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1. 发明申请

US20100029951A1 Process for producing acrylonitrile compound 有权
公开(公告)号：US20100029951A1
公开(公告)日：2010-02-04
申请号：US12588251
申请日：2009-10-08
申请人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
发明人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
IPC分类号： C07D213/84 , C07C255/18
CPC分类号： C07D231/12
摘要： There is provided a process for stereoselectively producing E-form of 3-acyloxyacrylonitrile compound (3) or Z-form which comprises reacting 3-oxopropionitrile compound (1) with an acid chloride (2), characterized in that the reaction is conducted with removal of hydrogen chloride, or by using an organic base or an inorganic base, to thereby regulate the stereostructure of the product; a process for producing the compound (1) characterized by reacting acetonitrile compound (5) with an aromatic ester compound (6) by use of an alkali metal alkoxide in a hydrocarbon solvent while removing alcohol formed as a by-product by azeotropic distillation in a separating tank; and a process for isomerizing E-form of 3-acyloxyacrylonitrile compound to Z-form thereof by use of an organic base.

2. 发明授权

US08324420B2 Process for producing acrylonitrile compound 有权
公开(公告)号：US08324420B2
公开(公告)日：2012-12-04
申请号：US13137584
申请日：2011-08-26
申请人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
发明人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
IPC分类号： C07C255/03
CPC分类号： C07D231/12
摘要： There is provided a process for stereoselectively producing E-form of 3-acyloxyacrylonitrile compound (3) or Z-form which comprises reacting 3-oxopropionitrile compound (1) with an acid chloride (2), characterized in that the reaction is conducted with removal of hydrogen chloride, or by using an organic base or an inorganic base, to thereby regulate the stereostructure of the product; a process for producing the compound (1) characterized by reacting acetonitrile compound (5) with an aromatic ester compound (6) by use of an alkali metal alkoxide in a hydrocarbon solvent while removing alcohol formed as a by-product by azeotropic distillation in a separating tank; and a process for isomerizing E-form of 3-acyloxyacrylonitrile compound to Z-form thereof by use of an organic base.

3. 发明申请

US20060178523A1 Process for producing acrylonitrile compound 有权
标题翻译：制备丙烯腈化合物的方法
公开(公告)号：US20060178523A1
公开(公告)日：2006-08-10
申请号：US10551041
申请日：2004-03-26
申请人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
发明人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
IPC分类号： C07C255/18
CPC分类号： C07D231/12
摘要： There is provided a process for stereoselectively producing E-form of 3-acyloxyacrylonitrile compound (3) or Z-form which comprises reacting 3-oxopropionitrile compound (1) with an acid chloride (2), characterized in that the reaction is conducted with removal of hydrogen chloride, or by using an organic base or an inorganic base, to thereby regulate the stereostructure of the product; a process for producing the compound (1) characterized by reacting acetonitrile compound (5) with an aromatic ester compound (6) by use of an alkali metal alkoxide in a hydrocarbon solvent while removing alcohol formed as a by-product by azeotropic distillation in a separating tank; and a process for isomerizing E-form of 3-acyloxyacrylonitrile compound to Z-form thereof by use of an organic base.
摘要翻译：提供了一种用于立体选择性地生产3-酰氧基丙烯腈化合物（3）或Z-型的E-型的方法，其包括使3-氧代丙腈化合物（1）与酰氯（2）反应，其特征在于反应进行除去的氯化氢，或通过使用有机碱或无机碱，从而调节产物的立体结构; 一种制备化合物（1）的方法，其特征在于在烃溶剂中使用碱金属醇盐使乙腈化合物（5）与芳族酯化合物（6）反应，同时通过共沸蒸馏除去形成副产物的醇分离罐以及通过使用有机碱将E-型3-酰氧基丙烯腈化合物异构化为Z-形式的方法。

4. 发明授权

US08138368B2 Process for producing acrylonitrile compound 有权
标题翻译：制备丙烯腈化合物的方法
公开(公告)号：US08138368B2
公开(公告)日：2012-03-20
申请号：US12588251
申请日：2009-10-08
申请人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
发明人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
IPC分类号： C07C255/03 , C07C211/78
CPC分类号： C07D231/12
摘要： There is provided a process for stereoselectively producing E-form of 3-acyloxyacrylonitrile compound (3) or Z-form which comprises reacting 3-oxopropionitrile compound (1) with an acid chloride (2), characterized in that the reaction is conducted with removal of hydrogen chloride, or by using an organic base or an inorganic base, to thereby regulate the stereostructure of the product; a process for producing the compound (1) characterized by reacting acetonitrile compound (5) with an aromatic ester compound (6) by use of an alkali metal alkoxide in a hydrocarbon solvent while removing alcohol formed as a by-product by azeotropic distillation in a separating tank; and a process for isomerizing E-form of 3-acyloxyacrylonitrile compound to Z-form thereof by use of an organic base.
摘要翻译：提供了一种用于立体选择性地生产3-酰氧基丙烯腈化合物（3）或Z-型的E-型的方法，其包括使3-氧代丙腈化合物（1）与酰氯（2）反应，其特征在于反应进行除去的氯化氢，或通过使用有机碱或无机碱，从而调节产物的立体结构; 一种制备化合物（1）的方法，其特征在于在烃溶剂中使用碱金属醇盐使乙腈化合物（5）与芳族酯化合物（6）反应，同时通过共沸蒸馏除去形成副产物的醇分离罐以及通过使用有机碱将E-型3-酰氧基丙烯腈化合物异构化为Z-形式的方法。

