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1. 发明授权

US5723637A Process for producing propylene oxide 失效
标题翻译：生产环氧丙烷的方法
公开(公告)号：US5723637A
公开(公告)日：1998-03-03
申请号：US754125
申请日：1996-11-22
申请人： Junpei Tsuji , Kenshi Uchida , Noriaki Oku , Mitsuhisa Tamura , Masaru Ishino
发明人： Junpei Tsuji , Kenshi Uchida , Noriaki Oku , Mitsuhisa Tamura , Masaru Ishino
IPC分类号： C07D301/19
CPC分类号： C07D301/19
摘要： A process for producing propylene oxide which comprises reacting a raw material solution which is a solution of ethylbenzene hydroperoxide in ethylbenzene obtained by liquid phase autoxidation of ethylbenzene with propylene in the presence of a Ti-containing solid catalyst to give propylene oxide, said raw material solution being a solution prepared by washing a solution of ethylbenzene hydroperoxide in ethylbenzene obtained by liquid phase autoxidation of ethylbenzene with an aqueous alkali solution to bring a lactic acid concentration to 5 ppm by weight or less.
摘要翻译：一种环氧丙烷的制造方法，其特征在于，在含钛固体催化剂的存在下，使作为乙苯的乙苯溶液在乙苯的液相自动氧化反应得到的原料溶液与丙烯反应，生成环氧丙烷，所述原料溶液是通过用碱水溶液液相自动氧化乙苯获得的乙苯中的乙苯过氧化氢溶液洗涤制备的溶液，使乳酸浓度为5重量ppm以下。

2. 发明申请

US20080035468A1 Method Of Purifying Propylene Oxide 失效
标题翻译：纯化环氧丙烷的方法
公开(公告)号：US20080035468A1
公开(公告)日：2008-02-14
申请号：US11570615
申请日：2005-06-21
申请人： Toshio Nakayama , Junpei Tsuji , Noriaki Oku , Koji Shinohara
发明人： Toshio Nakayama , Junpei Tsuji , Noriaki Oku , Koji Shinohara
IPC分类号： C07D301/32
CPC分类号： C07D303/04 , C07D301/32
摘要： A method of purifying propylene oxide, which comprises subjecting the propylene oxide containing methyl formate as an impurity to extractive distillation using a hydrocarbon of 7 to 10 carbon atoms as an extractant with an extractive distillation column, adding water to the distillate from the overhead of the extractive distillation column to conduct oil-water separation, recycling the oil layer separated to the extractive distillation column, removing the aqueous layer outside the system thereby to obtain propylene oxide in which a methyl formate concentration is reduced as a bottom liquid of the extractive distillation column.
摘要翻译：一种净化环氧丙烷的方法，其包括使用含有7〜10个碳原子的烃作为萃取蒸馏塔的含有甲酸甲酯的环氧丙烷作为杂质进行萃取蒸馏，从馏出物的塔顶馏出物向馏出液中加入水萃取蒸馏塔进行油水分离，将分离的油层再循环到萃取蒸馏塔，除去体系外的水层，得到甲酸甲酯浓度降低的环氧丙烷，作为萃取蒸馏塔的底部液体。

3. 发明授权

US08093412B2 Method of purifying propylene oxide 失效
标题翻译：环氧丙烷的纯化方法
公开(公告)号：US08093412B2
公开(公告)日：2012-01-10
申请号：US11570615
申请日：2005-06-21
申请人： Toshio Nakayama , Junpei Tsuji , Noriaki Oku , Koji Shinohara
发明人： Toshio Nakayama , Junpei Tsuji , Noriaki Oku , Koji Shinohara
IPC分类号： C07D301/32
CPC分类号： C07D303/04 , C07D301/32
摘要： A method of purifying propylene oxide, which comprises subjecting the propylene oxide containing methyl formate as an impurity to extractive distillation using a hydrocarbon of 7 to 10 carbon atoms as an extractant with an extractive distillation column, adding water to the distillate from the overhead of the extractive distillation column to conduct oil-water separation, recycling the oil layer separated to the extractive distillation column, removing the aqueous layer outside the system thereby to obtain propylene oxide in which a methyl formate concentration is reduced as a bottom liquid of the extractive distillation column.
摘要翻译：一种净化环氧丙烷的方法，其包括使用含有7〜10个碳原子的烃作为萃取蒸馏塔的含有甲酸甲酯的环氧丙烷作为杂质进行萃取蒸馏，从馏出物的塔顶馏出物向馏出液中加入水萃取蒸馏塔进行油水分离，将分离的油层再循环到萃取蒸馏塔，除去体系外的水层，得到甲酸甲酯浓度降低的环氧丙烷，作为萃取蒸馏塔的底部液体。

