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1. 发明授权

US5853693A Hydrogenation catalyst for production of hydrogen peroxide, and method for preparation of same 失效
标题翻译：用于生产过氧化氢的氢化催化剂及其制备方法
公开(公告)号：US5853693A
公开(公告)日：1998-12-29
申请号：US820085
申请日：1997-03-19
申请人： Kazuharu Ogasawara , Tomio Kato , Norikazu Okuda , Tetsuya Konishi , Kenji Kato
发明人： Kazuharu Ogasawara , Tomio Kato , Norikazu Okuda , Tetsuya Konishi , Kenji Kato
IPC分类号： B01J23/44 , B01J35/10 , C01B15/023
CPC分类号： B01J23/44 , B01J35/1038 , B01J35/1042 , B01J35/1061 , C01B15/023
摘要： A method for preparing hydrogen peroxide in accordance with an anthraquinone method, comprising hydrogenating at least one anthraquinone with a hydrogenation catalyst comprising palladium and at least one alkali metal, supported on a silica carrier, wherein the at least one alkali metal is in an amount of 0.1% to 5 wt % based on the weight of the silica carrier.
摘要翻译：一种根据蒽醌法制备过氧化氢的方法，包括用负载在二氧化硅载体上的包含钯和至少一种碱金属的氢化催化剂氢化至少一种蒽醌，其中所述至少一种碱金属的量为相对于二氧化硅载体的重量为0.1〜5重量％。

2. 发明授权

US06126914A Hydrogenation catalyst for production of hydrogen peroxide, and method for preparation of same 有权
标题翻译：用于生产过氧化氢的氢化催化剂及其制备方法
公开(公告)号：US06126914A
公开(公告)日：2000-10-03
申请号：US314537
申请日：1999-05-19
申请人： Kazuharu Ogasawara , Tomio Kato , Norikazu Okuda , Tetsuya Konishi , Kenji Kato
发明人： Kazuharu Ogasawara , Tomio Kato , Norikazu Okuda , Tetsuya Konishi , Kenji Kato
IPC分类号： B01J23/44 , B01J35/10 , C01B15/023
CPC分类号： B01J23/44 , B01J35/1038 , B01J35/1042 , B01J35/1061 , C01B15/023
摘要： A hydrogenation catalyst for the production of hydrogen peroxide by the hydrogenation of anthraquinones in accordance with a hydrogen peroxide production process utilizing an anthraquinone method. The catalyst includes palladium supported on a carrier. The carrier comprises spherical silica particles, wherein at least 90 wt % of the silica particles have particle diameters of 10 to 100 .mu.m. The silica particles have an average particle diameter of 30 to 60 .mu.m and a pore volume of 0.4 to 1.0 ml/g. The catalyst has desirable activity, strength, service life and selectivity.
摘要翻译：根据使用蒽醌法的过氧化氢生产方法，通过氢化蒽醌生产过氧化氢的氢化催化剂。催化剂包括负载在载体上的钯。载体包括球形二氧化硅颗粒，其中至少90重量％的二氧化硅颗粒具有10至100μm的粒径。二氧化硅粒子的平均粒径为30〜60μm，孔体积为0.4〜1.0ml / g。该催化剂具有所需的活性，强度，使用寿命和选择性。

3. 依法登记的发明

USH1787H Regeneration method of working solution 失效
标题翻译：工作液再生方法
公开(公告)号：USH1787H
公开(公告)日：1999-02-02
申请号：US829696
申请日：1997-03-26
申请人： Kazuharu Ogasawara , Tomio Kato , Kazuyuki Minato , Kenji Kato , Makoto Sumitani
发明人： Kazuharu Ogasawara , Tomio Kato , Kazuyuki Minato , Kenji Kato , Makoto Sumitani
IPC分类号： C01B15/023 , C07C50/18
CPC分类号： C01B15/023
摘要： A regeneration method of a working solution is herein disclosed in which various by-products which do not participate in the production of hydrogen peroxide and which are present in the working solution in a hydrogen peroxide production process utilizing an anthraquinone method can efficiently be converted into anthraquinones effective as reaction media for the production of hydrogen peroxide.The present invention is concerned with (1) a regeneration method of a working solution wherein at least a part of the unreduced working solution is brought into contact with a catalyst mainly comprising a .gamma.-alumina at a temperature of 40 to 150.degree. C., and (2) another regeneration method of a working solution wherein the working solution is brought into contact with a catalyst mainly comprising a .gamma.-alumina at a temperature of 20 to 150.degree. C. under conditions that a concentration h (mol/liter) of the alkyltetrahydroanthrahydroquinones in the working solution before the catalytic treatment meets the equation(0.0018.times.t-0.0285).times.h
摘要翻译：本文公开了一种工作溶液的再生方法，其中不参与过氧化氢生产的各种副产物在使用蒽醌方法的过氧化氢生产过程中存在于工作溶液中的各种副产物可有效地转化为蒽醌作为生产过氧化氢的反应介质有效。本发明涉及（1）一种工作溶液的再生方法，其中至少一部分未还原的工作溶液与主要包含γ-氧化铝的催化剂在40〜150℃的温度下接触，和（2）工作溶液的另一种再生方法，其中使工作溶液与主要包含γ-氧化铝的催化剂在20至150℃的温度下接触，在浓度h（mol / l）在催化处理之前的工作溶液中的烷基四氢蒽醌符合方程（0.0018xt-0.0285）xh <0.05，其中t为处理温度（℃），将工作溶液中的烷基四氢加成蒽转化为烷基四氢蒽醌。

