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1. 发明授权

US5770102A Ice nucleating-active materials and ice bank system 失效
标题翻译：冰成核活性物质和冰蓄积系统
公开(公告)号：US5770102A
公开(公告)日：1998-06-23
申请号：US796283
申请日：1997-02-07
申请人： Kazuo Torii , Hideo Yamamoto , Katuhiro Miyaji , Norio Murase
发明人： Kazuo Torii , Hideo Yamamoto , Katuhiro Miyaji , Norio Murase
IPC分类号： F24F5/00 , C09K5/06
CPC分类号： C09K5/063
摘要： The present invention provides ice nucleating-active materials which are free from problems like corrosiveness against a device owing to the materials used and harmfulness of the materials themselves; and have a function of elevating freezing temperature of water which is effective for releasing an over-cooling state of it, and generates a method for an ice bank system exhibiting a large energy-saving effect. This invention relates to ice nucleating-active materials containing trioctahedral smectites capable of being dispersive in water as effective components, and a method for an ice bank system comprising adding the trioctahedral smectites into a liquid in the ice bank system at a concentration of at least 30 ppm and freezing it by using a freezer.
摘要翻译：本发明提供了冰成核活性材料，其由于所使用的材料和材料本身的有害性而没有诸如对装置的腐蚀性的问题; 并且具有提高有效释放其过冷却状态的水的冷冻温度的功能，并且产生显示出大的节能效果的冰库系统的方法。本发明涉及含有能够作为有效成分分散在水中的三八面体蒙皂石的冰成核活性物质，以及一种用于冰库系统的方法，其包括将三八面体蒙皂石以至少30的浓度加入到冰库系统中的液体中 ppm，并使用冷冻器冷冻。

2. 发明授权

US07022842B2 Process for synthesizing beta-lactam 失效
标题翻译： β-内酰胺合成方法
公开(公告)号：US07022842B2
公开(公告)日：2006-04-04
申请号：US10450450
申请日：2001-03-07
申请人： Kiyotaka Hatakeda , Osamu Sato , Mitsuhiro Kanakubo , Yutaka Ikushima , Kazuo Torii
发明人： Kiyotaka Hatakeda , Osamu Sato , Mitsuhiro Kanakubo , Yutaka Ikushima , Kazuo Torii
IPC分类号： C07B43/06 , C07D205/08
CPC分类号： C07D201/08 , Y02P20/582
摘要： It is an object of the present invention to provide a method for synthesizing β-lactams and a method for manufacturing β-lactams in water of high-temperature and under high-pressure, and the present invention relates to a β-lactam synthesis method which is characterized in that β-lactams are synthesized by reacting β-amino acids in water at high-temperature and under high-pressure, this method being further characterized in that β-lactams are synthesized at a high speed by cyclizing β-amino acids in water at high-temperature and under high-pressure in which the temperature range is 200° C. or higher and the pressure range is 10 MPa or greater, and the present invention also relates to a method for manufacturing β-lactams which is characterized in that β-lactams are synthesized by reacting β-amino acids in water at high-temperature and under high-pressure, and are then separated and purified using a column separation medium.
摘要翻译：本发明的一个目的是提供一种合成β-内酰胺的方法和一种在高温和高压水中制备β-内酰胺的方法，本发明涉及一种β-内酰胺合成方法，其特征在于β-内酰胺是通过在高温和高压下在水中使β-氨基酸反应合成的，该方法的进一步特征在于通过使β-氨基酸在高温和高压下环化β-氨基酸来高速合成β-内酰胺在温度范围为200℃以上且压力范围为10MPa以上的高温高压下的水，本发明还涉及β-内酰胺的制造方法，其特征在于，该β-内酰胺通过在高温和高压下在水中使β-氨基酸反应合成，然后使用柱分离介质分离和纯化。

