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1. 发明授权

US5457243A Neutralization of crude MTBE effluent streams using solid bases 失效
标题翻译：使用固体碱中和粗制MTBE流出物流
公开(公告)号：US5457243A
公开(公告)日：1995-10-10
申请号：US172345
申请日：1993-12-23
申请人： John F. Knifton , Mark A. Mueller , Michael W. Peters
发明人： John F. Knifton , Mark A. Mueller , Michael W. Peters
IPC分类号： C07C41/36 , C07C29/88 , C07C31/12 , C07C41/44 , C07C43/04 , C07C41/00
CPC分类号： C07C41/44 , C07C29/88 , C07C31/12
摘要： Disclosed is a method for removing organic acids and derivatives thereof from a crude methyl tertiary butyl ether (MTBE) stream of the type found in the feed to, or effluent from, a reactor for a one-step process for producing MTBE which comprises:contacting said crude MTBE stream in a treating zone over one or more beds of a solid base for a period of time sufficient to neutralize said organic acids and derivatives thereof; andwithdrawing a substantially organic acid-free crude MTBE product from said treating zone.
摘要翻译：公开了一种从用于生产MTBE的一步方法的反应器的反应器或从流出物中的流出物类型的粗甲基叔丁基醚（MTBE）流中除去有机酸及其衍生物的方法，其包括：接触所述粗制MTBE流在处理区中超过一个或多个固体碱床，时间足以中和所述有机酸及其衍生物; 以及从所述处理区取出基本上无机酸的粗MTBE产物。

2. 发明授权

US4912266A Catalytic decomposition of tertiary butyl hydroperoxide 失效
标题翻译：叔丁基过氧化氢的催化分解
公开(公告)号：US4912266A
公开(公告)日：1990-03-27
申请号：US94174
申请日：1987-09-08
申请人： John R. Sanderson , John F. Knifton , Edward T. Marquis , Mark A. Mueller
发明人： John R. Sanderson , John F. Knifton , Edward T. Marquis , Mark A. Mueller
IPC分类号： C07C29/132
CPC分类号： C07C29/132
摘要： In order to prepare a feedstock, isobutane is reacted with oxygen in an oxidation zone to provide an oxidation product comprising a solution of tertiary butyl hydroperoxide in unreacted isobutane. A catalyst may be present to catalyze the reaction of the oxygen with the isobutane if desired.The feedstock is charged to a catalytic decomposition zone wherein the tertiary butyl hydroperoxide is decomposed in the presence of an imidazole-promoted metal phthalocyanine catalyst to provide a decomposition reaction product characterized by a compartively high conversion rate and a compartively high selectively of tertiary butyl hydroperoxide to tertiary butyl alcohol.
摘要翻译：为了制备原料，异丁烷在氧化区与氧反应以提供包含叔丁基过氧化氢在未反应的异丁烷中的溶液的氧化产物。如果需要，可以存在催化剂来催化氧与异丁烷的反应。将原料装入催化分解区，其中叔丁基过氧化氢在咪唑促进金属酞菁催化剂存在下分解，得到特征在于高转化率和高选择性的叔丁基过氧化氢的分解反应产物，叔丁醇。

3. 发明授权

US5464505A Use of propylene oxide adducts in the purification of propylene oxide by extractive distillation 失效
标题翻译：通过萃取蒸馏在环氧丙烷的纯化中使用环氧丙烷加合物
公开(公告)号：US5464505A
公开(公告)日：1995-11-07
申请号：US251158
申请日：1994-05-31
申请人： Michael W. Peters , William A. Smith , Mark A. Mueller , William K. Culbreth, III
发明人： Michael W. Peters , William A. Smith , Mark A. Mueller , William K. Culbreth, III
IPC分类号： B01D3/40 , C07D301/32 , C07D303/04
CPC分类号： C07D301/32 , B01D3/40
摘要： Propylene oxide adducts of oxyethylene glycols are used as extractive distillation agents in an extractive distillation column in the distillation of propylene oxide contaminated with water, acetone and methanol to obtain an overhead propylene oxide distillate fraction contaminated with reduced quantities of water, acetone and methanol, and a heavier bottoms distillation fraction containing substantially all of the extractive distillation agent, and acetone and some of the methanol and water introduced into the distillation column.
摘要翻译：氧化乙烯二醇的环氧丙烷加成物在萃取蒸馏塔中用于在被水，丙酮和甲醇污染的环氧丙烷的蒸馏中用作萃取蒸馏剂，以获得被减少量的水，丙酮和甲醇污染的顶部环氧丙烷馏分，以及含有基本上所有萃取蒸馏剂的较重的塔底蒸馏馏分，以及引入蒸馏塔中的丙酮和一些甲醇和水。

4. 发明授权

US5453160A Use of mixed polyoxypropylene glycols in the extractive distillation of propylene oxide 失效
标题翻译：在环氧丙烷的萃取蒸馏中使用混合的聚氧丙烯二醇
公开(公告)号：US5453160A
公开(公告)日：1995-09-26
申请号：US251151
申请日：1994-05-31
申请人： Michael W. Peters , William K. Culbreth, III , Mark A. Mueller
发明人： Michael W. Peters , William K. Culbreth, III , Mark A. Mueller
IPC分类号： B01D3/40 , C07D301/32 , C07D303/04
CPC分类号： C07D301/32 , B01D3/40 , Y10S203/09
摘要： An extractive distillation agent comprising a mixture of polyoxypropylene glycols is fed to an extractive distillation column used for the distillation of propylene oxide contaminated with water, acetone and methanol to obtain an overhead distillate anhydrous propylene oxide fraction contaminated with reduced quantities of methanol and a heavier bottoms distillation fraction containing the polyoxypropylene glycols, water and acetone and some of the methanol introduced into the distillation column.
摘要翻译：将包含聚氧丙烯二醇的混合物的萃取蒸馏剂进料到用于蒸馏被水，丙酮和甲醇污染的环氧丙烷的萃取蒸馏塔中，以获得被甲醇降低和较重底物污染的塔顶馏出物无水环氧丙烷馏分含有聚氧丙烯二醇的蒸馏馏分，水和丙酮以及一些引入蒸馏塔的甲醇。

