于水溶液中的氢氧化钠的总重量为75至85重量％的液体苛性碱按照JIS K 1203中规定的苏打水，以及JIS-8576中规定的氢氧化钠中的至少一种和JIS K 1202中规定的固体苛性钠中的至少一种的25〜15重量％的硫酸镍水溶液形成氢氧化镍，然后用肼还原所得的氢氧化镍并回收生产的镍细粉。通过该方法制备的镍微粉末，其一次粒子的平均粒径为0.1〜0.9μm，D90值不大于2.1μm，振实密度为3.5g / cc以上。镍微粉末具有低聚集度，窄粒度分布和高振实密度，因此该粉末非常适合用作制备用于层压陶瓷冷凝器的内部电极的材料。

6. 发明申请

US20070209475A1 Flaky Copper Powder, Method For Producing The Same, And Conductive Paste 审中-公开
标题翻译：片状铜粉，生产方法和导电膏
公开(公告)号：US20070209475A1
公开(公告)日：2007-09-13
申请号：US11587976
申请日：2005-04-26
申请人： Takahiko Sakaue , Katsuhiko Yoshimaru , Yoshinobu Nakamura , Hiroyuki Shimamura
发明人： Takahiko Sakaue , Katsuhiko Yoshimaru , Yoshinobu Nakamura , Hiroyuki Shimamura
IPC分类号： B22F9/24
CPC分类号： B22F1/0014 , B22F1/0044 , B22F1/0055 , B22F1/0062 , B22F9/24 , B22F2001/0033 , H01B1/22 , H05K1/095
摘要： It is an object of the present invention to provide a flaky copper powder composed of fine particles having a sharp distribution particle size, a large crystallite diameter and high oxidation resistance. The flaky copper powder of the present invention contains P and has a crystallite diameter/D1A ratio of 0.01 or more to achieve the object. The method for producing the flaky copper powder comprises four steps: a first step of preparing an aqueous solution containing a copper salt and complexing agent; a second step of adding an alkali hydroxide to the aqueous solution to prepare a first slurry containing cupric oxide; a third step of adding a first reducing agent which can reduce the cupric oxide into cuprous oxide to the first slurry to prepare a second slurry containing cuprous oxide; and a fourth step of adding a second reducing agent which can reduce the cuprous oxide into copper to the second slurry to provide a flaky copper powder, wherein phosphoric acid and its salt are added in at least one of the first to third steps and/or in the second slurry in the fourth step.
摘要翻译：本发明的目的是提供一种由具有尖锐分布粒度，大晶粒直径和高抗氧化性的细颗粒组成的片状铜粉末。本发明的片状铜粉含有P，并且具有0.01以上的微晶直径/ D 1A％比以达到目的。片状铜粉的制造方法包括四个步骤：制备含有铜盐和络合剂的水溶液的第一步骤; 向该水溶液中添加碱性氢氧化物以制备含有氧化铜的第一浆料的第二步骤; 第三步骤，将第一还原剂加入到第一浆料中以制备含有氧化亚铜的第二浆料; 以及第四步骤，添加第二还原剂，其可以将氧化亚铜还原成铜到第二浆料中以提供片状铜粉末，其中在第一至第三步骤中的至少一个中加入磷酸及其盐，和/或在第四步中的第二浆料中。

7. 发明申请

US20070295938A1 Electro Conductive Tin Oxide Powder and Method for Producing the Same 审中-公开
标题翻译：导电氧化锡粉及其制造方法
公开(公告)号：US20070295938A1
公开(公告)日：2007-12-27
申请号：US10588650
申请日：2005-02-04
申请人： Hiroshi Fujii , Koichi Kawaraya , Katsuhiko Yoshimaru , Hiroyuki Shimamura
发明人： Hiroshi Fujii , Koichi Kawaraya , Katsuhiko Yoshimaru , Hiroyuki Shimamura
IPC分类号： H01B1/12
CPC分类号： C08L101/12 , C01G19/02 , C01P2006/40 , C09D5/24
摘要： An object of the present invention is to provide an electro conductive tin oxide powder which is free from toxic dopant, e.g., antimony, which can provide excellent conductivity to a polymer, and easy to disperse in a paint and the conductive film formed shows excellent transparency; and also provide the method for producing an electro conductive tin oxide powder. In order to achieve the above objects, the present invention disclose the electro conductive tin oxide powder which is characterized in that it is free from a dopant and the paint prepared with it gives conductive film which shows a Haze value of 5% or less and surface resistance of 1010Ω/ or less. The electro conductive tin oxide powder is produced by the method which is characterized in that steps for production are, adding a sodium stannate solution slowly into an aqueous acid solution till the solution pH goes down to 5 or under; followed by rinsing, followed by filtering and drying the resulting slurry and milling of the resulting dry powder and calcining of the milled powder in a non-oxidizing atmosphere.
摘要翻译：本发明的目的是提供一种不含有毒的掺杂剂的导电氧化锡粉末，例如锑，其可以为聚合物提供优异的导电性，并且易于分散在涂料中，并且所形成的导电膜显示出优异的透明度 ; 并且还提供了制造导电氧化锡粉末的方法。为了实现上述目的，本发明公开了一种导电性氧化锡粉末，其特征在于，其不含掺杂剂，并且用其制备的涂料产生显示5％或更低的雾度值的导电膜和表面电阻为10 10Ω/或更小。通过以下方法制造导电氧化锡粉末，其特征在于，生产步骤是将酸式钠溶液缓慢加入到酸性水溶液中直到溶液pH降至5或更低; 然后冲洗，然后过滤并干燥所得浆料并研磨所得干粉，并在非氧化气氛中煅烧研磨的粉末。