4. 发明授权

US07053226B2 Process for producing cumene 失效
标题翻译：异丙苯生产工艺
公开(公告)号：US07053226B2
公开(公告)日：2006-05-30
申请号：US10489241
申请日：2002-09-10
申请人： Junpei Tsuji , Noriaki Oku
发明人： Junpei Tsuji , Noriaki Oku
IPC分类号： C07D301/19 , C07C1/22 , C07C1/24
CPC分类号： C07D301/19 , C07C1/20 , C07C2523/72 , C07D301/16 , C07D303/04 , Y02P20/52 , C07C15/085
摘要： A process for producing cumene, characterized by preparing a copper-based catalyst by reducing a copper-based catalyst precursor containing copper in an oxidized state with hydrogen in liquid cumene, and subjecting cumyl alcohol to hydrogenolysis in the presence of the copper-based catalyst, and a process for producing propylene oxide which includes that process.
摘要翻译：一种异丙基苯的制造方法，其特征在于，在氢氧化状态下，通过将含有铜的铜系催化剂前体与液态异丙基苯中的氢还原而制备铜系催化剂，在铜系催化剂的存在下，使枯烯醇进行氢解，以及包括该方法的环氧丙烷的制造方法。

5. 发明授权

US06736941B2 Process for purifying propylene oxide 失效
标题翻译：环氧丙烷的纯化方法
公开(公告)号：US06736941B2
公开(公告)日：2004-05-18
申请号：US10258411
申请日：2002-10-24
申请人： Noriaki Oku , Masaru Ishino
发明人： Noriaki Oku , Masaru Ishino
IPC分类号： B01D334
CPC分类号： C07D301/32
摘要： A process is described for purifying propylene oxide, which includes the step of distilling propylene oxide containing impurities in the presence of a hydrocarbon having 5 carbon atoms or less. According to the present invention, a process is provided for purifying propylene oxide which has a feature that impurities contained in a solution containing propylene oxide to be purified can be efficiently removed. Oxygen-containing impurities, in particular, can be very efficiently removed.
摘要翻译：描述了用于纯化环氧丙烷的方法，其包括在具有5个或更少碳原子的烃存在下蒸馏含有杂质的环氧丙烷的步骤。根据本发明，提供了一种净化环氧丙烷的方法，其特征在于可以有效地除去含有待纯化的环氧丙烷的溶液中所含的杂质。特别是含氧杂质可以非常有效地去除。

6. 发明授权

US06410806B1 Reduction-treated copper-based catalyst and process for producing &agr;-phenylethyl alcohol using the same 有权
公开(公告)号：US06410806B1
公开(公告)日：2002-06-25
申请号：US09761830
申请日：2001-01-18
申请人： Noriaki Oku , Masaru Ishino
发明人： Noriaki Oku , Masaru Ishino
IPC分类号： C07C2700
摘要： A reduction-treated copper-based catalyst obtained by reducing a copper-based catalyst with hydrogen in the presence of a liquid phase and a process for producing &agr;-phenylethyl alcohol, which comprises hydrogenating acetophenone in the presence of the same.

7. 发明授权

US6046369A Process for producing .alpha.-phenylethyl alcohol 失效
标题翻译：生产α-苯乙醇的方法
公开(公告)号：US6046369A
公开(公告)日：2000-04-04
申请号：US113294
申请日：1998-07-10
申请人： Noriaki Oku , Masaru Ishino
发明人： Noriaki Oku , Masaru Ishino
IPC分类号： C07C29/145
CPC分类号： C07C29/145
摘要： A process for producing .alpha.-phenylethyl alcohol, which comprises hydrogenating acetophenone by a fixed bed flow reaction in the presence of a catalyst, wherein the reaction is conducted in the state where the liquid hold up ratio in a reactor is in the range of from 30% to 90%.
摘要翻译：一种生产α-苯乙醇的方法，其包括在催化剂存在下通过固定床流动反应使苯乙酮氢化，其中反应在反应器中的液体保持率为30的范围内进行％〜90％。

