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1. 发明授权

US5977271A Process for preparing thermoset interpolymers and foams 失效
标题翻译：制备热固性互聚物和泡沫的方法
公开(公告)号：US5977271A
公开(公告)日：1999-11-02
申请号：US921642
申请日：1997-08-27
申请人： Kevin W. McKay , Francis J. Timmers , Edwin R. Feig , Thoi H. Ho , Seema V. Karande
发明人： Kevin W. McKay , Francis J. Timmers , Edwin R. Feig , Thoi H. Ho , Seema V. Karande
IPC分类号： C08F4/659 , C08F10/00 , C08L23/02 , C08L23/08 , C08L53/02 , C08F8/34 , C08F236/20
CPC分类号： C08L23/02 , C08F10/00 , C08L53/02 , C08L53/025 , C08F4/65908 , C08F4/65912 , C08L23/0838 , C08L2314/06
摘要： The subject invention provides a thermoset elastomer comprising a crosslinked pseudorandom or substantially random interpolymer of: (a) from 15 to 70 weight percent of at least one .alpha.-olefin, (b) from 30 to 70 weight percent of at least one vinylidene aromatic compound, and (c) from 0 to 15 weight percent of at least one diene. The subject invention further provides a thermoplastic vulcanizate comprising the thermoset elastomers of the invention as provided in a thermoplastic polyolefin matrix. The subject invention further provides processes for preparing the inventive thermoset elastomers and thermoplastic vulcanizates, as well as parts fabricated therefrom. The inventive materials have a superior balance of properties, as compared to EPM and EPDM based materials. The subject invention also pertains to foams and methods for their preparation.
摘要翻译：本发明提供了一种热固性弹性体，其包含交联的伪随机或基本上无规的互聚物：（a）15至70重量％的至少一种α-烯烃，（b）30至70重量％的至少一种亚乙烯基芳族化合物，和（c）0至15重量％的至少一种二烯。本发明进一步提供了一种热塑性硫化橡胶，其包含热塑性聚烯烃基质中提供的本发明的热固性弹性体。本发明还提供了制备本发明的热固性弹性体和热塑性硫化橡胶以及由其制造的部件的方法。与EPM和EPDM基材料相比，本发明的材料具有优异的性能平衡。本发明还涉及泡沫体及其制备方法。

2. 发明授权

US5869591A Thermoset interpolymers and foams 失效
标题翻译：热固性互聚物和泡沫
公开(公告)号：US5869591A
公开(公告)日：1999-02-09
申请号：US921641
申请日：1997-08-27
申请人： Kevin W. McKay , Francis J. Timmers , Edwin R. Feig , Thoi H. Ho , Seema V. Karande
发明人： Kevin W. McKay , Francis J. Timmers , Edwin R. Feig , Thoi H. Ho , Seema V. Karande
IPC分类号： C08F4/659 , C08F10/00 , C08L23/02 , C08L23/08 , C08L25/06 , C08L25/08 , C08L53/02 , C08F236/10 , C08L47/00
CPC分类号： C08L25/08 , C08F10/00 , C08L23/02 , C08L23/08 , C08L53/02 , C08L53/025 , C08F4/65908 , C08F4/65912 , C08K5/14 , C08L2205/22 , C08L23/0838 , C08L2312/00 , C08L2314/06 , C08L25/06
摘要： The subject invention provides a thermoset elastomer comprising a crosslinked pseudorandom or substantially random interpolymer of: (a) from 15 to 70 weight percent of monomer units derived from at least one a-olefin, (b) from 30 to 70 weight percent of monomer units derived from at least one vinylidene aromatic compound, and (c) from 0 to 15 weight percent of monomer units derived from at least one diene. The subject invention further provides a thermoplastic vulcanizate comprising the thermoset elastomers of the invention as provided in a thermoplastic polyolefin matrix. The subject invention further provides processes for preparing the inventive thermoset elastomers and thermoplastic vulcanizates, as well as parts fabricated therefrom. The inventive materials have a superior balance of properties, as compared to EPM and EPDM based materials. The subject invention also pertains to foams and methods for their preparation.
摘要翻译：本发明提供了一种热固性弹性体，其包含交联的伪随机或基本上无规的互聚物：（a）15至70重量％的衍生自至少一种α-烯烃的单体单元，（b）30至70重量％的单体单元衍生自至少一种亚乙烯基芳族化合物，和（c）0至15重量％的衍生自至少一种二烯的单体单元。本发明进一步提供了一种热塑性硫化橡胶，其包含热塑性聚烯烃基质中提供的本发明的热固性弹性体。本发明还提供了制备本发明的热固性弹性体和热塑性硫化橡胶以及由其制造的部件的方法。与EPM和EPDM基材料相比，本发明的材料具有优异的性能平衡。本发明还涉及泡沫体及其制备方法。

