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1. 发明授权

US08124690B2 Moisture curable polymer having SiF group, and curable composition containing the same 有权
标题翻译：具有SiF基的水分固化性聚合物和含有它们的固化性组合物
公开(公告)号：US08124690B2
公开(公告)日：2012-02-28
申请号：US12441270
申请日：2007-08-23
申请人： Katsuyu Wakabayashi , Taisuke Sasaki
发明人： Katsuyu Wakabayashi , Taisuke Sasaki
IPC分类号： C08L83/12
CPC分类号： C08G65/33306 , C08G65/2609 , C08G65/2663 , C08G65/30 , C08G65/323 , C08G65/33317 , C08G65/336 , C08G65/337 , C08G2650/48 , C08L71/02 , C08L2666/22 , C09J143/04 , C09J171/02
摘要： A moisture curable polymer and a curable composition having superior curability are provided. A polymer having a silicon group represented by the general formula: —SiFaR1bZc (wherein, R1 represents any one of a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms, or an organosiloxy group represented by R23SiO— (R2 is each independently, a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms). Z is a hydroxyl group or a hydrolyzable group other than fluorine. a is any one of 1, 2, or 3; b is any one of 0, 1, or 2; c is any one of 0, 1, or 2; and a+b+c is 3. When b or c is 2, two R1 or two Z may be each the same or different) and a curable composition including this polymer, and a sealant and an adhesive in which the curable composition is used.
摘要翻译：提供了一种可湿固化聚合物和具有优异固化性的可固化组合物。具有由以下通式表示的硅基的聚合物：-SiFaR1bZc（其中，R1表示取代或未取代的碳原子数1〜20的烃基或由R23SiO-表示的有机甲硅烷氧基（R2各自独立地为取代或未取代的碳原子数1〜20的烃基）Z是除氟以外的羟基或水解性基团，a为1,2或3中任一个，b为0,1或2中任一个， c是0，1或2中的任一个; a + b + c为3.当b或c为2时，两个R 1或两个Z可以相同或不同）和包含该聚合物的可固化组合物和使用可固化组合物的密封剂和粘合剂。

2. 发明申请

US20090275702A1 MOISTURE CURABLE POLYMER HAVING SiF GROUP, AND CURABLE COMPOSITION CONTAINING THE SAME 有权
标题翻译：具有SiF组的水分可固化聚合物和含有它的可固化组合物
公开(公告)号：US20090275702A1
公开(公告)日：2009-11-05
申请号：US12441270
申请日：2007-08-23
申请人： Katsuyu Wakabayashi , Taisuke Sasaki
发明人： Katsuyu Wakabayashi , Taisuke Sasaki
IPC分类号： C08L83/08 , C08G77/24
CPC分类号： C08G65/33306 , C08G65/2609 , C08G65/2663 , C08G65/30 , C08G65/323 , C08G65/33317 , C08G65/336 , C08G65/337 , C08G2650/48 , C08L71/02 , C08L2666/22 , C09J143/04 , C09J171/02
摘要： A moisture curable polymer and a curable composition having superior curability are provided. A polymer having a silicon group represented by the general formula: —SiFaR1bZc (wherein, R1 represents any one of a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms, or an organosiloxy group represented by R23SiO— (R2 is each independently, a substituted or unsubstituted hydrocarbon group having 1 to 20 carbon atoms). Z is a hydroxyl group or a hydrolyzable group other than fluorine. a is any one of 1, 2, or 3; b is any one of 0, 1, or 2; c is any one of 0, 1, or 2; and a+b+c is 3. When b or c is 2, two R1 or two Z may be each the same or different) and a curable composition including this polymer, and a sealant and an adhesive in which the curable composition is used.
摘要翻译：提供了一种可湿固化聚合物和具有优异固化性的可固化组合物。具有由以下通式表示的硅基的聚合物：-SiFaR1bZc（其中，R1表示取代或未取代的碳原子数1〜20的烃基或由R23SiO-表示的有机甲硅烷氧基（R2各自独立地为取代或未取代的碳原子数1〜20的烃基）Z是除氟以外的羟基或水解性基团，a为1,2或3中任一个，b为0,1或2中任一个， c是0，1或2中的任一个; a + b + c为3.当b或c为2时，两个R 1或两个Z可以相同或不同）和包含该聚合物的可固化组合物和使用可固化组合物的密封剂和粘合剂。

