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1. 发明授权

US06440885B1 Zeolite membrane and a process for the production thereof 失效
标题翻译：沸石膜及其制备方法
公开(公告)号：US06440885B1
公开(公告)日：2002-08-27
申请号：US09473930
申请日：1999-12-28
申请人： Kim D. Pierotti , Dell J. St. Julien
发明人： Kim D. Pierotti , Dell J. St. Julien
IPC分类号： B01J2904
CPC分类号： B01J20/28033 , B01D63/066 , B01D67/0051 , B01D71/028 , B01D2325/04 , B01D2325/10 , B01D2325/12 , B01D2325/48 , B01J20/18 , B01J20/2803 , B01J20/28042 , B01J20/28069 , B01J20/28085 , B01J35/065 , B01J37/0246 , B01J2229/64 , C04B41/009 , C04B41/5024 , C04B41/85 , C04B2111/00801 , C04B41/0072 , C04B41/4521 , C04B41/4535 , C04B41/4556 , C04B35/10 , C04B35/195 , C04B35/185 , C04B38/0006
摘要： The present invention is directed at a supported zeolite structure comprising substantially-sintered monolithic porous ceramic substrate having coated thereon a uniformly thin, essentially continuous zeolite crystal layer covering at least one surface and associated pores of the porous ceramic material. The zeolite crystal layer is comprised of a single layer of zeolite crystals and is free of any growth enhancing, selectivity enhancing, or reparation layer and exhibits an oriented structure whereby the crystals exhibit a substantially columnar cross-section. Preferably, the porous ceramic substrate support comprises, on an analyzed oxide basis, 10-90%, by weight alumina and exhibits a crystal phase assemblage selected from the group consisting of cordierite, mullite, alumina, and/or mixtures thereof. A method for forming a zeolite membrane disclosed herein is also provided. The method generally comprises the steps of providing porous ceramic substrate and hydrothermally treating the substrate with an aqueous solution comprising sodium oxide or sodium hydroxide and having an alumina concentration of less than about 0.01%. The pH of the solution and the treatment time and temperature are such that these reaction conditions result in partial dissolution of the alumina in the substrate and essentially no nucleation in the solution thereby resulting in growth of the zeolite which is essentially continuous over the porous support.
摘要翻译：本发明涉及一种支撑的沸石结构，其包括基本上烧结的整体式多孔陶瓷基体，其上涂覆均匀薄的基本上连续的沸石晶体层，其覆盖多孔陶瓷材料的至少一个表面和相关孔。沸石晶体层由单层沸石晶体组成，并且不含任何生长增强，选择性增强或修复层，并且表现出取向结构，由此晶体呈现基本上柱状横截面。优选地，多孔陶瓷衬底支撑体在分析的氧化物基础上包含10-90重量％的氧化铝，并显示出选自堇青石，莫来石，氧化铝和/或其混合物的晶相组合物。还提供了本文公开的形成沸石膜的方法。该方法通常包括提供多孔陶瓷基底并用包含氧化钠或氢氧化钠并且具有小于约0.01％的氧化铝浓度的水溶液水热处理底物的步骤。溶液的pH和处理时间和温度使得这些反应条件导致氧化铝在基材中的部分溶解，并且在溶液中基本上没有成核，从而导致在多孔载体上基本连续的沸石的生长。