3. 发明授权

US06325956B2 Crosslinking of polymers and foams thereof 失效
标题翻译：聚合物和泡沫的交联
公开(公告)号：US06325956B2
公开(公告)日：2001-12-04
申请号：US09140004
申请日：1998-08-26
申请人： Bharat I. Chaudhary , Thoi H. Ho , Seema V. Karande , Che-I. Kao , Robert H. Terbrueggen , David A. Babb , Clark H. Cummins , Michael J. Mullins , H. Craig Silvis
发明人： Bharat I. Chaudhary , Thoi H. Ho , Seema V. Karande , Che-I. Kao , Robert H. Terbrueggen , David A. Babb , Clark H. Cummins , Michael J. Mullins , H. Craig Silvis
IPC分类号： B29C4402
摘要： The invention includes a process comprising (a) forming a polymeric admixture including at least one polyolefin which has been prepared using a single site catalyst and at least a crosslinking amount of at least one poly(sulfonyl azide) crosslinking agent; (b) shaping the resulting admixture; and (c) heating the resulting shaped admixture to a temperature at least the decomposition temperature of the crosslinking agent. The steps take place in any sequence and optionally include substeps. The single site catalyst is preferably a constrained geometry or metallocene catalyst, but optionally another transition metal catalyst which is not a traditional Ziegler Natta Ti/MgCl2 catalyst such as a vanadium catalyst. The invention further includes all compositions obtainable by the process of the invention as well as all articles formed from these compositions. The articles are preferably thermoformed, compression molded, injection molded, extruded, cast, blow molded, blown, profile extruded, spun, foamed or molded of any composition of the invention. The invention includes a use of any composition of the invention in any process of thermoforming, injection molding, extrusion, casting, blow molding, spinning, blowing, profile extrusion, foaming, compression molding or a combination thereof.
摘要翻译：本发明包括一种方法，其包括（a）形成包含至少一种聚烯烃的聚合物混合物，所述聚合物混合物已经使用单中心催化剂和至少交联量的至少一种聚（磺酰基叠氮化物）交联剂制备; （b）成型所得混合物; 和（c）将所得成形的混合物加热至至少交联剂的分解温度的温度。步骤以任何顺序进行，并且可选地包括子步骤。单中心催化剂优选为约束几何形状或茂金属催化剂，但可选地为不是传统的齐格勒 - 纳塔Ti / MgCl 2催化剂如钒催化剂的另一种过渡金属催化剂。本发明还包括通过本发明的方法获得的所有组合物以及由这些组合物形成的所有制品。制品优选是由本发明的任何组合物进行热成型，压塑，注射成型，挤出，铸造，吹塑，吹塑，型材挤出，纺丝，发泡或模制的。本发明包括在热成型，注射成型，挤出，铸造，吹塑，纺丝，吹塑，型材挤出，发泡，压缩成型或其组合的任何方法中使用本发明的任何组合物。