8. 发明申请

US20050092593A1 Method of purifying propylene oxide 有权
标题翻译：环氧丙烷的纯化方法
公开(公告)号：US20050092593A1
公开(公告)日：2005-05-05
申请号：US10504548
申请日：2003-02-07
申请人： Noriaki Oku , Toshio Nakayama , Koji Shinohara
发明人： Noriaki Oku , Toshio Nakayama , Koji Shinohara
IPC分类号： C07D301/32 , C07D303/04 , B01D3/42 , B01D3/34
CPC分类号： C07D301/32
摘要： A process for purifying propylene oxide characterized by Subjecting a liquid reaction mixture containing propylene oxide, and water, hydrocarbons and oxygen-containing organic compounds as impurities obtained by reacting cumene hydroperoxide with propylene to extractive distillation using an extractant of a hydrocarbon having 7 to 20 carbon atoms with an extractive distillation column, and controlling a concentration of propylene glycol in the extractant supplied to the extractive distillation column to 20% by weight or less.
摘要翻译：一种净化环氧丙烷的方法，其特征在于，使用含有环氧丙烷的液体反应混合物和水，烃和含氧有机化合物作为通过使用氢过氧化枯烯和丙烯反应获得的杂质，使用具有7至20个碳的烃的萃取剂进行萃取蒸馏将萃取蒸馏塔的萃取剂中丙二醇的浓度控制在20重量％以下。

9. 发明授权

US07285187B2 Method of purifying propylene oxide 有权
标题翻译：环氧丙烷的纯化方法
公开(公告)号：US07285187B2
公开(公告)日：2007-10-23
申请号：US10504548
申请日：2003-02-07
申请人： Noriaki Oku , Toshio Nakayama , Koji Shinohara
发明人： Noriaki Oku , Toshio Nakayama , Koji Shinohara
IPC分类号： B01D3/40 , B01D3/42 , C07D301/32 , C07D303/04
CPC分类号： C07D301/32
摘要： A process for purifying propylene oxide characterized by subjecting a liquid reaction mixture containing propylene oxide, and water, hydrocarbons and oxygen-containing organic compounds as impurities obtained by reacting cumene hydroperoxide with propylene to extractive distillation using an extractant of a hydrocarbon having 7 to 20 carbon atoms with an extractive distillation column, and controlling a concentration of propylene glycol in the extractant supplied to the extractive distillation column to 20% by weight or less.
摘要翻译：一种净化环氧丙烷的方法，其特征在于，使用含有环氧丙烷的液体反应混合物和水，烃和含氧有机化合物作为通过使异丙基氢过氧化氢与丙烯反应获得的杂质，使用具有7至20碳的烃的萃取剂进行萃取蒸馏将萃取蒸馏塔的萃取剂中丙二醇的浓度控制在20重量％以下。

10. 发明授权

US06600054B2 Process for producing propylene oxide 失效
标题翻译：生产环氧丙烷的方法
公开(公告)号：US06600054B2
公开(公告)日：2003-07-29
申请号：US10221366
申请日：2002-09-12
申请人： Noriaki Oku , Toshikazu Omae
发明人： Noriaki Oku , Toshikazu Omae
IPC分类号： C07D30119
CPC分类号： C07D301/19
摘要： A process for producing propylene oxide, which comprises steps described below, wherein isopropylbenzene hydroperoxide supplied to an epoxidation step has not undergone a heat history including heating at a temperature not lower than the temperature (t° C.) represented by the following equation (1), t(° C.)=150−0.8×W (1) W: content (% by weight) of isopropylbenzene hydroperoxide in a solution containing isopropylbenzene hydroperoxide: oxidation step; a step in which isopropylbenzene is oxidized to obtain isopropylbenzene hydroperoxide, epoxidation step; a step in which isopropylbenzene hydroperoxide obtained in the oxidation step is reacted with propylene to obtain propylene oxide and cumyl alcohol, and hydrogenolysis step; a step in which cumyl alcohol obtained in the epoxidation step is subjected to hydrogenolysis to obtain isopropylbenzene, and said isopropylbenzene is recycled to the oxidation step as a raw material for the oxidation step.
摘要翻译：一种生产环氧丙烷的方法，其包括以下步骤，其中提供给环氧化步骤的异丙基苯氢过氧化物没有经历热历程，包括在不低于由下式（1）表示的温度（t℃）的温度下加热），W：含异丙基苯氢过氧化物的溶液中异丙苯氢过氧化物的含量（重量％）：氧化步骤; 异丙苯氧化得到异丙基苯氢过氧化物的步骤，环氧化步骤; 在氧化步骤中得到的异丙基苯氢过氧化物与丙烯反应得到环氧丙烷和枯
醇，并进行氢解步骤; 将在环氧化步骤中得到的异丙醇进行氢解以获得异丙基苯的步骤，并将所述异丙基苯循环到氧化步骤作为氧化步骤的原料。

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