2. 发明授权

US5350637A Microlaminated composites and method 失效
标题翻译：微孔复合材料及其制备方法
公开(公告)号：US5350637A
公开(公告)日：1994-09-27
申请号：US968667
申请日：1992-10-30
申请人： Thomas D. Ketcham , Leroy S. Share , Dell J. St. Julien
发明人： Thomas D. Ketcham , Leroy S. Share , Dell J. St. Julien
IPC分类号： B32B15/04 , B32B18/00
CPC分类号： B32B18/00 , B32B15/04 , C04B35/645 , C04B37/005 , C04B37/006 , C04B37/021 , C04B2235/6562 , C04B2235/6565 , C04B2235/6567 , C04B2235/6581 , C04B2237/068 , C04B2237/10 , C04B2237/121 , C04B2237/122 , C04B2237/123 , C04B2237/124 , C04B2237/16 , C04B2237/34 , C04B2237/341 , C04B2237/343 , C04B2237/346 , C04B2237/348 , C04B2237/36 , C04B2237/365 , C04B2237/368 , C04B2237/402 , C04B2237/403 , C04B2237/405 , C04B2237/406 , C04B2237/407 , C04B2237/567 , C04B2237/62 , C04B2237/66 , C04B2237/68 , C04B2237/704 , C04B2237/706 , C04B2237/708 , C04B2237/72 , C04B2237/76 , C04B2237/82 , F05C2201/0448 , Y10S264/36 , Y10S264/57 , Y10T428/12007
摘要： Microlaminated composite articles are made by combining one or more sheets of flexible sintered crystalline ceramic foil with one or multiple inorganic substrate layers, e.g., of metal foil, to form a stack which is then heated below the melting temperatures of the foil and substrate layers, and under slight or moderate pressure, to provide a well-bonded composite article which is essentially free of interlaminar cementing or sealing materials.
摘要翻译：微结构复合制品通过将一片或多片柔性烧结结晶陶瓷箔与一种或多种无机基底层（例如金属箔）组合以形成叠层，然后将其加热到箔和基底层的熔融温度以下，并且在轻微或中等压力下，提供基本上不含层间粘合或密封材料的良好结合的复合制品。

3. 发明授权

US07947213B2 Method of making a textured electrolyte sheet for a fuel cell device 有权
标题翻译：制造用于燃料电池装置的纹理电解质片的方法
公开(公告)号：US07947213B2
公开(公告)日：2011-05-24
申请号：US11824910
申请日：2007-07-03
申请人： Michael E. Badding , Jacqueline L. Brown , Sean M. Garner , Thomas D. Ketcham , Dell J. St. Julien
发明人： Michael E. Badding , Jacqueline L. Brown , Sean M. Garner , Thomas D. Ketcham , Dell J. St. Julien
IPC分类号： C04B35/64 , B28B1/14
CPC分类号： C04B35/486 , C04B35/64 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3232 , C04B2235/3251 , C04B2235/3256 , C04B2235/3258 , C04B2235/3286 , C04B2235/3293 , C04B2235/602 , C04B2235/945 , H01M8/1246 , H01M8/1253 , H01M2300/0077 , Y02E60/525 , Y02P70/56
摘要： According to one aspect of the present invention the fuel cell device includes an electrolyte sheet. The electrolyte sheet has a substantially non-porous body of a varied thickness, a relatively smooth surface and a more textured surface with multiple indentations therein, wherein the thickest part of the electrolyte sheet is at least 0.5 micrometers greater than the thinnest part of said electrolyte sheet. The side of the electrolyte sheet with a relatively smooth surface is subjected to the predominately tensile force and the other, more textured surface subjected to predominately compressive force. According to one embodiment, the fuel cell also includes one cathode disposed on the more textured side of said electrolyte sheet at least at least one anode disposed opposite the cathode on the relatively smooth side of aid electrolyte sheet. According to one embodiment, the relatively smooth side of the electrolyte sheet is the fuel facing side and the more textured side is the air-facing side.
摘要翻译：根据本发明的一个方面，燃料电池装置包括电解质片。电解质片具有基本上无孔的体，其具有不同的厚度，相对光滑的表面和在其中具有多个凹口的更纹理的表面，其中电解质片的最厚部分比所述电解质的最薄部分大至少0.5微米片。具有相对平滑表面的电解质片的侧面受到主要的拉伸力，而另一个更具纹理的表面受到主要的压缩力。根据一个实施例，燃料电池还包括设置在所述电解质片的更纹理化侧的至少一个阳极，其设置在辅助电解质片的较平滑侧上与阴极相对设置的至少一个阳极。根据一个实施例，电解质片的相对平滑的一侧是面向燃料的侧面，更纹理的一面是面向空气的一侧。

