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1. 发明授权

US4330481A Process for preparing polycarbonates 失效
标题翻译：聚碳酸酯的制备方法
公开(公告)号：US4330481A
公开(公告)日：1982-05-18
申请号：US177030
申请日：1980-08-11
申请人： John F. Timberlake , Daniel W. Baugh, Jr. , Bobby Burkes
发明人： John F. Timberlake , Daniel W. Baugh, Jr. , Bobby Burkes
IPC分类号： C08G64/02 , C08G64/18 , C08G64/30 , C07C69/96
CPC分类号： C08G64/305 , C08G64/0208 , C08G64/18
摘要： Polycarbonate type nonionic surfactant compositions comprising monohydroxy alcohols capped with polycarbonate groups. More specifically, the surfactant compositions comprise aliphatic, nonaromatic cycloaliphatic or aromatic alcohols which have been capped with block polycarbonate groups formed by the reaction of the alcohols with ethylene carbonate in the presence of an alkali metal salt catalyst. The surfactant properties of the compositions may be varied by first reacting the alcohols with ethylene oxide to form a block polyether group cap on the alcohols before the reaction with ethylene carbonate or by further reacting the polycarbonate capped alcohols with ethylene oxide to form a terminal polyether block group. The surfactants formed are a random distribution mixture of compositions wherein 2 to 20 moles of ethylene carbonate and 3 to 50 moles of ethylene oxide per mole of the alcohols are reacted together.
摘要翻译：包含用聚碳酸酯基封端的一羟基醇的聚碳酸酯型非离子表面活性剂组合物。更具体地说，表面活性剂组合物包括脂肪族，非芳族的脂环族或芳族醇，其已经用碱金属盐催化剂存在下通过醇与碳酸亚乙酯的反应形成的嵌段聚碳酸酯基封端。组合物的表面活性剂性质可以通过首先使醇与环氧乙烷反应来改变，以在与碳酸亚乙酯反应之前在醇上形成嵌段聚醚基帽，或通过使聚碳酸酯封端的醇与环氧乙烷进一步反应形成末端聚醚嵌段组。所形成的表面活性剂是一种组合物的随机分布混合物，其中每摩尔醇将2至20摩尔碳酸亚乙酯和3至50摩尔环氧乙烷反应。

2. 发明授权

US4415502A Polycarbonate type nonionic surfactants 失效
标题翻译：聚碳酸酯型非离子表面活性剂
公开(公告)号：US4415502A
公开(公告)日：1983-11-15
申请号：US327375
申请日：1981-12-04
申请人： John F. Timberlake , Daniel W. Baugh, Jr. , Bobby Burkes
发明人： John F. Timberlake , Daniel W. Baugh, Jr. , Bobby Burkes
IPC分类号： C08G64/02 , C08G64/18 , C08G64/30 , C07C69/96
CPC分类号： C08G64/0208 , C08G64/18 , C08G64/305 , Y10S516/01
摘要： Polycarbonate type nonionic surfactant compositions comprising monohydroxy alcohols capped with polycarbonate groups. More specifically, the surfactant compositions comprise aliphatic, nonaromatic cycloaliphatic or aromatic alcohols which have been capped with block polycarbonate groups formed by the reaction of the alcohols with ethylene carbonate in the presence of an alkali metal salt catalyst. The surfactant properties of the compositions may be varied by first reacting the alcohols with ethylene oxide to form a block polyether group cap on the alcohols before the reaction with ethylene carbonate or by further reacting the polycarbonate capped alcohols with ethylene oxide to form a terminal polyether block group. The surfactants formed are a random distribution mixture of compositions wherein 2 to 20 moles of ethylene carbonate and 3 to 50 moles of ethylene oxide per mole of the alcohols are reacted together.
摘要翻译：包含用聚碳酸酯基封端的一羟基醇的聚碳酸酯型非离子表面活性剂组合物。更具体地说，表面活性剂组合物包括脂肪族，非芳族的脂环族或芳族醇，其已经用碱金属盐催化剂存在下通过醇与碳酸亚乙酯的反应形成的嵌段聚碳酸酯基封端。组合物的表面活性剂性质可以通过首先使醇与环氧乙烷反应来改变，以在与碳酸亚乙酯反应之前在醇上形成嵌段聚醚基帽，或通过使聚碳酸酯封端的醇与环氧乙烷进一步反应形成末端聚醚嵌段组。所形成的表面活性剂是一种组合物的随机分布混合物，其中每摩尔醇将2至20摩尔碳酸亚乙酯和3至50摩尔环氧乙烷反应。