4. 发明授权

US06624254B1 Silane functionalized olefin interpolymer derivatives 失效
标题翻译：硅烷官能化烯烃互聚物衍生物
公开(公告)号：US06624254B1
公开(公告)日：2003-09-23
申请号：US09593861
申请日：2000-06-14
申请人： Daniel J. Arriola , Matthew T. Bishop , Richard E. Campbell, Jr. , David D. Devore , Stephen E. Hahn , Thoi H. Ho , Thomas J. McKeand , Francis J. Timmers
发明人： Daniel J. Arriola , Matthew T. Bishop , Richard E. Campbell, Jr. , David D. Devore , Stephen E. Hahn , Thoi H. Ho , Thomas J. McKeand , Francis J. Timmers
IPC分类号： C08F3008
CPC分类号： C08F290/148 , C08F8/12 , C08F230/08 , C08F2810/50 , C08F210/06 , C08F210/02
摘要： Silane functional polymers having uniform silane distribution, long chain branching or tertiary silane functionality and conversion thereof through coupling, hydrolysis, hydrolysis and neutralization, condensation, oxidation or hydrosilation are disclosed.
摘要翻译：公开了具有均匀的硅烷分布，长链支化或叔硅烷官能团以及通过偶联，水解，水解和中和，缩合，氧化或硅氢化的转化的硅烷官能聚合物。

5. 发明授权

US06512049B1 Sulfonated substantially random interpolymers, blends therewith and articles made therefrom 失效
标题翻译：磺化的基本无规互聚物，与其混合并由其制成的制品
公开(公告)号：US06512049B1
公开(公告)日：2003-01-28
申请号：US10141591
申请日：2002-05-08
申请人： Yunwa W. Cheung , Stephen F. Hahn , James C. Stevens , Francis J. Timmers , Gregory F. Schmidt , Robert H. Terbrueggen , Thoi H. Ho
发明人： Yunwa W. Cheung , Stephen F. Hahn , James C. Stevens , Francis J. Timmers , Gregory F. Schmidt , Robert H. Terbrueggen , Thoi H. Ho
IPC分类号： C08L2500
CPC分类号： F16F9/48 , C08F8/36 , C08F8/44 , C08F212/00 , C08F2800/10 , C08F2800/20 , C08F2810/50 , C08L23/00 , C08L23/02 , C08L23/08 , C08L23/0815 , C08L23/0838 , C08L23/0876 , C08L23/32 , C08L23/34 , C08L25/18 , C08L77/00 , C08L2205/08 , F16F9/0209 , C08L2666/04 , C08L2666/20 , C08L2666/02 , C08F210/02 , C08F212/08
摘要： Sulfonated substantially random interpolymers made from monomer components comprise from 1 to 65 mole percent of (a) at least one vinyl or vinylidene aromatic monomer, or (b) at least one hindered aliphatic or cycloaliphatic vinylidene monomer, or (c) a combination of at least one vinyl or vinylidene aromatic monomer and at lest one hindered aliphatic or cycloaliphatic vinylidene monomer, and from 35 to 99 mole percent of at least one aliphatic &agr;-olefin having from 2 to 20 carbon atoms; and optionally, from 0 to 20 mole percent of a diene containing from 4 to 20 carbon atoms; wherein the sulfonated interpolymer contains at least one mer (or moiety) of a group represented by the formula —SO3M where M is hydrogen or a group 1, 7 or 12 metal in ionic form or combination thereof. Blends of these polymers with polyamides and polyolefins are made.
摘要翻译：由单体组分制备的磺化的基本上无规的互聚物包含1至65摩尔％的（a）至少一种乙烯基或亚乙烯基芳族单体，或（b）至少一种受阻脂族或脂环族亚乙烯基单体，或（c）至少一个乙烯基或亚乙烯基芳族单体和至少一个受阻的脂族或脂环族亚乙烯基单体，以及35至99摩尔％的至少一种具有2至20个碳原子的脂族α-烯烃; 和任选的0至20摩尔％的含有4至20个碳原子的二烯; 其中所述磺化互聚物包含至少一个由式-SO 3 M表示的基团的聚合物（或部分），其中M为氢或基团为离子形式或其组合的第1,7或12族金属。制备这些聚合物与聚酰胺和聚烯烃的共混物。