4. 发明授权

US06299958B1 Manufacture of cellular honeycomb structures 有权
标题翻译：细胞蜂窝结构的制造
公开(公告)号：US06299958B1
公开(公告)日：2001-10-09
申请号：US09211379
申请日：1998-12-14
申请人： Dell J. St. Julien , John F. Wight, Jr. , Shy-Hsien Wu , Kenneth E. Zaun
发明人： Dell J. St. Julien , John F. Wight, Jr. , Shy-Hsien Wu , Kenneth E. Zaun
IPC分类号： B32B312
CPC分类号： B29D99/0089 , B22F2998/00 , B28B3/269 , B28B11/003 , B29C43/00 , B29C45/00 , C03B19/06 , C03B23/0006 , C03B23/0066 , C03B23/047 , C03B23/06 , C04B38/0009 , E04C2/365 , Y10T156/1003 , Y10T428/236 , Y10T428/24149 , C04B35/03 , C04B41/45 , B22F3/1115
摘要： A powder-formed cellular honeycomb body of novel tapered, curved and/or very high cell density configuration is provided through a reforming procedure wherein a precursor honeycomb shaped from a plasticized powder batch material is filled with a compatible plastic filler, reshaped at a temperature at which the plastic deformation characteristics of the honeycomb and filler are matched, and then solidified after removal of the filler to fix the final configuration of the body.
摘要翻译：通过重整程序提供了新颖的锥形，弯曲和/或非常高的泡孔密度构型的粉末形蜂窝体，其中由塑化粉末批料形成的前体蜂窝体填充有相容的塑料填料，其中蜂窝和填料的塑性变形特性匹配，然后在去除填料之后固化以固定体的最终构型。

5. 发明授权

US6077436A Device for altering a feed stock and method for using same 失效
标题翻译：用于改变原料的装置和使用它的方法
公开(公告)号：US6077436A
公开(公告)日：2000-06-20
申请号：US781996
申请日：1997-01-06
申请人： Lawrence S. Rajnik , Dell J. St. Julien , Yuming Xie
发明人： Lawrence S. Rajnik , Dell J. St. Julien , Yuming Xie
IPC分类号： B01D53/22 , B01D63/06 , C01B3/50 , B01D71/02
CPC分类号： B01D53/22 , B01D53/228 , B01D63/066 , C01B3/503 , B01D2313/42 , C01B2203/0405 , C01B2203/048
摘要： A device for altering a feed stock is made of a structure for passage of a feed stock. The structure can be either an extruded unibody structure, or a nested structure. The structure has an interior and an exterior section, and a longitudinal axis, and walls defining two sets of open-ended passages which extend along the longitudinal axis. The two sets of passages have different cross sectional shapes or dimensions with respect to each other. When the structure is nested, at least one set of channels have a cross section in the shape of truncated arcs. A method for making the unibody structure involves extruding a plasticized raw material mixture through a die, followed by heat-treating. A method of altering a feed stock which involves passing a feed stock into the device through one set of passages to cause an altering of the feed stock, and thereafter passing the output stream into and through the other set of channels to the exterior of the device.
摘要翻译：用于更换原料的装置由用于原料通过的结构制成。该结构可以是挤出的一体结构，也可以是嵌套结构。该结构具有内部和外部部分以及纵向轴线，以及限定沿着纵向轴线延伸的两组开放式通道的壁。两组通道相对于彼此具有不同的横截面形状或尺寸。当结构被嵌套时，至少一组通道具有截断圆弧形状的横截面。制造一体结构的方法包括通过模头挤出增塑的原料混合物，随后进行热处理。一种改变原料的方法，其包括将原料通过一组通道进入装置以引起原料的改变，然后使输出流通过另一组通道进入装置的外部。