5. 发明申请

US20110313173A1 Process for producing acrylonitrile compound 有权
标题翻译：制备丙烯腈化合物的方法
公开(公告)号：US20110313173A1
公开(公告)日：2011-12-22
申请号：US13137584
申请日：2011-08-26
申请人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
发明人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
IPC分类号： C07D403/06 , C07D231/12
CPC分类号： C07D231/12
摘要： There is provided a process for stereoselectively producing E-form of 3-acyloxyacrylonitrile compound (3) or Z-form which comprises reacting 3-oxopropionitrile compound (1) with an acid chloride (2), characterized in that the reaction is conducted with removal of hydrogen chloride, or by using an organic base or an inorganic base, to thereby regulate the stereostructure of the product; a process for producing the compound (1) characterized by reacting acetonitrile compound (5) with an aromatic ester compound (6) by use of an alkali metal alkoxide in a hydrocarbon solvent while removing alcohol formed as a by-product by azeotropic distillation in a separating tank; and a process for isomerizing E-form of 3-acyloxyacrylonitrile compound to Z-form thereof by use of an organic base.
摘要翻译：提供了一种用于立体选择性地生产3-酰氧基丙烯腈化合物（3）或Z-型的E-型的方法，其包括使3-氧代丙腈化合物（1）与酰氯（2）反应，其特征在于反应进行除去的氯化氢，或通过使用有机碱或无机碱，从而调节产物的立体结构; 一种制备化合物（1）的方法，其特征在于在烃溶剂中使用碱金属醇盐使乙腈化合物（5）与芳族酯化合物（6）反应，同时通过共沸蒸馏除去形成副产物的醇分离罐以及通过使用有机碱将E-型3-酰氧基丙烯腈化合物异构化为Z-形式的方法。

6. 发明授权

US07649104B2 Process for producing acrylonitrile compound 有权
标题翻译：制备丙烯腈化合物的方法
公开(公告)号：US07649104B2
公开(公告)日：2010-01-19
申请号：US10551041
申请日：2004-03-26
申请人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
发明人： Kenzo Fukuda , Yasuo Kondo , Norio Tanaka , Hideaki Suzuki , Masatoshi Ohnari , Koichi Nishio
IPC分类号： C07C255/07
CPC分类号： C07D231/12
摘要： There is provided a process for stereoselectively producing E-form of 3-acyloxyacrylonitrile compound (3) or Z-form which comprises reacting 3-oxopropionitrile compound (1) with an acid chloride (2), characterized in that the reaction is conducted with removal of hydrogen chloride, or by using an organic base or an inorganic base, to thereby regulate the stereostructure of the product; a process for producing the compound (1) characterized by reacting acetonitrile compound (5) with an aromatic ester compound (6) by use of an alkali metal alkoxide in a hydrocarbon solvent while removing alcohol formed as a by-product by azeotropic distillation in a separating tank; and a process for isomerizing E-form of 3-acyloxyacrylonitrile compound to Z-form thereof by use of an organic base.
摘要翻译：提供了一种用于立体选择性地生产3-酰氧基丙烯腈化合物（3）或Z-型的E-型的方法，其包括使3-氧代丙腈化合物（1）与酰氯（2）反应，其特征在于反应进行除去的氯化氢，或通过使用有机碱或无机碱，从而调节产物的立体结构; 一种制备化合物（1）的方法，其特征在于在烃溶剂中使用碱金属醇盐使乙腈化合物（5）与芳族酯化合物（6）反应，同时通过共沸蒸馏除去形成副产物的醇分离罐以及通过使用有机碱将E-型3-酰氧基丙烯腈化合物异构化为Z-形式的方法。

7. 发明授权

US4445934A Method of manufacturing aluminum by using blast furnace 失效
标题翻译：采用高炉生产铝的方法
公开(公告)号：US4445934A
公开(公告)日：1984-05-01
申请号：US463595
申请日：1983-02-03
申请人： Masao Fujishige , Masayuki Dokiya , Tetsuya Kameyama , Harumi Yokokawa , Seiichi Ujiie , Kenzo Fukuda , Akihiro Motoe
发明人： Masao Fujishige , Masayuki Dokiya , Tetsuya Kameyama , Harumi Yokokawa , Seiichi Ujiie , Kenzo Fukuda , Akihiro Motoe
IPC分类号： C22B21/02
CPC分类号： C22B21/02
摘要： This invention provides a method of smelting aluminum by using a blast furnace. An oxygen gas is introduced into a carbon material packed in a reactor, to burn the same to form a plurality of raceways and a high-temperature reduction region among the raceways. A mixture containing an alumina-containing starting material and a carbon material is then supplied selectively into the high-temperature reduction region while substantially preventing the mixture from contacting the raceways, to reduce the alumina to aluminum.
摘要翻译：本发明提供使用高炉冶炼铝的方法。将氧气引入填充在反应器中的碳材料中，以将其燃烧以在滚道中形成多个滚道和高温还原区域。然后将含有含氧化铝的原料和碳材料的混合物选择性地供入高温还原区域，同时基本上防止混合物与滚道接触，将氧化铝还原成铝。