6. 发明授权

US06844399B2 Sulfonated substantially random interpolymers, blends therewith and articles made therefrom 失效
标题翻译：磺化的基本无规互聚物，与其混合并由其制成的制品
公开(公告)号：US06844399B2
公开(公告)日：2005-01-18
申请号：US10265931
申请日：2002-10-07
申请人： Yunwa W. Cheung , Stephen F. Hahn , James C. Stevens , Francis J. Timmers , Gregory F. Schmidt , Thoi H. Ho , Robert H. Terbrueggen
发明人： Yunwa W. Cheung , Stephen F. Hahn , James C. Stevens , Francis J. Timmers , Gregory F. Schmidt , Thoi H. Ho , Robert H. Terbrueggen
IPC分类号： C08L23/00 , C08F8/36 , C08F210/00 , C08F212/00 , C08L23/02 , C08L23/08 , C08L23/32 , C08L23/34 , C08L25/00 , C08L25/18 , C08L77/00 , F16F9/02 , F16F9/48
CPC分类号： F16F9/48 , C08F8/36 , C08F8/44 , C08F212/00 , C08F2800/10 , C08F2800/20 , C08F2810/50 , C08L23/00 , C08L23/02 , C08L23/08 , C08L23/0815 , C08L23/0838 , C08L23/0876 , C08L23/32 , C08L23/34 , C08L25/18 , C08L77/00 , C08L2205/08 , F16F9/0209 , C08L2666/04 , C08L2666/20 , C08L2666/02 , C08F210/02 , C08F212/08
摘要： Sulfonated substantially random interpolymers made from monomer components comprise from 1 to 65 mole percent of (a) at least one vinyl or vinylidene aromatic monomer, or (b) at least one hindered aliphatic or cycloaliphatic vinylidene monomer, or (c) a combination of at least one vinyl or vinylidene aromatic monomer and at lest one hindered aliphatic or cycloaliphatic vinylidene monomer, and from 35 to 99 mole percent of at least one aliphatic α-olefin having from 2 to 20 carbon atoms; and optionally, from 0 to 20 mole percent of a diene containing from 4 to 20 carbon atoms; wherein the sulfonated interpolymer contains at least one mer (or moiety) of a group represented by the formula —SO3−M where M is hydrogen or a group 1, 7 or 12 metal in ionic form or combination thereof. Blends of these polymers with polyamides and polyolefins are made.
摘要翻译：由单体组分制备的磺化的基本上无规的互聚物包含1至65摩尔％的（a）至少一种乙烯基或亚乙烯基芳族单体，或（b）至少一种受阻脂族或脂环族亚乙烯基单体，或（c）至少一个乙烯基或亚乙烯基芳族单体和至少一个受阻的脂族或脂环族亚乙烯基单体，以及35至99摩尔％的至少一种具有2至20个碳原子的脂族α-烯烃; 和任选的0至20摩尔％的含有4至20个碳原子的二烯; 其中所述磺化互聚物包含至少一个由式-SO 3 M表示的基团的聚合物（或部分），其中M是氢或1-7或12族离子形式或其组合的金属。制备这些聚合物与聚酰胺和聚烯烃的共混物。

