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1. 发明授权

US06183865B2 Regenerated cellulosic fibers and process for producing the same 失效
标题翻译：再生纤维素纤维及其制造方法
公开(公告)号：US06183865B2
公开(公告)日：2001-02-06
申请号：US09308608
申请日：1999-07-06
申请人： Kazuyuki Yabuki , Yoshikazu Tanaka , Hisato Kobayashi
发明人： Kazuyuki Yabuki , Yoshikazu Tanaka , Hisato Kobayashi
IPC分类号： D01F200
CPC分类号： D01F2/00 , Y10T428/2913 , Y10T428/2965
摘要： It is an object of the present invention to overcome the problem of fibrillation which is a drawback found in solvent-spun regenerated cellulosic fibers and to thereby provide high-quality regenerated cellulosic fibers. The regenerated cellulosic fibers are produced by the use of a spinning dope of cellulose dissolved in a solvent containing N-methylmorpholine N-oxide under the conditions that the average degree of polymerization of cellulose contained in the spinning dope is held to 400 or lower and 5% to 30% by weight of the cellulose is adjusted to a degree of polymerization of 500 or higher. Thus a pseudo-liquid-crystalline phenomenon can be allowed to occur in the stretched filaments during spinning, so that the resulting regenerated cellulosic fibers have improved resistance to fibrillation as well as improved dyeability and feeling.
摘要翻译：本发明的目的是克服原纤维化问题，这是在溶剂纺丝再生纤维素纤维中发现的缺点，从而提供高质量的再生纤维素纤维。再生纤维素纤维是通过使用溶解在含有N-甲基吗啉N-氧化物的溶剂中的纤维素的纺丝原液在纺丝原液中所含的纤维素的平均聚合度保持在400以下且5以下的条件下制造的将30％（重量）的纤维素调节至聚合度为500以上。因此，在纺丝期间，拉伸长丝中可能会发生伪液晶现象，因此所得到的再生纤维素纤维具有改善的抗纤维化性能，以及改善的染色性和感觉性。

2. 发明授权

US06527987B1 Process for producing regenerated cellulosic fibers 失效
标题翻译：生产再生纤维素纤维的方法
公开(公告)号：US06527987B1
公开(公告)日：2003-03-04
申请号：US09697434
申请日：2000-10-27
申请人： Kazuyuki Yabuki , Yoshikazu Tanaka , Hisato Kobayashi
发明人： Kazuyuki Yabuki , Yoshikazu Tanaka , Hisato Kobayashi
IPC分类号： D01D524
CPC分类号： D01F2/00 , Y10T428/2913 , Y10T428/2965
摘要： It is an object of the present invention to overcome the problem of fibrillation which is a drawback found in solvent-spun regenerated cellulosic fibers and to thereby provide high-quality regenerated cellulosic fibers. The regenerated cellulosic fibers are produced by the use of a spinning dope of cellulose dissolved in a solvent containing N-methylmorpholine N-oxide under the conditions that the average degree of polymerization of cellulose contained in the spinning dope is held to 400 or lower and 5% to 30% by weight of the cellulose is adjusted to a degree of polymerization of 500 or higher. Thus a pseudo-liquid-crystalline phenomenon can be allowed to occur in the stretched filaments during spinning, so that the resulting regenerated cellulosic fibers have improved resistance to fibrillation as well as improved dyeability and feeling.
摘要翻译：本发明的目的是克服原纤维化问题，这是在溶剂纺丝再生纤维素纤维中发现的缺点，从而提供高质量的再生纤维素纤维。再生纤维素纤维是通过使用溶解在含有N-甲基吗啉N-氧化物的溶剂中的纤维素的纺丝原液在纺丝原液中所含的纤维素的平均聚合度保持在400以下且5以下的条件下制造的将30％（重量）的纤维素调节至聚合度为500以上。因此，在纺丝期间，拉伸长丝中可能会发生伪液晶现象，因此所得到的再生纤维素纤维具有改善的抗纤维化性能，以及改善的染色性和感觉性。