3. 发明授权

US09051501B2 Curable composition and catalyst composition 有权
标题翻译：可固化组合物和催化剂组成
公开(公告)号：US09051501B2
公开(公告)日：2015-06-09
申请号：US12514417
申请日：2007-11-22
申请人： Katsuyu Wakabayashi , Noriko Matsushita , Katsuya Ouchi , Taisuke Sasaki
发明人： Katsuyu Wakabayashi , Noriko Matsushita , Katsuya Ouchi , Taisuke Sasaki
IPC分类号： C08K3/26 , C09D17/00 , C09K3/10 , C08K3/16 , C08K3/36 , C08K5/16 , C08L83/00 , C08L83/04 , C08G77/08 , C08L21/00 , C08L101/10
CPC分类号： C09K3/10 , C08G77/08 , C08K3/16 , C08K3/26 , C08K3/36 , C08K5/16 , C08L21/00 , C08L101/10 , C08L71/02
摘要： An object of the present invention is to provide a curable composition made mainly of an organic polymer having a reactive silicon group, exhibits a good curability without using any organic tin compound substantially, and gives a cured product having a sufficient strength; and to provide a catalyst composition. The object is solved by a curable composition, comprising a polymer (A) having a silicon-containing group which can be crosslinked by forming a siloxane bond, and a fluoride salt compound (B).
摘要翻译：本发明的目的是提供一种主要由具有反应性硅基团的有机聚合物制成的可固化组合物，其基本上不使用任何有机锡化合物，显示出良好的固化性，并且得到具有足够强度的固化产物; 并提供催化剂组合物。该目的是通过可固化组合物来解决的，该组合物包含具有可通过形成硅氧烷键而交联的含硅基团的聚合物（A）和氟化物盐化合物（B）。

4. 发明授权

US08815985B2 Curable composition 有权
标题翻译：可固化组合物
公开(公告)号：US08815985B2
公开(公告)日：2014-08-26
申请号：US12526751
申请日：2008-02-13
申请人： Katsuyu Wakabayashi , Katsuya Ouchi
发明人： Katsuyu Wakabayashi , Katsuya Ouchi
IPC分类号： C08K5/34 , C08K5/16 , C08K5/00 , C08K5/24
CPC分类号： C08L83/04 , C08G65/2609 , C08G65/2663 , C08G65/336 , C08G65/337 , C08K5/16 , C08K5/31 , C08K5/5419 , C08K5/5425 , C08L101/10 , C08L2312/08 , C09D133/08 , C09J171/02 , C09K3/10 , C09K2200/0239 , C09K2200/0657
摘要： An object of the present invention is to provide a curable composition which is made mainly of a polymer having one or more reactive silicon groups, has good curability even when filler is used while a non-organotin catalyst is used, and is further high in industrial practicability. The object is solved by a curable composition, comprising, as constituents, a polymer (A) having one or more reactive silicon groups on average per molecule thereof, the reactive silicon group(s) being (each) a group which can be crosslinked by forming a siloxane bond, a Lewis acid and/or derivative thereof (B), an amine compound (C), a compound (D) having a reactive silicon group, and filler (E), and obtained by mixing the constituents with each other.
摘要翻译：本发明的目的是提供一种主要由具有一个或多个反应性硅基团的聚合物制成的可固化组合物，即使使用非有机锡催化剂，即使使用填料也具有良好的固化性，并且工业上更高实用性。该目的通过一种可固化组合物来解决，该组合物包含平均每分子具有一个或多个反应性硅基团的聚合物（A），反应性硅基团为（各自）可以被形成硅氧烷键，路易斯酸和/或其衍生物（B），胺化合物（C），具有反应性硅基团的化合物（D）和填料（E），并且通过将组分彼此混合。

5. 发明申请

US20110207886A1 Method for Producing a-hereto-Substituted Alkylhalohydrosilane and Use Thereof 审中-公开
标题翻译：制备α-取代的烷基卤代氢硅烷的方法及其用途
公开(公告)号：US20110207886A1
公开(公告)日：2011-08-25
申请号：US13003300
申请日：2011-01-09
申请人： Katsuyu Wakabayashi , Hidenori Tanaka
发明人： Katsuyu Wakabayashi , Hidenori Tanaka
IPC分类号： C08G65/336 , C08F8/42
CPC分类号： C07F7/126 , C08F8/42 , C08G65/336 , C08L63/00
摘要： Method for efficiently producing α-hetero-substituted alkylhalohydrosilane, and use thereof. A method for producing (A) a halohydrosilane compound represented by the general formula (1): H—SiR2c(CR13-bYb)aX3-a-c (1) (wherein, R1 represents a hydrogen atom or a substituted or unsubstituted hydrocarbon group; R2 represents a substituted or unsubstituted hydrocarbon group; X represents a halogen atom; Y represents a hetero substituent; a is 1 or 2; b is any one of 1, 2 and 3; c is 1 or 0), by allowing (B) a halosilane compound represented by the general formula (2): SiR2c(CR13-bYb)aX4-a-c (2) (wherein, R1, R2, X, Y, a, b and c are as defined above) to react with (C) a hydrosilane compound. A method for producing a reactive silicon group-containing polymer using the halohydrosilane compound (A).
摘要翻译：有效生产α-取代烷基卤代氢硅烷的方法及其应用。（A）由通式（1）表示的卤代氢硅烷化合物的制备方法：H-SiR2c（CR13-bYb）aX3-ac（1）（其中，R1表示氢原子或取代或未取代的烃基; R2 表示取代或未取代的烃基; X表示卤素原子; Y表示杂取代基; a表示1或2; b表示1,2或3中的任一个，c表示1或0）由式（2）表示的卤代硅烷化合物：（C））与SiRcc（CR13-bYb）aX4-ac（2）（其中R1，R2，X，Y，a，b和c如上定义）氢硅烷化合物。使用卤代氢硅烷化合物（A）制造含反应性含硅基团的聚合物的方法。