7. 发明授权

US06479594B1 Sulfonated substantially random interpolymers, blends therewith and articles made therefrom 失效
标题翻译：磺化的基本无规互聚物，与其混合并由其制成的制品
公开(公告)号：US06479594B1
公开(公告)日：2002-11-12
申请号：US09529903
申请日：2000-04-20
申请人： Yunwa W. Cheung , Stephen F. Hahn , James C. Stevens , Francis J. Timmers , Gregory F. Schmidt , Thoi H. Ho , Robert H. Terbrueggen
发明人： Yunwa W. Cheung , Stephen F. Hahn , James C. Stevens , Francis J. Timmers , Gregory F. Schmidt , Thoi H. Ho , Robert H. Terbrueggen
IPC分类号： C08F836
CPC分类号： F16F9/48 , C08F8/36 , C08F8/44 , C08F212/00 , C08F2800/10 , C08F2800/20 , C08F2810/50 , C08L23/00 , C08L23/02 , C08L23/08 , C08L23/0815 , C08L23/0838 , C08L23/0876 , C08L23/32 , C08L23/34 , C08L25/18 , C08L77/00 , C08L2205/08 , F16F9/0209 , C08L2666/04 , C08L2666/20 , C08L2666/02 , C08F210/02 , C08F212/08
摘要： Sulfonated substantially random interpolymers made from monomer components comprise from 1 to 65 mole percent of (a) at least one vinyl or vinylidene aromatic monomer, or (b) at least one hindered aliphatic or cycloaliphatic vinylidene monomer, or (c) a combination of at least one vinyl or vinylidene aromatic monomer and at least one hindered aliphatic or cycloaliphatic vinylidene monomer, and from 35 to 99 mole percent of at least one aliphatic &agr;-olefin having from 2 to 20 carbon atoms; and optionally, from 0 to 20 mole percent of a diene containing from 4 to 20 carbon atoms; wherein the sulfonated interpolymer contains at least one mer (or moiety) of a group represented by the formula —SO3−M where M is hydrogen or a group 1, 7 or 12 metal in ionic form or combination thereof. Blends of these polymers with polyamides and polyolefins are made.
摘要翻译：由单体组分制备的磺化的基本上无规的互聚物包含1至65摩尔％的（a）至少一种乙烯基或亚乙烯基芳族单体，或（b）至少一种受阻脂族或脂环族亚乙烯基单体，或（c）至少一种乙烯基或亚乙烯基芳族单体和至少一种受阻的脂族或脂环族亚乙烯基单体，以及35至99摩尔％的至少一种具有2至20个碳原子的脂族α-烯烃; 和任选的0至20摩尔％的含有4至20个碳原子的二烯; 其中所述磺化互聚物包含至少一个由式-SO 3-M表示的基团的聚合物（或部分），其中M为氢或基团为离子形式或其组合的1或7族或12族金属。制备这些聚合物与聚酰胺和聚烯烃的共混物。

8. 发明申请

US20100000903A1 HIGH-DENSITY POLYETHYLENE COMPOSITIONS, METHOD OF PRODUCING THE SAME, ARTICLES MADE THEREFROM, AND METHOD OF MAKING SUCH ARTICLES 审中-公开
标题翻译：高密度聚乙烯组合物，其制备方法，制备方法及制备这些制品的方法
公开(公告)号：US20100000903A1
公开(公告)日：2010-01-07
申请号：US12375847
申请日：2007-07-25
申请人： Nancy Costolnick , Thoi H. Ho , Kevin Nylin , Dale A. Wright
发明人： Nancy Costolnick , Thoi H. Ho , Kevin Nylin , Dale A. Wright
IPC分类号： C08K5/101 , B29C31/10 , B65D1/00
CPC分类号： C08L23/06 , C08K5/1345 , C08L71/00 , C08L91/06 , C08L2666/14
摘要： The instant invention is a high-density polyethylene composition, method of producing the same, articles made therefrom, and method of making such articles. The high-density polyethylene composition according to instant invention includes a first component, a second component, and a third component. The first component is a high-density polyethylene polymer having a density in the range of 0.940 to 0.980 g/cm3. The second component is polyethylene glycol, and the third component is octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate. The high-density polyethylene composition of the instant invention has a Yellowness Index of less than about −2.5 at 0 hour of accelerated aging at 100° C. according to ASTM D-6290. The process for producing the high-density polyethylene composition according to instant invention includes the following steps: (1) providing a first component, wherein the first component is a high-density polyethylene polymer having a density in the range of 0.940 to 0.980 g/cm3; (2) providing a second component, wherein the second component is polyethylene glycol; (3) providing a third component, wherein the third component is octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate; (4) blending the second and third components into the first component thereby forming a blend; (5) pelletizing the blend; and (6) thereby forming pellets of the high-density polyethylene composition having a Yellowness Index of less than about −2.5 at 0 hour of accelerated aging at 100° C. according to ASTM D-6290. Articles according to instant invention comprises the above-described inventive high-density polyethylene composition.
摘要翻译：本发明是高密度聚乙烯组合物，其制造方法，由其制成的制品及其制造方法。根据本发明的高密度聚乙烯组合物包括第一组分，第二组分和第三组分。第一组分是密度在0.940至0.980g / cm3范围内的高密度聚乙烯聚合物。第二组分是聚乙二醇，第三组分是3-（3,5-二叔丁基-4-羟基苯基）丙酸十八烷基酯。根据ASTM D-6290，本发明的高密度聚乙烯组合物在100℃加速老化的0小时时的黄度指数小于约-2.5。根据本发明的高密度聚乙烯组合物的制造方法包括以下步骤：（1）提供第一组分，其中第一组分是密度在0.940至0.980g / cm 3的密度的高密度聚乙烯聚合物， cm3; （2）提供第二组分，其中第二组分是聚乙二醇; （3）提供第三组分，其中第三组分是3-（3,5-二叔丁基-4-羟基苯基）丙酸十八烷基酯; （4）将第二和第三组分混合到第一组分中，从而形成共混物; （5）将混合物造粒; 和（6），根据ASTM D-6290，在加速老化的0小时，在100℃下形成黄度指数小于约-2.5的高密度聚乙烯组合物的颗粒。根据本发明的制品包括上述本发明的高密度聚乙烯组合物。

