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    • 1. 发明授权
    • Process for dry dispersal of particles, and a device for carrying out
this process
    • 颗粒的干燥分散方法,以及进行该方法的装置
    • US4868128A
    • 1989-09-19
    • US112507
    • 1987-08-20
    • Karl SommerRolf FathWalter PeschkeUlrich Bohnaus
    • Karl SommerRolf FathWalter PeschkeUlrich Bohnaus
    • G01N1/02G01N1/28G01N15/00G01N33/04
    • G01N1/2813G01N33/04Y10T436/25
    • A process of dry dispersal of fine-grained particles on a specimen slide for the purpose of macroscopic or microscopic analysis, and a corresponding instrument for carrying out this process are described. The process permits random, homogeneous distribution of dry particles on a specimen slide in a unilayered, planar distribution, the particles not touching one another at all or only doing so to a negligible extent, i.e. being positioned on the speciment slide without agglomeration. The process steps are: metered input of the fine-grained substance into a sample container; aspiration of the substance by means of a defined partial vacuum, produced in a turbulence chamber, the substance reaching the turbulence chamber via an accelerator tube and then via a distributor tube, and deposition of the accelerated particles on a transparent speciment slide. The device can, in addition, contain a baffle, against which the powder-like sample substance is projected after rushing through the accelerator tube, in order to then pass through a distributor tube, from which the substance falls in deagglomerated form onto the specimen slide. The process and the device can be used for dry dispersal of a great variety of substances in mixed and pure form, for example foods, luxury foods and medicaments or the precursors thereof, mineral or industrial substances, medical or pharmaceutical preparations or precursors thereof, etc. The main area of application is the preparation of powder-like substances for automatic particle analysis.
    • PCT No.PCT / DE86 / 00118 Sec。 371日期1987年8月20日 102(e)日期1987年8月20日PCT申请日1986年3月20日PCT公布。 公开号WO87 / 03959 日期1987年7月2日。为了宏观或微观分析的目的,将样品载玻片上的细颗粒干燥分散的过程以及用于进行该方法的相应仪器。 该方法允许干燥颗粒在单层,平面分布上随机均匀分布在样品载玻片上,所述颗粒完全不相互接触或者仅仅这样做可忽略的程度,即定位在没有聚集的样品载玻片上。 处理步骤是:将细粒物质计量输入到样品容器中; 通过在湍流室中产生的限定的部分真空吸收物质,该物质通过加速管到达湍流室,然后经由分配器管,并将加速的颗粒沉积在透明的样品载玻片上。 此外,该装置还可以包含挡板,粉碎样品物质在冲入加速器管之后投射到该挡板上,以便然后通过分配器管,物质以分散管的形式从分散管中沉淀到样品载玻片上 。 该方法和装置可用于各种各样的混合和纯净形式的物质的干散,例如食品,奢侈食品和药物或其前体,矿物或工业物质,医药或药物制剂或其前体等 主要应用领域是制备粉状物质进行自动粒子分析。