3. 发明授权

US4147733A Fluorination of chlorinated hydrocarbons 失效
标题翻译：氯化烃的氟化
公开(公告)号：US4147733A
公开(公告)日：1979-04-03
申请号：US908310
申请日：1978-05-22
申请人： Tom R. Fiske , Daniel W. Baugh, Jr.
发明人： Tom R. Fiske , Daniel W. Baugh, Jr.
IPC分类号： C07C17/20 , C07C17/08 , C07C17/15
CPC分类号： C07C17/206
摘要： Chlorine atoms in chlorinated lower aliphatic hydrocarbons are replaced by fluorine in the vapor phase reaction of the chlorinated hydrocarbons with aqueous HF at 275.degree. C.- 425.degree. C. in the presence of a metal fluoride catalyst, particularly where the metal is one or more of aluminum, nickel, or chromium. The fluorinated products are blowing agents, refrigerants, monomers, or intermediates for making them.
摘要翻译：在金属氟化物催化剂存在下，氯化烃与HF水溶液在275°C-425℃的气相反应中氯代低级脂族烃中的氯原子被氟代替，特别是在金属为一种或多种的情况下的铝，镍或铬。氟化产物是用于制造它们的发泡剂，制冷剂，单体或中间体。

4. 发明授权

US4272455A Production of monoalkyleneglycols, monoalkanolamines and alkylenediamine 失效
标题翻译：单亚烷基二醇，单链烷醇胺和亚烷基二胺的生产
公开(公告)号：US4272455A
公开(公告)日：1981-06-09
申请号：US107287
申请日：1979-12-26
申请人： Frank T. Cook , Daniel W. Baugh, Jr. , Robert V. Chambers, Jr.
发明人： Frank T. Cook , Daniel W. Baugh, Jr. , Robert V. Chambers, Jr.
IPC分类号： C07C29/00 , C07C29/09 , C07C85/145 , C07C85/20 , C07C89/00
CPC分类号： C07C29/00 , C07C29/095
摘要： A method for the formation of monoalkyleneglycols, monoalkanolamines and alkylenediamines, comprising the steps of: (a) reacting ammonia or ammonium carbonate with an alkylenecarbonate to form a carbamate, (b) heating the carbamate to form a monoalkyleneglycol, an alkyleneurea and a 2-oxazolidinone, (c) further reacting the alkyleneurea and the 2-oxazolidinone with ammonium hydroxide to form ammonia or ammonium carbonate, a monoalkanolamine, and an alkylenediamine, (d) separating the ammonia or ammonium carbonate, the monoalkyleneglycol, the alkylenediamine, and the monoalkanolamine, and (e) recycling the ammonia or ammonium carbonate to reaction step (a).
摘要翻译：一种形成单亚烷基二醇，单烷醇胺和亚烷基二胺的方法，包括以下步骤：（a）使氨或碳酸铵与亚烷基碳酸酯反应以形成氨基甲酸酯，（b）加热氨基甲酸酯以形成单亚烷基二醇，亚烷基脲和2- 恶唑烷酮，（c）使亚烷基脲和2-恶唑烷酮与氢氧化铵进一步反应以形成氨或碳酸铵，单烷醇胺和亚烷基二胺，（d）分离氨或碳酸铵，单亚烷基二醇，亚烷基二胺和单链烷醇胺，和（e）将氨或碳酸铵再循环到反应步骤（a）中。

