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1. 发明授权

US5100841A Porous glass and process for its production 失效
标题翻译：多孔玻璃及其生产工艺
公开(公告)号：US5100841A
公开(公告)日：1992-03-31
申请号：US574365
申请日：1990-08-29
申请人： Keisuke Wada , Yasushi Tsurita
发明人： Keisuke Wada , Yasushi Tsurita
IPC分类号： C03C11/00
CPC分类号： C03C11/00
摘要： Porous glass consisting essentially of silica, zirconia and an alkali metal compound, wherein the content of zirconia is at least 5% by weight and the content of the alkali metal compound is at least 2% by weight as calculated as M.sub.2 O wherein M is an alkali metal element, and the total pore volume (A) of pores having pore radii of from 20 to 10,000 .ANG. is at least 0.2 ml/g, and the proportion of the pore volume (B) of pores having pore radii of from 100 to 10,000 .ANG. to the total pore volume (A) of pores having pore radii of from 210 to 10,000 .ANG. is at least 80%.

2. 发明授权

US4978641A Porous glass and process for its production 失效
标题翻译：多孔玻璃及其生产工艺
公开(公告)号：US4978641A
公开(公告)日：1990-12-18
申请号：US393772
申请日：1989-08-15
申请人： Keisuke Wada , Yasushi Tsurita
发明人： Keisuke Wada , Yasushi Tsurita
IPC分类号： C03C11/00
CPC分类号： C03C11/00
摘要： Porous glass consisting essentially of silica, zicronia and an alkali metal compound, wherein the content of zirconia is at least 5% by weight and the content of the alkali metal compound is at least 2% by weight as calculated as M.sub.2 O wherein M is an alkali metal element, and the total pore volume (A) of pores having pore radii of from 20 to 10,000 .ANG. is at least 0.2 ml/g. and the proportion of the pore volume (B) of pores having pore radii of from 100 to 10,000 .ANG. to the total pore volume (A) of pores having pore radii of from 20 to 10,000 .ANG. is at least 80%.
摘要翻译：基本上由二氧化硅，紫苏碱和碱金属化合物组成的多孔玻璃，其中氧化锆的含量为至少5重量％，碱金属化合物的含量为M 2计算的至少2重量％，其中M为碱金属元素，孔半径为20〜10,000的孔的总孔体积（A）为0.2ml / g以上。并且孔半径为100〜10,000Ag的孔的孔体积（B）与孔径为20〜10,000的孔的总孔体积（A）的比例为80％以上。

3. 发明授权

US5530144A Process for producing a phosphorus-vanadium oxide catalyst precursor, process for producing a phosphorus-vanadium oxide catalyst, and process for producing maleic anhydride by vapor phase oxidation using the catalyst 失效
标题翻译：磷钒氧化物催化剂前体的制造方法，磷 - 钒氧化物催化剂的制造方法，使用该催化剂的气相氧化法制造马来酸酐的方法
公开(公告)号：US5530144A
公开(公告)日：1996-06-25
申请号：US359596
申请日：1994-12-20
申请人： Yasushi Tsurita , Masayoshi Murayama , Kenji Shima , Masumi Ito
发明人： Yasushi Tsurita , Masayoshi Murayama , Kenji Shima , Masumi Ito
IPC分类号： B01J27/198 , C01B25/08 , C07C51/215 , C07D307/34 , C01B15/16 , C07D307/36
CPC分类号： C07C51/215 , B01J23/002 , B01J27/198 , C01B25/08 , B01J2523/00
摘要： A process for producing a precursor of a phosphorus-vanadium oxide catalyst for production of maleic anhydride by vapor phase oxidation of a hydrocarbon having 4 carbon atoms, which comprises reacting phosphoric acid and a pentavalent vanadium compound in an organic solvent capable of reducing at least a portion of the pentavalent vanadium to a valence state of +4, the phosphoric acid being substantially composed of orthophosphoric acid, and a phosphoric acid solution whose concentration is 88 to 96% being used as a source of the phosphoric acid; and a process for producing the catalyst comprising dry-pulverizing the catalyst precursor.
摘要翻译：一种用于通过气相氧化具有4个碳原子的烃来生产马来酸酐的磷 - 钒氧化物催化剂的前体的方法，该方法包括使磷酸和五价钒化合物在至少能够还原至少一种五价钒的一部分为+4的价态，磷酸基本上由正磷酸组成，浓度为88〜96％的磷酸溶液用作磷酸源; 以及一种生产该催化剂的方法，包括将该催化剂前体干粉碎。