6. 发明授权

US5814262A Method for producing thin flexible sintered structures 失效
标题翻译：薄柔性烧结结构的制造方法
公开(公告)号：US5814262A
公开(公告)日：1998-09-29
申请号：US964002
申请日：1992-10-21
申请人： Thomas D. Ketcham , Wayne B. Sanderson, deceased , by Stuart R. Sanderson, administrator , Dell J. St. Julien , Kathleen A. Wexell
发明人： Thomas D. Ketcham , Wayne B. Sanderson, deceased , by Stuart R. Sanderson, administrator , Dell J. St. Julien , Kathleen A. Wexell
IPC分类号： C04B35/622 , B29C33/58
CPC分类号： C04B35/62218
摘要： Thin inorganic sintered structures having strength and flexibility sufficient to permit bending without breakage in at least one direction to a radius of curvature of less than 20 centimeters, methods for making them, and products incorporating them, are described. Preferred sintered ceramic structures according to the invention can comprise zirconias, titanias, aluminas, silicas, rare earth metal oxides, alkaline oxides, alkaline earth metal oxides and first, second, and third transition series metal oxides and combinations thereof and therebetween. Sintered metal structures can also be provided.
摘要翻译：描述了具有足够的强度和柔性的薄无机烧结结构，其允许在至少一个方向上弯曲而不破裂到小于20厘米的曲率半径，制备它们的方法和结合它们的产品。根据本发明的优选的烧结陶瓷结构可以包括氧化锆，氧化钛，氧化铝，二氧化硅，稀土金属氧化物，碱性氧化物，碱土金属氧化物和第一，第二和第三过渡系列金属氧化物及其组合。也可以提供烧结金属结构。

7. 发明申请

US20080160376A1 Fuel cells with enhanced via fill compositions and/or enhanced via fill geometries 有权
公开(公告)号：US20080160376A1
公开(公告)日：2008-07-03
申请号：US12075497
申请日：2008-03-12
申请人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Susan L. Schiefelbein , Dell J. St. Julien , Raja R. Wusirika
发明人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Susan L. Schiefelbein , Dell J. St. Julien , Raja R. Wusirika
IPC分类号： H01M8/10
CPC分类号： H01M4/8621 , H01M4/9066 , H01M8/0206 , H01M8/0208 , H01M8/0247 , H01M8/0256 , H01M8/1226 , H01M8/1231 , H01M8/1246 , H01M8/2425 , H01M8/2432 , H01M8/2457 , Y02E60/525 , Y02P70/56
摘要： A fuel cell and method for manufacturing the fuel cell are described herein. Basically, the fuel cell is formed from an electrode/electrolyte structure including an array of anode electrodes and cathode electrodes disposed on opposing sides of an electrolyte sheet, the anode and cathode electrodes being electrically connected in series, parallel, or a combination thereof by electrical conductors that traverse via holes in the electrolyte sheet. Several different embodiments of electrical conductors which have a specific composition and/or a specific geometry are described herein.

8. 发明授权

US06852436B2 High performance solid electrolyte fuel cells 有权
标题翻译：高性能固体电解质燃料电池
公开(公告)号：US06852436B2
公开(公告)日：2005-02-08
申请号：US10077301
申请日：2002-02-15
申请人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Dell J. St. Julien , Raja R. Wusirika
发明人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Dell J. St. Julien , Raja R. Wusirika
IPC分类号： H01M4/86 , H01M8/02 , H01M8/12 , H01M8/24
CPC分类号： H01M4/8621 , H01M4/9066 , H01M8/0206 , H01M8/0208 , H01M8/0247 , H01M8/0256 , H01M8/1226 , H01M8/1231 , H01M8/1246 , H01M8/2425 , H01M8/2432 , H01M8/2457 , Y02E60/525 , Y02P70/56
摘要： The present invention relates to a fuel cell apparatus which includes arrays of positive air electrodes and negative fuel electrodes with via interconnections disposed on an electrolyte sheet; optional electrode designs include symmetric electrodes comprising a conductive silver alloy metal phase and a thermally stabilizing ceramic phase, the latter providing low interface resistance and matching thermal properties.
摘要翻译：燃料电池装置技术领域本发明涉及一种燃料电池装置，其包括正空气电极阵列和负极燃料电极，通孔互连设置在电解质片上; 可选的电极设计包括包括导电银合金金属相和热稳定陶瓷相的对称电极，后者提供低界面电阻和匹配的热性能。