3. 发明授权

US5573673A Hydrous composite cerium-phosphorus oxide for immobilization of strontium ions in solution 失效
标题翻译：用于在溶液中固定锶离子的水性复合铈 - 磷氧化物
公开(公告)号：US5573673A
公开(公告)日：1996-11-12
申请号：US404097
申请日：1995-03-14
申请人： Hiromichi Hayashi , Yoshio Onodera , Takashi Iwasaki , Osamu Itabashi , Kazuo Torii
发明人： Hiromichi Hayashi , Yoshio Onodera , Takashi Iwasaki , Osamu Itabashi , Kazuo Torii
IPC分类号： B01D15/00 , B01J20/02 , C01F11/00 , G21F9/12 , C01F17/00 , C02F1/42
CPC分类号： B01J20/02 , B01J20/0207 , B01J20/0292 , G21F9/12
摘要： Disclosed is a novel hydrous composite oxide of cerium (IV) and phosphorus characterized by the specified chemical composition and the unique X-ray diffractometric pattern, which is useful as an adsorbent or immobilizing agent of strontium ions in an aqueous solution such as radioactive wastes from atomic power plants. The composite oxide prepared by the precipitation reaction of a Ce (IV) salt in an aqueous solution and phosphoric acid can be imparted with an increased adsorption capacity for strontium ions when the precipitates are heat-treated under hydrothermal conditions at up to 300.degree. C. Immobilization of strontium ions adsorbed on the adsorbent can be more complete when the adsorbent bearing strontium ions is dried and subjected to a heat treatment at a temperature of 200.degree. C. or higher.
摘要翻译：公开了一种铈（Ⅳ）和磷的新型含水复合氧化物，其特征在于具有特定的化学成分和独特的X射线衍射图谱，其可用作锶离子在水溶液中的吸附剂或固定剂，例如放射性废物原子能发电厂。当在高达300℃的水热条件下对沉淀物进行热处理时，通过Ce（IV）盐在水溶液中的沉淀反应制备的复合氧化物可以赋予锶离子增加的吸附能力。当吸附剂负载锶离子干燥并在200℃或更高的温度下进行热处理时，吸附在吸附剂上的锶离子的固定可以更完整。

4. 发明授权

US07250537B2 Method of hydrogenating phenol 失效
标题翻译：氢化苯酚的方法
公开(公告)号：US07250537B2
公开(公告)日：2007-07-31
申请号：US10553792
申请日：2004-03-30
申请人： Masayuki Shirai , Chandrashekhar Vasant Rode , Uday Dattopant Joshi , Kazuo Torii , Takafumi Sato
发明人： Masayuki Shirai , Chandrashekhar Vasant Rode , Uday Dattopant Joshi , Kazuo Torii , Takafumi Sato
IPC分类号： C07C45/00 , C07C27/00 , C07C29/00
CPC分类号： C07C29/20 , C07C29/145 , C07C45/006 , C07C2601/14 , C07C2602/10 , C07C2602/28 , Y02P20/52 , C07C49/403 , C07C49/67 , C07C35/08 , C07C35/36
摘要： The present invention provides a novel method of hydrogenating a phenol for hydrogenating a phenol industrially advantageously. The present invention relates, in the case of phenol hydrogenation in which carbon dioxide is made to participate in the reaction, to a method of hydrogenating a phenol characterized by using a supported rhodium and/or ruthenium catalyst, whereby the phenol is hydrogenated efficiently at a lower reaction temperature than with prior art; such a method characterized in that carbon dioxide having a temperature of 20 to 250° C. and a pressure of 0.1 to 50 MPa is used as the carbon dioxide; and such a method characterized in that hydrogen under conditions of a temperature of 20 to 250° C. and a pressure of 0.1 to 50 MPa is used.An environmentally friendly phenol hydrogenation process that uses no harmful organic solvents can be realized.
摘要翻译：本发明提供了一种氢化苯酚以在工业上有利地氢化酚的新方法。本发明涉及在其中使二氧化碳参与反应的苯酚氢化的情况下，以使用负载的铑和/或钌催化剂为特征的苯酚氢化方法，由此苯酚在比现有技术低的反应温度; 这种方法的特征在于使用温度为20〜250℃，压力为0.1〜50MPa的二氧化碳作为二氧化碳; 其特征在于，在温度为20〜250℃，压力为0.1〜50MPa的条件下使用氢。可以实现不使用有害有机溶剂的环保酚加氢方法。