8. 发明授权

US07226544B2 Magnetite particles 有权
标题翻译：磁铁矿颗粒
公开(公告)号：US07226544B2
公开(公告)日：2007-06-05
申请号：US10500935
申请日：2003-06-09
申请人： Tomio Hayashi , Hiroyuki Shimamura
发明人： Tomio Hayashi , Hiroyuki Shimamura
IPC分类号： C01G49/08 , H01F1/11 , G03G9/083
CPC分类号： B82Y30/00 , C01G49/08 , C01P2004/41 , C01P2004/62 , C01P2004/64 , C01P2006/12 , C01P2006/42 , C01P2006/80 , G03G9/0833 , G03G9/0835 , G03G9/0837 , H01F1/36
摘要： Magnetite particles (and their manufacturing method) that enable suppression of blooming caused because of their large coercive force when used as magnetic toner, exert a light environment load, and are excellent in cost. The magnetite particles contain 0.1 to 1 mass % of phosphorus, have a coercive force of 10 to 25 kA/m at a load magnetic field of 796 kA/m, and have a shape of octahedron.
摘要翻译：当作为磁性调色剂使用时，由于其矫顽力大而能够抑制起霜的磁铁矿颗粒（及其制造方法），施加轻的环境负荷，成本优异。磁铁矿颗粒含有0.1〜1质量％的磷，在796kA / m的负荷磁场下具有10〜25kA / m的矫顽力，具有八面体形状。

9. 发明授权

US06632524B1 Nickel powder, method for preparing the same and paste for use in making electrodes for electronic parts 有权
标题翻译：镍粉，其制备方法和用于制造电子部件用电极的糊剂
公开(公告)号：US06632524B1
公开(公告)日：2003-10-14
申请号：US09716238
申请日：2000-11-21
申请人： Yoshiharu Toshima , Takao Hayashi , Yasuhide Yamaguchi , Hiroyuki Shimamura
发明人： Yoshiharu Toshima , Takao Hayashi , Yasuhide Yamaguchi , Hiroyuki Shimamura
IPC分类号： B32B1502
CPC分类号： H01G4/0085 , H01B1/02 , H01B1/22 , Y10T428/29 , Y10T428/2982 , Y10T428/2991
摘要： Nickel powder comprises, on the basis of the total number of particles, not less than 10% of particles whose particle size is not less than 1.2 time the average particle size, as determined by the SEM observation; and not less than 10% of particles whose particle size is not more than 0.8 time the average particle size, as determined by the SEM observation. The nickel powder can be prepared by, for instance, precipitating nickel particles from an aqueous solution containing a nickel salt and a hydrazine reducing agent, without forming any hydroxide of nickel as an intermediate. A conductive paste containing the nickel powder can be applied onto the positions on which an internal or external electrode for electronic parts and then baking the coated paste to give an electrode.
摘要翻译：根据SEM观察，镍粉基于粒子总数不少于粒径不小于1.2倍平均粒度的粒子的10％; 和通过SEM观察确定的粒径不大于平均粒径的0.8倍的粒子的不少于10％。镍粉可以通过例如从含有镍盐和肼还原剂的水溶液中沉淀镍颗粒而不形成任何镍的氢氧化物作为中间体来制备。施加到用于电子部件的内部或外部电极的位置上，然后烘烤涂覆的糊料以产生电极。

10. 发明授权

US06162277A Nickel fine powder and method for preparing the same 有权
标题翻译：镍粉及其制备方法
公开(公告)号：US06162277A
公开(公告)日：2000-12-19
申请号：US240629
申请日：1999-02-01
申请人： Yoshiharu Toshima , Takayuki Araki , Takao Hayashi , Hiroyuki Shimamura
发明人： Yoshiharu Toshima , Takayuki Araki , Takao Hayashi , Hiroyuki Shimamura
IPC分类号： C01G53/00 , B22F1/00 , B22F5/00 , B22F9/24 , C22B3/44 , C22B5/00 , C22B23/00 , C22C1/04 , C22C19/00 , H01G4/008 , H01G4/12 , B22F9/00
CPC分类号： H01G4/0085 , B22F9/24 , C22C1/0433
摘要： A nickel fine powder includes 0.02 to 1.0% by weight of magnesium and/or 0.02 to 0.1% by weight of calcium dispersed in the nickel. A method for preparing the nickel fine powder includes the steps of forming nickel hydroxide by mixing an aqueous solution containing a magnesium salt and/or a calcium salt and a nickel salt with an aqueous solution of sodium hydroxide and then reducing the hydroxide with a hydrazine reducing agent. The nickel fine powder has thermal shrinkage characteristics very close to those observed for ceramic substrates and is accordingly suitable as a material for producing an internal electrode for laminated ceramic condensers.
摘要翻译：镍微粉末包含0.02〜1.0重量％的镁和/或0.02〜0.1重量％的分散在镍中的钙。制备镍微粉的方法包括以下步骤：通过将含有镁盐和/或钙盐和镍盐的水溶液与氢氧化钠水溶液混合形成氢氧化镍，然后用还原肼还原氢氧化物代理商镍微粉末的热收缩特性与陶瓷基板的热收缩特性非常接近，因此适合作为层叠陶瓷电容器的内部电极的制造用材料。

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