9. 发明申请

US20090012224A1 Polyolefin Compositions Comprising Hydrated Inorganic or Organic Compounds for the Prevention of Discoloration 审中-公开
标题翻译：包含水合无机或有机化合物以防止变色的聚烯烃组合物
公开(公告)号：US20090012224A1
公开(公告)日：2009-01-08
申请号：US10590097
申请日：2005-02-04
申请人： Christoph Krohnke , Jan Malik , Peter Staniek , Gert Berendsen , Robin J. Lee , Thoi H. Ho
发明人： Christoph Krohnke , Jan Malik , Peter Staniek , Gert Berendsen , Robin J. Lee , Thoi H. Ho
IPC分类号： C08K3/32
CPC分类号： C08K3/32 , C08K3/38 , C08K5/098 , C08L23/02
摘要： The invention relates to a polyolefin composition comprising a water releasing additive comprising hydrated inorganic or organic compounds as well as to a process for prevention of discoloration in polyolefins.
摘要翻译：本发明涉及包含水分无机或有机化合物的脱水添加剂以及防止聚烯烃变色的方法的聚烯烃组合物。

10. 发明申请

US20080132654A1 Polymer Containing Polysiloxane Processing Aid and Catalyst Neutralizer 审中-公开
标题翻译：含聚合物聚合物加工助剂和催化剂中和剂的聚合物
公开(公告)号：US20080132654A1
公开(公告)日：2008-06-05
申请号：US11792458
申请日：2005-11-17
申请人： Thoi H. Ho , Pascal E.R.E.J. Lakeman , Robin J. Lee , Ronald Wevers
发明人： Thoi H. Ho , Pascal E.R.E.J. Lakeman , Robin J. Lee , Ronald Wevers
IPC分类号： C08L83/04 , C08L23/00 , C08L71/02 , C08G77/04
CPC分类号： C08L23/02 , C08L23/0815 , C08L71/02 , C08L83/04 , C08L2205/03 , C08L2205/06 , C08L2666/14 , C08L83/00 , C08L2666/02
摘要： A polymeric composition having improved melt extrusion properties comprising:A) an olefin polymer;B) a cationic derivative of a poly(oxyalkylene) compound; andC) an interactive diorganopolysiloxane compound containing hydroxyl-, carboxylic acid-, di(C1-20 hydrocarbyl)amine-, or C2-10alkenyl- functional groups.
摘要翻译：一种具有改进的熔融挤出性能的聚合物组合物，其包含：A）烯烃聚合物; B）聚（氧化烯）化合物的阳离子衍生物; 和C）含有羟基，羧酸 - ，二（C 1-20 - 烃基）胺或C 2-10 - 烯基 - 官能团的交互式二有机聚硅氧烷化合物。

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