5. 发明授权

US07071350B2 Method of introducing amino group and method of synthesizing amino acid compound 失效
标题翻译：引入氨基的方法和合成氨基酸化合物的方法
公开(公告)号：US07071350B2
公开(公告)日：2006-07-04
申请号：US10450157
申请日：2001-10-30
申请人： Kiyotaka Hatakeda , Osamu Sato , Mitsuhiro Kanakubo , Yutaka Ikushima , Kazuo Torii
发明人： Kiyotaka Hatakeda , Osamu Sato , Mitsuhiro Kanakubo , Yutaka Ikushima , Kazuo Torii
IPC分类号： C07C61/00 , C07C229/00 , C07C205/00
CPC分类号： C07C227/08 , C07C227/40 , C07C229/08 , C07C229/24 , C07C229/26
摘要： The present invention relates to a method for introducing an amino group into an organic acid or an organic ester by reacting an organic salt or an organic ester and ammonia under high-temperature and high-pressure water conditions, a method for synthesizing an amino acid or an amino ester by the above method, and a method for manufacturing an amino acid compound by synthesizing an amino acid or an amino ester by the above method and separating and refining it with an ion exchange resin.
摘要翻译：本发明涉及通过有机盐或有机酯与氨在高温高压水条件下反应而将氨基引入有机酸或有机酯的方法，用于合成氨基酸或通过上述方法的氨基酯，以及通过用上述方法合成氨基酸或氨基酯制备氨基酸化合物的方法，并用离子交换树脂分离和精制。

6. 发明申请

US20060194989A1 Method of hydrogenating phenol 失效
标题翻译：氢化苯酚的方法
公开(公告)号：US20060194989A1
公开(公告)日：2006-08-31
申请号：US10553792
申请日：2004-03-30
申请人： Masayuki Shirai , Chandrashekhar Rode , Uday Joshi , Kazuo Torii , Takafumi Sato
发明人： Masayuki Shirai , Chandrashekhar Rode , Uday Joshi , Kazuo Torii , Takafumi Sato
IPC分类号： C07C49/175
CPC分类号： C07C29/20 , C07C29/145 , C07C45/006 , C07C2601/14 , C07C2602/10 , C07C2602/28 , Y02P20/52 , C07C49/403 , C07C49/67 , C07C35/08 , C07C35/36
摘要： The present invention provides a novel method of hydrogenating a phenol for hydrogenating a phenol industrially advantageously. The present invention relates, in the case of phenol hydrogenation in which carbon dioxide is made to participate in the reaction, to a method of hydrogenating a phenol characterized by using a supported rhodium and/or ruthenium catalyst, whereby the phenol is hydrogenated efficiently at a lower reaction temperature than with prior art; such a method characterized in that carbon dioxide having a temperature of 20 to 250° C. and a pressure of 0.1 to 50 MPa is used as the carbon dioxide; and such a method characterized in that hydrogen under conditions of a temperature of 20 to 250° C. and a pressure of 0.1 to 50 MPa is used. An environmentally friendly phenol hydrogenation process that uses no harmful organic solvents can be realized.
摘要翻译：本发明提供了一种氢化苯酚以在工业上有利地氢化酚的新方法。本发明涉及在其中使二氧化碳参与反应的苯酚氢化的情况下，以使用负载的铑和/或钌催化剂为特征的苯酚氢化方法，由此苯酚在比现有技术低的反应温度; 这种方法的特征在于使用温度为20〜250℃，压力为0.1〜50MPa的二氧化碳作为二氧化碳; 其特征在于，在温度为20〜250℃，压力为0.1〜50MPa的条件下使用氢。可以实现不使用有害有机溶剂的环保酚加氢方法。