4. 发明授权

US5399333A Process for producing hydrogen peroxide 失效
标题翻译：生产过氧化氢的方法
公开(公告)号：US5399333A
公开(公告)日：1995-03-21
申请号：US162305
申请日：1993-12-06
申请人： Tomio Kato , Yukio Ishiuchi , Hiroshi Takamiya , Kazuharu Ogasawara , Kazuyuki Minato
发明人： Tomio Kato , Yukio Ishiuchi , Hiroshi Takamiya , Kazuharu Ogasawara , Kazuyuki Minato
IPC分类号： C01B15/023
CPC分类号： C01B15/023
摘要： A process for producing hydrogen peroxide by subjecting a working solution containing anthraquinones as the reaction medium, to reduction and oxidation alternately, which process is characterized in that (1) the anthraquinones as the reaction medium contained in the working solution are a mixture of an alkyl-substituted anthraquinone and an alkyl-substituted tetrahydroanthraquinone, (2) in the reduction step, the total amount of the alkyl-substituted tetrahydroanthraquinone in the working solution and part or the total amount of the alkyl-substituted anthraquinone in the working solution are reduced, and (3) in the working solution after the reduction step, the content of the alkyl-substituted anthrahydroquinone formed is kept higher than the content of the alkyl-substituted tetrahydroanthrahydroquinone formed.
摘要翻译：通过对含有蒽醌作为反应介质的工作溶液进行交替的还原和氧化而生产过氧化氢的方法，其特征在于：（1）工作溶液中含有的作为反应介质的蒽醌是烷基取代的蒽醌和烷基取代的四氢蒽醌，（2）在还原步骤中，工作溶液中烷基取代的四氢蒽醌的总量和工作溶液中烷基取代的蒽醌的总量以及总量减少，和（3）在还原步骤后的工作溶液中，形成的烷基取代的蒽醌的含量保持高于形成的烷基取代的四氢蒽氢醌的含量。

5. 发明授权

US4751022A Humidity-sensing component composition 失效
标题翻译：湿度传感元件组成
公开(公告)号：US4751022A
公开(公告)日：1988-06-14
申请号：US37997
申请日：1987-04-14
申请人： Akitoshi Sugio , Tadashi Shimomura , Hidechika Wakabayashi , Osamu Kondo , Kazuharu Ogasawara , Chiharu Nishizawa
发明人： Akitoshi Sugio , Tadashi Shimomura , Hidechika Wakabayashi , Osamu Kondo , Kazuharu Ogasawara , Chiharu Nishizawa
IPC分类号： G01N27/12 , H01B1/06
CPC分类号： G01N27/121
摘要： A humidity-sensing component composition includes a metallic oxide and a chalcogen oxyacid salt represented by a general formula A.sub.x B.sub.y O.sub.z where A is one of an alkali metal and an alkaline earth metal, B is one of sulphur, selenium, and tellurium, O is oxygen, x is 1 to 2, y 1 to 5, and z 2 to 7. The chalcogen oxyacid salt is blended by an amount of 0.01 to 99.99 mol % in the metallic oxide with the sum of the metallic oxide and the chalcogen oxyacid salt as a reference. The metallic oxide and the chalcogen oxyacid salt are sintered under an atmosphere of molecular oxygen.
摘要翻译：湿度感测组分组合物包括金属氧化物和由通式AxByOz表示的硫族元素含氧酸盐，其中A是碱金属和碱土金属之一，B是硫，硒和碲之一，O是氧， x为1〜2，y 1〜5，z 2〜7。金属氧化物中的硫属元素含氧酸盐的配合量为0.01〜99.99摩尔％，金属氧化物和硫属元素含氧酸盐的总量为参考。金属氧化物和硫属元素含氧酸盐在分子氧气氛下烧结。

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