4. 发明授权

US06692665B2 Lithium managanese oxide, cathode material for lithium secondary battery, cathode, lithium secondary battery and process for manufacturing lithium manganese oxide 有权
标题翻译：锂锰氧化物，锂二次电池用正极材料，阴极锂二次电池及锂锰氧化物的制造方法
公开(公告)号：US06692665B2
公开(公告)日：2004-02-17
申请号：US09843865
申请日：2001-04-30
申请人： Koji Shima , Akira Utsunomiya , Yasushi Tsurita
发明人： Koji Shima , Akira Utsunomiya , Yasushi Tsurita
IPC分类号： C01G4500
CPC分类号： H01M10/052 , C01G45/1242 , C01P2002/32 , C01P2002/52 , C01P2002/54 , C01P2002/86 , C01P2004/32 , C01P2004/61 , C01P2004/62 , C01P2006/12 , C01P2006/40 , H01M4/505 , H01M2004/028
摘要： The invention provides a lithium manganese oxide spinel suited as a cathode active material for lithium ion secondary batteries showing excellent high-temperature cycling behavior. The lithium manganese oxide is represented by the following general formula (1): Li1+&agr;Mn2−&agr;−yMyO4−&dgr; wherein O≦&agr;≦0.5, 0.005≦y≦0.5, −0.1≦&dgr;÷0.1, and M represents a metal element other than Li and Mn, and which shows the ratio of a main peak intensity at 5±40 ppm to a main peak intensity at 525+40 ppm (I0ppm/I500ppm), each intensity being obtained by 7Li-NMR measurement according to the following measuring method, falling within the following range: I0ppm/I500ppm≦0.65y+0.02.
摘要翻译：本发明提供一种锂锰氧化物尖晶石，其适用于锂离子二次电池的正极活性物质，其显示出优异的高温循环性能。锂锰氧化物由以下通式（1）表示：其中O <=α<=0.5,0.005≤y≤0.5,0.1≤δ/ 0.1，M表示除Li以外的金属元素， Mn，其显示5±40ppm的主峰强度与525±40ppm的主峰强度（I0ppm / I500ppm）的比例，各强度根据以下测定得到<7> Li-NMR测定方法，落在以下范围内：

5. 发明授权

US5498731A Oxide catalyst and process for producing maleic anhydride by using oxide catalyst 失效
标题翻译：氧化物催化剂和使用氧化物催化剂生产马来酸酐的方法
公开(公告)号：US5498731A
公开(公告)日：1996-03-12
申请号：US266510
申请日：1994-06-27
申请人： Yasushi Tsurita , Masumi Ito , Ken Shiraga
发明人： Yasushi Tsurita , Masumi Ito , Ken Shiraga
IPC分类号： B01J27/198
CPC分类号： B01J27/198
摘要： An oxide catalyst for producing maleic anhydride by vapor phase oxidation of a hydrocarbon having 4 carbon atoms, obtainable by (1) reacting a pentavalent vanadium compound and a pentavalent phosphorus compound in an organic solvent in the presence of a reducing agent capable of reducing the pentavalent vanadium to the tetravalent state to produce the crystalline composite oxide particles containing tetravalent vanadium and pentavalent phosphorus, (2) dry-pulverizing the obtained crystalline composite oxide particles in a high-speed gas flow, (3) mixing the pulverized particles with an aqueous solution containing tetravalent vanadium and pentavalent phosphorus to form a slurry, and (4) spray-drying the slurry and then calcining.
摘要翻译：一种用于通过气相氧化具有4个碳原子的烃来生产马来酸酐的氧化物催化剂，其可通过以下方式得到：（1）使五价钒化合物和五价磷化合物在有机溶剂中，在还原剂的存在下反应，所述还原剂能够还原五价钒至四价状态，生成含有四价钒和五价磷的结晶复合氧化物粒子，（2）以高速气流将得到的结晶复合氧化物粒子干粉碎，（3）将粉碎的粒子与水溶液含有四价钒和五价磷以形成浆料，（4）喷雾干燥浆料，然后煅烧。

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