5. 发明授权

US4405794A Preparation of 2-oxazolidinone and ethyleneurea 失效
标题翻译： 2-恶唑烷酮和亚乙基脲的制备
公开(公告)号：US4405794A
公开(公告)日：1983-09-20
申请号：US332290
申请日：1981-12-18
申请人： Robert M. Harnden , Daniel W. Baugh, Jr.
发明人： Robert M. Harnden , Daniel W. Baugh, Jr.
IPC分类号： C07D233/34 , C07D263/22 , C07D233/30
CPC分类号： C07D263/22 , C07D233/34
摘要： The present invention provides a method for reacting urea and beta-hydroxyethylcarbamate to make 2-oxazolidinone and ethyleneurea in a good yield and high selectivity, whereby the reaction method can be controlled to provide either the 2-oxazolidinone or the ethyleneurea as the major reaction product.
摘要翻译：本发明提供了一种使脲和β-羟乙基氨基甲酸酯以良好的产率和高选择性使2-恶唑烷酮和亚乙基脲反应的方法，由此可以控制反应方法以提供2-恶唑烷酮或亚乙基脲作为主要的反应产物。

6. 发明授权

US4122095A Actinide nitrate ditetrahydrofuranate and method of production 失效
标题翻译：锕系硝酸二氢四氢呋喃及其生产方法
公开(公告)号：US4122095A
公开(公告)日：1978-10-24
申请号：US733875
申请日：1976-10-19
申请人： George W. Watt , Daniel W. Baugh, Jr.
发明人： George W. Watt , Daniel W. Baugh, Jr.
IPC分类号： C01G43/025 , C01G99/00 , C07D307/08
CPC分类号： C01G99/006 , C01G43/025 , C01P2006/60 , C01P2006/80
摘要： An actinide dioxide, e.g. uranium dioxide, is prepared by reacting an actinide nitrate or hydrate or tetrahydrofuranate thereof, e.g. uranyl nitrate, a hydrate of uranyl nitrate or a tetrahydrofuranate of uranyl nitrate with an alkali or alkaline earth metal adduct of a monocyclic or polycyclic hydrocarbon in the presence of an inert organic solvent. Typically, the starting material may be uranyl nitrate dihydrate or uranyl nitrate ditetrahydrofuranate (the latter material is a novel composition of matter) with a reactant such as the sodium adduct of naphthalene in the presence of a solvent such as tetrahydrofuran. The resultant uranium dioxide may be further purified by heating it in the presence of hydrogen.
摘要翻译：二氧化，二氧化铀是通过使硝酸锕系元素或其水合物或四氢呋喃，例如，硝酸铀酰，硝酸铀酰的水合物或硝酸铀酰的四氢化物与单环或多环烃的碱金属或碱土金属加成物在惰性有机溶剂的存在下进行。通常，起始原料可以是硝酸铀酰二水合物或硝酸铀酰二硝酸二铀酸盐（后者是物质的新型组合物）与反应物如萘的加合物在溶剂如四氢呋喃的存在下反应。所得的二氧化铀可以通过在氢存在下加热来进一步纯化。