7. 发明授权

US06750336B2 Method of production of lactam 失效
标题翻译：内酰胺的生产方法
公开(公告)号：US06750336B2
公开(公告)日：2004-06-15
申请号：US10285571
申请日：2002-11-01
申请人： Osamu Sato , Kiyotaka Hatakeda , Yutaka Ikushima , Kazuo Torii
发明人： Osamu Sato , Kiyotaka Hatakeda , Yutaka Ikushima , Kazuo Torii
IPC分类号： C07D20104
CPC分类号： C07D201/04 , Y02P20/582
摘要： A method for producing a lactam by using an organic solvent as a substrate solution, which makes it possible to introduce a high-concentration oxime into flowing high-temperature and high-pressure water, thereby allowing the high-concentration lactam to be synthesized with a high efficiency. With this method, the lactam is continuously synthesized at a high rate from the oxime under high-temperature and high-pressure water mixture conditions within a temperature range of no less than 250° C. and a pressure range of no less than 15 MPa.
摘要翻译：通过使用有机溶剂作为底物溶液制备内酰胺的方法，可以将高浓度肟引入流动的高温高压水中，从而使高浓度的内酰胺与高效率。通过该方法，在不低于250℃的温度范围和不低于15MPa的压力范围内，在高温和高压水混合条件下，从肟连续合成内酰胺。

8. 发明授权

US5595716A Synthetic mixed-layer silicate and method for the preparation thereof 失效
标题翻译：合成混合层状硅酸盐及其制备方法
公开(公告)号：US5595716A
公开(公告)日：1997-01-21
申请号：US516533
申请日：1995-08-18
申请人： Kazuo Torii , Takashi Iwasaki , Yoshio Onodera
发明人： Kazuo Torii , Takashi Iwasaki , Yoshio Onodera
IPC分类号： C01B33/38 , B01J21/16 , C01B33/40
CPC分类号： C01B33/40 , B01J21/16
摘要： A novel synthetic mixed-layer silicate consisting of the layers of serpentine and layers of saponite each having a specified chemical composition is proposed, which has excellent dispersibility in water to form a colloidal dispersion capable of being converted into a gel by standing to be useful as a gelating agent exhibiting thixotropy along with unique porosity characteristics which enable the use thereof as an adsorbent. The mixed-layer silicate is prepared by the process comprising the steps of: (a) preparing an acidic aqueous solution containing silicic acid, magnesium salt and aluminum salt; (b) alkalifying the solution by the addition of an alkaline compound to precipitate a hydrous composite oxide containing silicon, magnesium and aluminum; (c) collecting the precipitates of the hydrous composite oxide; (d) admixing the precipitates of the hydrous composite oxide with an aqueous solution of an alkali metal hydroxide to give an aqueous slurry; and (e) subjecting the aqueous slurry of the hydrous composite oxide to a hydrothermal treatment by heating at a temperature up to 500.degree. C.
摘要翻译：提出了由蛇纹石层和皂石层组成的新型合成混合层状硅酸盐，它们都具有特定的化学成分，其在水中具有优异的分散性，从而形成能够通过静置转化为凝胶的胶体分散体，以用作具有触变性以及独特的孔隙特性的凝胶剂，其能够用作吸附剂。混合层硅酸盐通过包括以下步骤的方法制备：（a）制备含有硅酸，镁盐和铝盐的酸性水溶液; （b）通过加入碱性化合物使溶液碱化以沉淀含硅，镁和铝的含水复合氧化物; （c）收集含水复合氧化物的析出物; （d）将含水复合氧化物的沉淀物与碱金属氢氧化物的水溶液混合，得到含水浆液; 和（e）在高达500℃的温度下加热水合复合氧化物的水性浆料进行水热处理。