3. 发明授权

US5756040A Process of making polybenzazole nonwoven fabric 失效
标题翻译：制造聚吲哚无纺布的工艺
公开(公告)号：US5756040A
公开(公告)日：1998-05-26
申请号：US793039
申请日：1997-01-30
申请人： Kazuyuki Yabuki
发明人： Kazuyuki Yabuki
IPC分类号： D01F6/74 , D04H3/10 , D01D5/06 , D01F6/26 , D02G3/02
CPC分类号： D04H3/10 , D01F6/74
摘要： A continuous process for preparing nonwoven fabrics of polybenzazole filaments, which comprises spinning at least two polybenzazole dope filaments simultaneously, and intermingling and depositing the filaments on a substantially planar collecting surface, thereby forming a nonwoven fabric.
摘要翻译： PCT No.PCT / US95 / 09818 Sec。 371日期1997年1月30日 102（e）1997年1月30日PCT PCT 1995年8月2日PCT公布。出版物WO96 / 04413 日期1996年2月15日制备聚吲哚长丝的无纺布的连续方法，其包括同时旋转至少两种聚吲哚染料丝，并将长丝混合并沉积在基本平坦的收集表面上，从而形成无纺织物。

4. 发明授权

US5527609A Crimped polybenzazole staple fiber and manufacture thereof 失效
标题翻译：卷曲聚吲哚短纤维及其制造
公开(公告)号：US5527609A
公开(公告)日：1996-06-18
申请号：US425493
申请日：1995-04-20
申请人： Kazuyuki Yabuki , Takaharu Ichiryu , Tadao Kuroki , Mitsuhiro Sakuda
发明人： Kazuyuki Yabuki , Takaharu Ichiryu , Tadao Kuroki , Mitsuhiro Sakuda
IPC分类号： C08G73/22 , C08G75/32 , D01F6/74 , D02G3/00
CPC分类号： D01F6/74 , C08G73/22 , C08G75/32 , Y10T428/2904 , Y10T428/2967
摘要： Crimped polybenzazole staple fibers which satisfy the following specifications at the same time:(1) 2.ltoreq.number of crimps (number/inch).ltoreq.40(2) 2.ltoreq.crimp index (%).ltoreq.30(3) 0.3.ltoreq.crimp index/number of crimps.ltoreq.3.0; methods for manufacturing crimped polybenzazole staple fibers; and the rotary cutter therefor. The crimped polybenzazole staple fibers of the present invention are superior in crimp property and are useful for manufacturing spun yarn and unwoven fabric. According to the method of the present invention, crimped polybenzazole staple fibers superior in spinnability can be manufactured with ease. In addition, the cutting blade of the present invention stands a long time use for manufacturing staple fibers from a continuous filaments tow of high tenacity fibers.
摘要翻译：卷曲聚吲哚短纤维同时满足以下规格：（1）2

5. 发明授权

US5851466A Process of making polybenzazole staple fibers 失效
标题翻译：制备聚吲哚短纤维的工艺
公开(公告)号：US5851466A
公开(公告)日：1998-12-22
申请号：US555128
申请日：1995-11-08
申请人： Kazuyuki Yabuki , Takaharu Ichiryu , Tadao Kuroki , Mitsuhiro Sakuda
发明人： Kazuyuki Yabuki , Takaharu Ichiryu , Tadao Kuroki , Mitsuhiro Sakuda
IPC分类号： C08G73/22 , C08G75/32 , D01F6/74 , D01D5/202 , D01D5/26 , D02G1/00
CPC分类号： D01F6/74 , C08G73/22 , C08G75/32 , Y10T428/2904 , Y10T428/2967
摘要： Crimped polybenzazole staple fibers which satisfy the following specifications at the same time: (1) 2.ltoreq.number of crimps (number/inch).ltoreq.40 (2) 2.ltoreq.crimp index (%).ltoreq.30 (3) 0.3.ltoreq.crimp index/number of crimps.ltoreq.3.0; methods for manufacturing crimped polybenzazole staple fibers; and the rotary cutter therefor. The crimped polybenzazole staple fibers of the present invention are superior in crimp property and are useful for manufacturing spun yarn and unwoven fabric. According to the method of the present invention, crimped polybenzazole staple fibers superior in spinnability can be manufactured with ease. In addition, the cutting blade of the present invention stands a long time use for manufacturing staple fibers from a continuous filaments tow of high tenacity fibers.
摘要翻译：卷曲聚吲哚短纤维同时满足以下规格：（1）2