7. 发明授权

US4211757A Actinide sulfite tetrahydrate and actinide oxysulfite tetrahydrate 失效
标题翻译：锕系亚硫酸四水合物和锕系氧化亚硫酸氢盐四水合物
公开(公告)号：US4211757A
公开(公告)日：1980-07-08
申请号：US830751
申请日：1977-09-06
申请人： George W. Watt , Daniel W. Baugh, Jr.
发明人： George W. Watt , Daniel W. Baugh, Jr.
IPC分类号： C01G43/00 , C01G56/00
CPC分类号： C01G56/008 , C01G43/00 , C01G56/004 , C01G56/005 , C01P2006/80 , C01P2006/82
摘要： An actinide dioxide, e.g. uranium dioxide, plutonium dioxide, neptunium dioxide, etc., is prepared by reacting the actinide nitrate hexahydrate with sodium dithionite as a first step; the reaction product from this first step is a novel composition of matter comprising the actinide sulfite tetrahydrate. The reaction product resulting from this first step is then converted to the actinide dioxide by heating it in the absence of an oxygen-containing atmosphere (e.g. nitrogen) to a temperature of about 500.degree. to about 950.degree. C. for about 15 to about 135 minutes. If the reaction product resulting from the first step is, prior to carrying out the second heating step, exposed to an oxygen-containing atmosphere such as air, the resultant product is a novel composition of matter comprising the actinide oxysulfite tetrahydrate which can also be readily converted to the actinide dioxide by heating it in the absence of an oxygen-containing atmosphere (e.g. nitrogen) at a temperature of about 400.degree. to about 900.degree. C. for about 30 to about 150 minutes. Further, the actinide oxysulfite tetrahydrate can be partially dehydrated at reduced pressures (and in the presence of a suitable dehyrating agent such as phosphorus pentoxide). The partially dehydrated product may be readily converted to the dioxide form by heating it in the absence of an oxygen-containing atmosphere (e.g. nitrogen) at a temperature of about 500.degree. to about 900.degree. C. for about 30 to about 150 minutes.
摘要翻译：二氧化，作为第一步，通过使硝酸锕系六水合物与连二亚硫酸钠反应来制备二氧化铀，二氧化钚，二氧化，等。来自该第一步骤的反应产物是包含锕系亚硫酸盐四水合物的新物质组合物。然后将由该第一步产生的反应产物在不含氧气氛（例如氮气）的条件下加热至约500℃至约950℃的温度加热至约135℃至约135℃ 分钟。如果由第一步产生的反应产物在进行第二加热步骤之前暴露于含氧气氛如空气中，则所得产物是包含锕系亚硫酸亚铁盐四水合物的新型组合物，其也可容易地通过在约400℃至约900℃的温度下在不存在含氧气氛（例如氮气）的条件下将其加热至约30至约150分钟而转化为二氧化锕。此外，锕系亚硫酸氢四水合物可以在减压下（和在合适的脱氢剂如五氧化二磷存在下）部分脱水。通过在约500℃至约900℃的温度下在不存在含氧气氛（例如氮气）的条件下加热部分脱水产物可容易地转化为二氧化物形式约30至约150分钟。

8. 发明授权

US4139568A Process for making methyl fluoride 失效
标题翻译：制造氟化氟的方法
公开(公告)号：US4139568A
公开(公告)日：1979-02-13
申请号：US908308
申请日：1978-05-22
申请人： Daniel W. Baugh, Jr. , Marylu B. Gibbs
发明人： Daniel W. Baugh, Jr. , Marylu B. Gibbs
IPC分类号： C07C17/16 , C07C17/00
CPC分类号： C07C17/16
摘要： Methanol and aqueous HF react in the vapor phase at 250.degree. C.-400.degree. C. in the presence of activated carbon, nickel fluoride, chromium fluoride, aluminum fluoride, or a mixture thereof to produce methyl fluoride plus dimethyl ether as the principal by-product.
摘要翻译：在活性炭，氟化镍，氟化铬，氟化铝或其混合物的存在下，甲醇和HF水溶液在250℃-400℃下在气相中反应，以产生甲基氟加二甲醚为主要 -产品。