8. 发明授权

US4588438A Moulded object of alumina matter-containing raw material for aluminum smelting by blast furnace method 失效
标题翻译：通过高炉法生产含铝物质的铝冶炼原料的成型对象
公开(公告)号：US4588438A
公开(公告)日：1986-05-13
申请号：US685229
申请日：1984-12-27
申请人： Masao Fujishige , Masayuki Dokiya , Tetsuya Kameyama , Harumi Yokokawa , Seiichi Ujiie , Kenzo Fukuda
发明人： Masao Fujishige , Masayuki Dokiya , Tetsuya Kameyama , Harumi Yokokawa , Seiichi Ujiie , Kenzo Fukuda
IPC分类号： C22B21/00 , C22B21/02
CPC分类号： C22B21/0007 , C22B21/02
摘要： The present invention provides a moulded object of alumina matter-containing raw material for aluminum smelting by a blast furnace method. The moulded object for aluminum smelting is formed by coating a moulded object comprising the alumina matter-containing raw material and a carbon material with carbon material coating layers on its surface.
摘要翻译：本发明提供一种通过高炉法进行铝冶炼原料的成型体。用于铝冶炼的成型物体通过在其表面上涂覆包含含氧化铝物质的原料的模制物和具有碳材料涂层的碳材料而形成。

9. 发明授权

US6087500A Methods for producing pyrimidine compounds 失效
标题翻译：制备嘧啶化合物的方法
公开(公告)号：US6087500A
公开(公告)日：2000-07-11
申请号：US147260
申请日：1998-11-13
申请人： Kenzo Fukuda , Masataka Hatanaka , Takahiro Makabe , Kenichi Ishii
发明人： Kenzo Fukuda , Masataka Hatanaka , Takahiro Makabe , Kenichi Ishii
IPC分类号： C07D239/46 , C07D239/52 , C07D239/54 , C07D239/545 , C07D239/28 , C07D239/30
CPC分类号： C07D239/47 , C07D239/52 , C07D239/545
摘要： A method for producing 2-amino-4,6-dimethoxypyrimidine, wherein 2-amino-5-chloro-4,6-dimethoxypyrimidine produced by reacting heptachloropropane or hexachloropropene and guanidine with methanol in the presence of a base, or by reacting 2-amino-4,5,6-trichloropyrimidine with methanol in the presence of a base, is used; and a method for producing 2-amino-4,6-dimethoxypyrimidine, characterized by reacting hexachloropropane or pentachloropropene and guanidine with methanol in the presence of a base.
摘要翻译： PCT No.PCT / JP97 / 01534 Sec。 371日期：1998年11月13日 102（e）1998年11月13日PCT PCT 1997年5月7日PCT公布。出版物WO97 / 43265 日期1997年11月20日制备2-氨基-4,6-二甲氧基嘧啶的方法，其中2-碱基-5-氯-4,6-二甲氧基嘧啶通过在碱存在下使七氯丙烷或六氯丙烯与胍与甲醇反应而制得，或在碱存在下使2-氨基-4,5,6-三氯嘧啶与甲醇反应; 以及2-氨基-4,6-二甲氧基嘧啶的制备方法，其特征在于在碱的存在下使六氯丙烷或五氯丙烯与胍与甲醇反应。

10. 发明授权

US4225733A Method for hydrogenating an aromatic compound 失效
标题翻译：芳香族化合物的氢化方法
公开(公告)号：US4225733A
公开(公告)日：1980-09-30
申请号：US919985
申请日：1978-06-28
申请人： Tetsuya Kameyama , Masayuki Dokiya , Kenzo Fukuda
发明人： Tetsuya Kameyama , Masayuki Dokiya , Kenzo Fukuda
IPC分类号： C07C13/48 , C07B31/00 , C07B35/02 , C07B61/00 , C07C1/00 , C07C5/10 , C07C13/18 , C07C67/00
CPC分类号： C07C5/10 , C07C2101/14 , C07C2523/46
摘要： Provided is a method for hydrogenating an aromatic compound by reacting the aromatic compound with hydrogen iodide in the presence of ruthenium catalyst.
摘要翻译：本发明提供一种在钌催化剂存在下使芳族化合物与碘化氢反应来氢化芳族化合物的方法。

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