6. 发明授权

US07973108B2 Curable composition 有权
标题翻译：可固化组合物
公开(公告)号：US07973108B2
公开(公告)日：2011-07-05
申请号：US11579553
申请日：2005-04-25
申请人： Toshihiko Okamoto , Katsuyu Wakabayashi
发明人： Toshihiko Okamoto , Katsuyu Wakabayashi
IPC分类号： C08G77/08 , C08G77/46 , C08G77/48 , C08L83/14 , C08F283/06
CPC分类号： C08G65/336 , C08K3/014 , C08K5/0091 , C08K5/544 , C09D171/02 , C09J171/02 , C09K3/10 , C08L101/10 , C08L71/02
摘要： [Problem] There is provided a curable composition having good curability and adhesion by use of a non-organotin catalyst.[Means to Solve] A curable composition comprising (A) an organic polymer having a silicon-containing group being capable of crosslinking by forming siloxane bonds, (B) one or more kinds selected from a titanium catalyst, an aluminum catalyst and a zirconium catalyst and (C) a low molecular weight compound containing a hydrolyzable silicon group and having a molecular weight of from 100 to 1,000, characterized in that a ratio (a/b) of the total mole (a) of titanium atoms, aluminum atoms and zirconium atoms of the component (B) in the composition to the total mole (b) of silicon atoms of the component (C) in the composition is more than 0.4.
摘要翻译： [问题]提供了通过使用非有机锡催化剂具有良好固化性和粘合性的可固化组合物。 [解决方案]一种可固化组合物，其包含（A）具有能够通过形成硅氧烷键交联的含硅基团的有机聚合物，（B）选自钛催化剂，铝催化剂和锆催化剂中的一种或多种和（C）含有水解性硅基且分子量为100〜1000的低分子量化合物，其特征在于钛原子，铝原子和锆的总摩尔数（a）的比（a / b）组合物中组分（B）的原子与组合物中组分（C）的硅原子的总摩尔数（b）大于0.4。

7. 发明申请

US20090281253A1 CURABLE COMPOSITION IMPROVED IN CURABILITY AND STORAGE STABILITY 审中-公开
标题翻译：改善耐腐蚀性和储存稳定性的可固化组合物
公开(公告)号：US20090281253A1
公开(公告)日：2009-11-12
申请号：US12088814
申请日：2006-09-26
申请人： Toshihiko Okamoto , Katsuyu Wakabayashi
发明人： Toshihiko Okamoto , Katsuyu Wakabayashi
IPC分类号： C08L83/06
CPC分类号： C08K5/42 , C08K5/098 , C08L101/10
摘要： The present invention has its object to provide a curable composition excellent in curability and storage stability.The present invention relates to a curable composition which comprises, for instance,(A) an organic polymer having a silicon-containing group capable of crosslinking under siloxane bond formation, (B) a carboxylic acid metal salt (b1) and/or a carboxylic acid (b2), and (C) an organic sulfonic acid ester represented by the general formula (1): R1SO3R2 (1) (wherein R1 and R2 each independently represents a substituted or unsubstituted hydrocarbon group).
摘要翻译：本发明的目的是提供固化性和保存稳定性优异的固化性组合物。本发明涉及一种可固化组合物，其包含例如（A）具有在硅氧烷键形成下能够交联的含硅基团的有机聚合物，（B）羧酸金属盐（b1）和/或羧酸酸（b2）和（C）由通式（1）表示的有机磺酸酯：R1SO3R2（1）（其中R1和R2各自独立地表示取代或未取代的烃基）。