9. 发明授权

US4012489A Process for the preparation of uranium dioxide 失效
标题翻译：二氧化铀的制备方法
公开(公告)号：US4012489A
公开(公告)日：1977-03-15
申请号：US579494
申请日：1975-05-21
申请人： George W. Watt , Daniel W. Baugh, Jr.
发明人： George W. Watt , Daniel W. Baugh, Jr.
IPC分类号： C01G43/00 , C01G43/025 , C01G56/00 , C01G43/02
CPC分类号： C01G43/025 , C01G43/00 , C01G56/004 , C01G56/008 , C01P2006/80
摘要： An actinide dioxide, e.g., uranium dioxide, plutonium dioxide, neptunium dioxide, etc., is prepared by reacting the actinide nitrate hexahydrate with sodium dithionite as a first step; the reaction product from this first step is a novel composition of matter comprising the actinide sulfite tetrahydrate. The reaction product resulting from this first step is then converted to the actinide dioxide by heating it in the absence of an oxygen-containing atmosphere (e.g., nitrogen) to a temperature of about 500.degree. to about 950.degree. C. for about 15 to about 135 minutes. If the reaction product resulting from the first step is, prior to carrying out the second heating step, exposed to an oxygen-containing atmosphere such as air, the resultant product is a novel composition of matter comprising the actinide oxysulfite tetrahydrate which can also be readily converted to the actinide dioxide by heating it in the absence of an oxygen-containing atmosphere (e.g., nitrogen) at a temperature of about 400.degree. to about 900.degree. C. for about 30 to about 150 minutes. Further, the actinide oxysulfite tetrahydrate can be partially dehydrated at reduced pressures (and in the presence of a suitable dehydrating agent such as phosphorus pentoxide). The partially dehydrated product may be readily converted to the dioxide form by heating it in the absence of an oxygen-containing atmosphere (e.g., nitrogen) at a temperature of about 500.degree. to about 900.degree. C. for about 30 to about 150 minutes.
摘要翻译：作为第一步，通过使硝酸锕系六水合物与连二亚硫酸钠反应来制备二氧化act二氧化物，二氧化dioxide二氧化物，二氧化，等。来自该第一步骤的反应产物是包含锕系亚硫酸盐四水合物的新物质组合物。然后将由该第一步产生的反应产物在不存在含氧气氛（例如氮气）的条件下加热至约500℃至约950℃的温度约15至约 135分钟。如果由第一步产生的反应产物在进行第二加热步骤之前暴露于含氧气氛如空气中，则所得产物是包含锕系亚硫酸亚铁盐四水合物的新型组合物，其也可容易地通过在约400℃至约900℃的温度下在不存在含氧气氛（例如氮气）的条件下将其加热至约30至约150分钟而转化为二氧化锕。此外，锕系氧化亚硫酸氢盐四水合物可以在减压下（和在合适的脱水剂如五氧化二磷的存在下）部分脱水。通过在约500℃至约900℃的温度下在不存在含氧气氛（例如氮气）的条件下加热部分脱水产物可容易地转化为二氧化物形式约30至约150分钟。

10. 发明授权

US4003980A Uranium dioxide preparation 失效
标题翻译：二氧化铀制备
公开(公告)号：US4003980A
公开(公告)日：1977-01-18
申请号：US579495
申请日：1975-05-21
申请人： George W. Watt , Daniel W. Baugh, Jr.
发明人： George W. Watt , Daniel W. Baugh, Jr.
IPC分类号： C01G43/025 , C01G99/00 , C01G43/02
CPC分类号： C01G99/006 , C01G43/025 , C01P2006/60 , C01P2006/80
摘要： An actinide dioxide, e.g. uranium dioxide, is prepared by reacting an actinide nitrate or hydrate or tetrahydrofuranate thereof, e.g. uranyl nitrate, a hydrate of uranyl nitrate or a tetrahydrofuranate of uranyl nitrate with an alkali or alkaline earth metal adduct of a monocyclic or polycyclic hydrocarbon in the presence of an inert organic solvent. Typically, the starting material may be uranyl nitrate dihydrate or uranyl nitrate ditetrahydrofuranate (the latter material is a novel composition of matter) with a reactant such as the sodium adduct of naphthalene in the presence of a solvent such as tetrahydrofuran. The resultant uranium dioxide may be further purified by heating it in the presence of hydrogen.
摘要翻译：二氧化，二氧化铀是通过使硝酸锕系元素或其水合物或四氢呋喃，例如，硝酸铀酰，硝酸铀酰的水合物或硝酸铀酰的四氢化物与单环或多环烃的碱金属或碱土金属加成物在惰性有机溶剂的存在下进行。通常，起始原料可以是硝酸铀酰二水合物或硝酸铀酰二硝酸二铀酸盐（后者是物质的新型组合物）与反应物如萘的加合物在溶剂如四氢呋喃的存在下反应。所得的二氧化铀可以通过在氢存在下加热来进一步纯化。

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