6. 发明授权

US5252407A Rubber composite 失效
标题翻译：橡胶复合材料
公开(公告)号：US5252407A
公开(公告)日：1993-10-12
申请号：US794623
申请日：1991-11-18
申请人： Kiyosuke Kamiyama , Shuzo Sawada , Kazuyuki Yabuki , Yasuo Sano
发明人： Kiyosuke Kamiyama , Shuzo Sawada , Kazuyuki Yabuki , Yasuo Sano
IPC分类号： C08J5/10 , C08K5/35 , B32B27/06 , C08K5/34
CPC分类号： C08J5/10 , C08K5/35 , C08J2321/00 , Y10S156/91 , Y10T428/254 , Y10T428/2969 , Y10T428/31786
摘要： A rubber composite comprising polyester fibers as the reinforcing material, wherein a compound having at least one cyclic imino ether group of a specific structure in its molecule is incorporated in a rubber composite except for adhesive-treated polyester cords.
摘要翻译： PCT No.PCT / JP88 / 00983 Sec。 371日期：1989年5月25日 102（e）日期1989年5月25日PCT提交1988年9月28日PCT公布。公开号WO89 / 02908 日本1989年4月6日。一种包含聚酯纤维作为增强材料的橡胶复合材料，其中在其分子中具有至少一个具有特定结构的环亚氨基醚基团的化合物被加入除了粘合剂处理的聚酯帘线之外的橡胶复合材料中。

7. 发明授权

US5171506A Process for producing polyester fibers 失效
标题翻译：生产聚酯纤维的方法
公开(公告)号：US5171506A
公开(公告)日：1992-12-15
申请号：US683542
申请日：1991-04-10
申请人： Mitsuhiro Sakuda , Kazuyuki Yabuki , Hideaki Ishihara , Yoshimitsu Sakaguchi , Tooru Kitagawa
发明人： Mitsuhiro Sakuda , Kazuyuki Yabuki , Hideaki Ishihara , Yoshimitsu Sakaguchi , Tooru Kitagawa
IPC分类号： C08G63/185 , C08G63/181 , C08G63/19 , C08G63/199 , C08G63/60 , C08G63/66 , C08G63/672 , D01D5/098 , D01F6/62 , D01F6/84
CPC分类号： D01D5/098 , D01F6/84
摘要： Polyester fibers having high tenacity and high modulus can be produced practically and economically by melt-spinning a copolyester at a take-up speed of 3,000 meters/min. or more. The copolyester comprises at least 60 mol % of ethylene terephthalate units, has a persistence length of 15 angstroms or more and does not show a liquid crystalline nature in the molten state.
摘要翻译：具有高强度和高模量的聚酯纤维可以通过以3,000米/分钟的卷取速度熔融纺丝共聚聚酯来实际和经济地生产。或者更多。共聚酯包含至少60摩尔％的对苯二甲酸乙二醇酯单元，其持续长度为15埃以上，并且在熔融状态下不显示液晶性质。

8. 发明授权

US4827999A Polyester fiber having excellent thermal dimensional _ stability, chemical stability and high _ tenacity and process for the production thereof 失效
标题翻译：具有优异的热尺寸稳定性，化学稳定性和高强度的聚酯纤维及其生产方法
公开(公告)号：US4827999A
公开(公告)日：1989-05-09
申请号：US725516
申请日：1985-04-22
申请人： Kazuyuki Yabuki , Yohji Kohmura , Mitsuo Iwasaki , Hiroshi Yasuda
发明人： Kazuyuki Yabuki , Yohji Kohmura , Mitsuo Iwasaki , Hiroshi Yasuda
IPC分类号： D01D5/08 , D01D5/088 , D01F6/62
CPC分类号： D01F6/62 , D01D5/08
摘要： A polyester fiber having excellent thermal dimensional stability and chemical stability as well as high tenacity, which is a drawn yarn produced by melt-spinning a polyester comprising predominantly polyethylene terephthalate, solidification the spun yarn and then drawing the yarn under specified conditions and has specified properties such as intrinsic viscosity, diethylene glycol content, carboxyl group content, birefringence, yarn tenacity and difference of average birefringence between surface and center of monofilament, and further low dry heat shrink and work loss when heat-treated, said polyester fiber being useful as a reinforcement for rubber goods, specifically as a tire cord, and processes for the production of the polyester fiber.
摘要翻译：具有优异的热尺寸稳定性和化学稳定性以及高强度的聚酯纤维，其是通过将主要包含聚对苯二甲酸乙二醇酯的聚酯熔融纺丝制备的拉伸丝，固化该细纱，然后在规定条件下拉伸纱线，并具有特定的性能例如特性粘度，二甘醇含量，羧基含量，双折射率，纱线强度和单丝表面和中心之间的平均双折射差异，以及进一步低热收缩和热处理时的工作损失，所述聚酯纤维可用作橡胶制品的加固，特别是轮胎帘线，以及聚酯纤维的生产方法。