9. 发明授权

US5559070A Synthetic inorganic porous material and method for the preparation thereof 失效
标题翻译：合成无机多孔材料及其制备方法
公开(公告)号：US5559070A
公开(公告)日：1996-09-24
申请号：US319573
申请日：1994-10-07
申请人： Kazuo Torii , Takashi Iwasaki , Yoshio Onodera , Hiromichi Hayashi
发明人： Kazuo Torii , Takashi Iwasaki , Yoshio Onodera , Hiromichi Hayashi
IPC分类号： B01J20/18 , B01J20/10 , B01J21/10 , B01J23/00 , B01J23/755 , C01B33/20 , G03G15/01 , G06T1/00 , G06T5/00 , H04N1/409 , H04N1/46 , H04N1/60 , B01J21/08
CPC分类号： B01J23/755 , B01J21/10 , B01J23/002 , B01J2523/00
摘要： Proposed is a novel synthetic inorganic porous material having a chemical composition of the general formula[(SiO.sub.2).sub.8 .multidot.(MO.sub.2/3).sub.a .multidot.(OH).sub.2/3a+b ].sup.b- .multidot.b/c(A.sup.c+),in which M is an ion of a divalent metal, e.g., Mg, A is a cation of an alkali metal, alkaline earth metal, hydrogen or ammonium, the subscript a is a positive number of 3 to 10, b is a positive number of 0.1 to 1 and c is a positive number of 1 to 2, and characterized by a specific surface area of 100 to 800 m.sup.2 /g, average pore diameter of 2 to 8 nm, pore volume of 0.1 to 0.8 cm.sup.3 /g and cation exchange capacity of 0.1 to 1.2 meq/g. This porous material is prepared by a method comprising the steps of: (a) mixing an aqueous solution of sodium silicate and an aqueous solution of a water-soluble salt of a divalent metal M, e.g., magnesium, to form hydrous oxides; (b) separating the hydrous oxides from the precipitation medium; (c) subjecting an aqueous slurry of the hydrous oxides to a hydrothermal reaction at a temperature of from 100.degree. to 300.degree. C.; and (d) drying and heating the hydrothermally obtained product at a temperature of from 100.degree. to 1000.degree. C. to effect dehydration.
摘要翻译：提出了具有通式[（SiO 2）8x（MO + E，fra 2/3 + EE）ax（OH）+ E，fra 2/3 + EE a + b]的化学组成的新型合成无机多孔材料。 b-xb / c（Ac +），其中M为二价金属的离子，例如Mg，A为碱金属，碱土金属，氢或铵的阳离子，下标a为正数3 至10，b为0.1〜1的正数，c为1〜2的正数，特征在于比表面积为100〜800m 2 / g，平均孔径为2〜8nm，孔体积为 0.1〜0.8cm 3 / g，阳离子交换容量为0.1〜1.2meq / g。这种多孔材料是通过包括以下步骤的方法制备的：（a）将硅酸钠水溶液与二价金属M例如镁的水溶性盐的水溶液混合以形成水合氧化物; （b）从沉淀介质中分离含水氧化物; （c）使水合氧化物的水性浆料在100℃至300℃的温度下进行水热反应; 和（d）在100℃至1000℃的温度下干燥并加热水热制得的产物以进行脱水。

10. 发明授权

US07084269B2 Process for producing lactam 失效
标题翻译：生产内酰胺的方法
公开(公告)号：US07084269B2
公开(公告)日：2006-08-01
申请号：US10471750
申请日：2002-03-05
申请人： Kiyotaka Hatakeda , Osamu Sato , Yutaka Ikushima , Kazuo Torii
发明人： Kiyotaka Hatakeda , Osamu Sato , Yutaka Ikushima , Kazuo Torii
IPC分类号： C07D201/04
CPC分类号： C07D201/04
摘要： It is an object of the present invention to provide an efficient method of continuously producing a lactam in high-temperature high-pressure water, and the present invention relates to a method of producing a lactam characterized by efficiently synthesizing the lactam while suppressing oxime hydrolysis by introducing an oxime as a reaction substrate and an acid into a reaction zone through which high-temperature high-pressure water is flowing, or introducing an oxime into flowing high-temperature high-pressure water containing an acid, thus raising the temperature of the reaction substrate to put the reaction substrate into a prescribed high-temperature high-pressure state within a short time and subjecting the reaction substrate to reaction; through the method, the lactam can be efficiently and continuously synthesized at a high rate from the oxime using an acid catalyst in water at a high temperature of at least 250° C. and a high pressure of at least 15 MPa.
摘要翻译：本发明的目的是提供一种在高温高压水中连续生产内酰胺的有效方法，本发明涉及一种制备内酰胺的方法，其特征在于在抑制肟水解的同时有效地合成内酰胺将肟作为反应基质和酸引入高温高压水流过的反应区，或将肟引入流入含有酸的高温高压水中，从而提高反应温度将反应基材在短时间内放入规定的高温高压状态，使反应基板反应; 通过该方法，可以使用酸催化剂在高温下在高温至少250℃，高压至少15MPa的水中，以高速从肟高效连续地合成内酰胺。

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