9. 发明授权

US06623881B2 High performance solid electrolyte fuel cells 有权
标题翻译：高性能固体电解质燃料电池
公开(公告)号：US06623881B2
公开(公告)日：2003-09-23
申请号：US09858124
申请日：2001-05-15
申请人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Dell J. St. Julien , Raja R. Wusirika
发明人： Michael E. Badding , Jacqueline L. Brown , Thomas D. Ketcham , Dell J. St. Julien , Raja R. Wusirika
IPC分类号： H01M400
CPC分类号： H01M8/0247 , H01M4/8621 , H01M4/9066 , H01M8/0206 , H01M8/0208 , H01M8/0256 , H01M8/1226 , H01M8/1231 , H01M8/1246 , H01M8/2425 , H01M8/2432 , Y02E60/525 , Y02P70/56
摘要： The present invention relates to a compliant fuel cell apparatus which includes arrays of positive air electrodes and negative fuel electrodes with via interconnections disposed on a thin compliant electrolyte sheet; optional electrode designs include symmetric electrodes comprising a conductive silver alloy metal phase and a thermally stabilizing ceramic phase, the latter providing low interface resistance and matching thermal properties, with the resulting fuel cells remaining sufficiently compliant to demonstrate good resistance to thermal shock damage.
摘要翻译：本发明涉及一种兼容的燃料电池装置，其包括正空气电极和负极燃料电极的阵列，其中通孔互连设置在薄柔顺电解质片上; 可选的电极设计包括包括导电银合金金属相和热稳定陶瓷相的对称电极，后者提供低界面电阻和匹配的热性能，所得到的燃料电池保持足够的柔顺性以显示出良好的耐热冲击损伤性。

10. 发明授权

US5458834A Extrusion of low viscosity batch 失效
标题翻译：挤出低粘度批料
公开(公告)号：US5458834A
公开(公告)日：1995-10-17
申请号：US132923
申请日：1993-10-07
申请人： Margaret K. Faber , Thomas D. Ketcham , Dell J. St. Julien
发明人： Margaret K. Faber , Thomas D. Ketcham , Dell J. St. Julien
IPC分类号： B29C47/00 , B28B3/20 , B28B11/24 , B29C47/12 , B29C47/20 , C04B35/622 , C04B35/634 , C04B35/636 , C04B35/638 , B29C47/08
CPC分类号： C04B35/63404 , B28B11/243 , B28B3/269 , B29C47/0028 , B29C47/12 , C04B35/622 , C04B35/634 , C04B35/63416 , C04B35/63424 , C04B35/63448 , C04B35/6365 , C04B35/638 , C04B38/04 , B29C47/0014 , B29C47/0021 , B29L2031/60 , C04B2201/10
摘要： A method of forming complex shapes from soft solvent-containing batches and maintaining the integrity of such formed bodies. The formed bodies are made self-supporting immediately after forming or soon thereafter by contacting the shaped body with a drying or hardening liquid in which the solvent is soluble. A method is also disclosed for simultaneously drying a formed body and creating or increasing the porosity of the body by adding solid particles which are soluble in the drying liquid.
摘要翻译：从含有软质溶剂的批次形成复杂形状并保持这种成形体的完整性的方法。成形体在成型后立即自立，或者在此之后通过使成形体与溶剂可溶的干燥或硬化液接触。还公开了一种通过添加可溶于干燥液体的固体颗粒同时干燥成形体并产生或增加机体孔隙率的方法。

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