9. 发明授权

US4164114A High strength polyester fibrous products 失效
标题翻译：高强度聚酯纤维制品
公开(公告)号：US4164114A
公开(公告)日：1979-08-14
申请号：US897480
申请日：1978-04-18
申请人： Kazuyuki Yabuki , Mitsuo Iwasaki
发明人： Kazuyuki Yabuki , Mitsuo Iwasaki
IPC分类号： D02G3/48 , B29C70/04 , C08L67/02 , D01F6/92
CPC分类号： D01F6/92 , C08L67/02 , Y10S57/902
摘要： A high strength polyester fibrous product reduced in heat build-up and improved in durability and useful for reinforcing rubber materials, which can be prepared by twisting drawn yarns obtained by (1) melt spinning a polymeric composition comprising polyethylene terephthalate as the main polymer component and at least one methylene group-containing polyester in such an amount that the proportion of the total number of methylene groups to the total number of terephthalic acid residues in all the polymer components is more than 2.0 and less than 2.5,The polyester having a glass transition temperature lower than that of the polyethylene terephthalate and being selected from the group consisting of (i) polyalkylene terephthalates wherein the alkylene unit is a straight chain having 3 to 8 carbon atoms, (ii) polyalkylene isophthalates wherein the alkylene unit is a straight chain having 2 to 6 carbon atoms and (iii) aliphatic polyesters wherein the number of the methylene groups between two ester linkages is from 2 to 10,And (2) drawing the resulting as spun yarns, and having the following melting point (Tm):Tm pet.gtoreq.Tm.gtoreq.Tm pet-10.degree. C.(wherein Tm pet is the melting point of the polyethylene terephthalate) and the following peak temperature (T.alpha.) of the main absorption appearing in the temperature distribution of the mechanical loss tangent when heat treated in the air at 240.degree. C. for 2 minutes while keeping a constant length after the drawing:T.alpha. pet-2.degree. C..gtoreq.T.alpha..gtoreq.T.alpha. pet-20.degree. C.(wherein T.alpha. pet is the peak temperature of the main absorption of the yarns made of polyethylene terephthalate alone drawn and heat treated under the same conditions as applied to the said as spun yarns made of the polymeric composition).
摘要翻译：高强度聚酯纤维制品减少了热量累积并提高了耐久性，并且可用于增强橡胶材料，该橡胶材料可以通过扭转由（1）熔融纺丝包含聚对苯二甲酸乙二醇酯作为主要聚合物组分的聚合物组合物而得到的拉伸丝，以及至少一种含亚甲基的聚酯，其量使得所有聚合物组分中亚甲基总数与对苯二甲酸残基总数的比例大于2.0且小于2。

10. 发明授权

US5948186A Light weight tire including polybenzazole fibers 失效
标题翻译：轻质轮胎，包括聚吲哚纤维
公开(公告)号：US5948186A
公开(公告)日：1999-09-07
申请号：US491832
申请日：1995-07-10
申请人： Kazuyuki Yabuki
发明人： Kazuyuki Yabuki
IPC分类号： B60C9/00 , B60C9/02 , B60C9/18 , C08G73/06 , C08G73/22
CPC分类号： B60C9/0042 , Y10T428/2913 , Y10T428/298
摘要： A tire includes polybenzazole (PBZ) fibers, preferably either polybenzoxazole (PBO) or polybenzothiazole (PBT) fibers which are liquid-crystalline. The PBZ fibers can be incorporated into either the carcass of the tire, the reinforcing belts, or both. Preferably the PBZ fibers have a) a tensile strength of at least 4.0 GPa; b) a tensile modulus of at least 140 GPa; and c) an average void diameter of 25 .ANG. or less.
摘要翻译： PCT No.PCT / US94 / 01404 Sec。 371日期：1995年7月10日 102（e）日期1995年7月10日PCT 1994年2月8日PCT PCT。公开号WO94 / 18015 日期1994年8月18日轮胎包括聚吲哚（PBZ）纤维，优选为液晶的聚苯并恶唑（PBO）或聚苯并噻唑（PBT）纤维。 PBZ纤维可以结合到轮胎的胎体，加强带中或两者中。优选地，PBZ纤维具有a）抗拉强度至少为4.0GPa; b）至少140GPa的拉伸模量; 和c）平均空隙直径为25安培或更小。

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