8. 发明申请

US20090171025A1 CURABLE COMPOSITION 有权
标题翻译：可固化组合物
公开(公告)号：US20090171025A1
公开(公告)日：2009-07-02
申请号：US12088799
申请日：2006-10-02
申请人： Noriko Matsushita , Katsuyu Wakabayashi , Toshihiko Okamoto , Hiroshi Iwakiri
发明人： Noriko Matsushita , Katsuyu Wakabayashi , Toshihiko Okamoto , Hiroshi Iwakiri
IPC分类号： C08F283/12
CPC分类号： C09K3/1018 , C08G65/336 , C08K5/3462 , C08L71/02 , C08L101/10
摘要： The present invention has its object to provide, by using a non-organotin curing catalyst, a curable composition having a practical level of curability. Furthermore, the present invention has its object to provide a curable composition excellent in adhesiveness while it secures a practical level of curability.The present invention relates to a curable composition which comprises:(A) an organic polymer containing a silicon-containing group capable of crosslinking by siloxane bond formation and (B) a silanol condensation catalyst: and that the silanol condensation catalyst is an amine compound and that an aqueous solution prepared by adding 5 millimoles of the amine compound to 100 g of a mixed solvent composed of isopropyl alcohol and water in a weight ratio of 10:3 has a pH value of not lower than 13.4 as measured at 23° C. according to JIS Z 8802.
摘要翻译：本发明的目的是通过使用非有机锡固化催化剂来提供具有实用的固化性水平的可固化组合物。此外，本发明的目的是提供一种固化性优异的固化性组合物，同时确保了固化性的实用性。本发明涉及一种可固化组合物，其包含：（A）含有能够通过硅氧烷键形成交联的含硅基团的有机聚合物和（B）硅烷醇缩合催化剂;所述硅烷醇缩合催化剂是胺化合物，通过向100g由异丙醇和水组成的混合溶剂中加入5毫摩尔胺化合物而制备的水溶液，其重量比为10:3，在23℃下测得的pH值不低于13.4。根据JIS Z 8802。

9. 发明授权

US07550547B2 Curable composition 有权
标题翻译：可固化组合物
公开(公告)号：US07550547B2
公开(公告)日：2009-06-23
申请号：US11091509
申请日：2005-03-29
申请人： Katsuyu Wakabayashi , Toshihiko Okamoto , Hiroshi Ando
发明人： Katsuyu Wakabayashi , Toshihiko Okamoto , Hiroshi Ando
IPC分类号： C08G77/08
CPC分类号： C08L83/04 , C08K5/09 , C09K3/1018
摘要： The present invention provides a curable composition which has a high recovery ratio, a high creep resistance, a practical curability and storage stability. The present invention relates to a curable composition comprising a reactive silicon group containing organic polymer (A) and a carboxylic acid (B), wherein the composition comprises (I), as the carboxylic acid (B), a carboxylic acid (C) in which the carbon adjacent to the carbonyl group is a quaternary carbon atoms and/or the composition comprises (II) a metal carboxylate (D) formed between a carboxylic acid in which the carbon atoms adjacent to the carbonyl group is a quaternary carbon atoms and a metal atom of 208 or less in atomic weight.
摘要翻译：本发明提供了具有高回收率，高抗蠕变性，实用的固化性和储存稳定性的可固化组合物。本发明涉及包含含有有机聚合物（A）和羧酸（B）的反应性硅基团的可固化组合物，其中组合物包含（I）作为羧酸（B）的羧酸（C）其中与羰基相邻的碳是季碳原子和/或组合物包含（II）在其中与羰基相邻的碳原子是季碳原子的羧酸之间形成的金属羧酸盐（D）和原子量为208以下的金属原子。

10. 发明申请

US20080269405A1 Single-Component Curable Composition 审中-公开
标题翻译：单组分可固化组合物
公开(公告)号：US20080269405A1
公开(公告)日：2008-10-30
申请号：US11547030
申请日：2005-03-18
申请人： Toshihiko Okamoto , Katsuyu Wakabayashi , Masato Kusakabe
发明人： Toshihiko Okamoto , Katsuyu Wakabayashi , Masato Kusakabe
IPC分类号： C08L83/04
CPC分类号： C08K5/0025 , C08K5/098 , C08K5/544 , C08L71/02
摘要： The present invention has its object to provide a one package curable composition which has good adhesion while containing an organotin-free catalyst.The present invention provides a one package curable composition which comprises (A) an organic polymer having a silicon-containing group capable of crosslinking by forming a siloxane bond, (B) a carboxylic acid metal salt (b1) and/or a carboxylic acid (b2), (C) a filler, and (D) an amino group-containing silane coupling agent: and has the total amount of carbonyl group composing an acid group in the component (B) per 100 g of the component (A) of 12 mmol or lower; contains substantially no organotin compound; and has the water content of 2,000 ppm or lower.
摘要翻译：本发明的目的是提供一种包含无机锡催化剂的粘合性良好的一包装可固化组合物。本发明提供一种包装可固化组合物，其包含（A）具有能够通过形成硅氧烷键交联的含硅基团的有机聚合物，（B）羧酸金属盐（b1）和/或羧酸（ b2），（C）填料和（D）含氨基的硅烷偶联剂，并且组合物（B）中的每100克组分（A）中构成酸基的羰基的总量为 12 mmol或更低; 基本上不含有机锡化合物; 水含量为2000ppm以下。

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