5. 发明授权

US06518474B1 Process for producing isobutylene from tertiary butyl alcohol 有权
标题翻译：从叔丁醇生产异丁烯的方法
公开(公告)号：US06518474B1
公开(公告)日：2003-02-11
申请号：US09692021
申请日：2000-10-19
申请人： John R. Sanderson , Mark A. Mueller
发明人： John R. Sanderson , Mark A. Mueller
IPC分类号： C07C120
CPC分类号： C07C1/20 , C07C2529/08 , C07C11/09
摘要： A process for producing substantially pure isobutylene containing relatively small amounts of higher oligomer byproducts. The process may employ a Y-zeolite catalyst having a silica to alumina ratio of less than or equal to about ten.
摘要翻译：一种制备基本上纯的含有较少量低级副产物的异丁烯的方法。该方法可以使用二氧化硅与氧化铝之比小于或等于约十的Y-沸石催化剂。

6. 发明授权

US5620568A Extractive distillation of propylene oxide using propanol 失效
标题翻译：用丙醇萃取环氧丙烷
公开(公告)号：US5620568A
公开(公告)日：1997-04-15
申请号：US659975
申请日：1996-06-03
申请人： William A. Smith , Mark A. Mueller
发明人： William A. Smith , Mark A. Mueller
IPC分类号： B01D3/40 , C07B63/00 , C07D301/32 , C07D303/04
CPC分类号： B01D3/40 , C07D301/32
摘要： An extractive distillation agent of 1-propanol is fed to an extractive distillation column used for the distillation of propylene oxide contaminated with water, acetone and methanol to obtain an overhead distillate fraction of essentially anhydrous propylene oxide contaminated with reduced quantities of acetone and methanol, and a heavier bottoms distillation fraction containing substantially all of the 1-propanol, water and acetone, some of the methanol and heavier by-products of propylene oxide formed in the distillation column.
摘要翻译：将1-丙醇的萃取蒸馏装置进料到用于蒸馏被水，丙酮和甲醇污染的环氧丙烷的萃取蒸馏塔中，得到被丙酮和甲醇减少的基本上无水的环氧丙烷的塔顶蒸馏馏分，以及含有基本上所有1-丙醇，水和丙酮的较重的塔底蒸馏馏分，在蒸馏塔中形成的环氧丙烷的一些甲醇和较重的副产物。

7. 发明授权

US5607776A Article formed by in-situ cleaning a Ti target in a Ti+TiN coating process 失效
标题翻译：通过在Ti + TiN涂层工艺中原位清洗Ti靶而形成的制品
公开(公告)号：US5607776A
公开(公告)日：1997-03-04
申请号：US403169
申请日：1995-03-13
申请人： Mark A. Mueller , Xin Guo , John C. Egermeier
发明人： Mark A. Mueller , Xin Guo , John C. Egermeier
IPC分类号： C23C14/00 , C23C14/06 , C23C14/18 , C23C14/56 , B32B15/04
CPC分类号： C23C14/0036 , C23C14/0641 , C23C14/185 , C23C14/564 , Y10T428/24975 , Y10T428/265
摘要： A novel method of in-situ cleaning a Ti target in a Ti+TiN anti-reflective coating process when such Ti and TiN deposition process are conducted in the same process chamber by the addition of a simple process step and without the use of a shutter.
摘要翻译：当在相同的处理室中进行这种Ti和TiN沉积工艺时，通过添加简单的工艺步骤并且不使用快门，在Ti + TiN抗反射涂覆工艺中原位清洁Ti靶的新方法。

8. 发明授权

US5401889A Preparation of tertiary butyl alcohol by catalytic decomposition of tertiary butyl hydroperoxide 失效
标题翻译：通过叔丁基过氧化氢的催化分解制备叔丁醇
公开(公告)号：US5401889A
公开(公告)日：1995-03-28
申请号：US150916
申请日：1993-11-12
申请人： John R. Sanderson , Mark A. Mueller , Yu-Hwa E. Sheu
发明人： John R. Sanderson , Mark A. Mueller , Yu-Hwa E. Sheu
IPC分类号： B01J23/52 , C07B61/00 , C07C27/00 , C07C29/132 , C07C31/12 , C07C29/00 , C07C29/88
CPC分类号： C07C29/132
摘要： A method for preparing tertiary butyl alcohol wherein a feedstock comprising a solution of tertiary butyl hydroperoxide in a cosolvent mixture of tertiary butyl alcohol with isobutane is charged to a hydroperoxide decomposition reaction zone containing a catalytically effective amount of a hydroperoxide decomposition catalyst and is brought into contact with the catalyst in liquid phase with agitation under hydroperoxide decomposition reaction conditions to convert the tertiary butyl hydroperoxide to decomposition products, principally tertiary butyl alcohol.
摘要翻译：制备叔丁醇的方法，其中在叔丁醇与异丁烷的共溶剂混合物中包含叔丁基过氧化氢溶液的原料加入含有催化有效量的氢过氧化物分解催化剂的氢过氧化物分解反应区，并与之接触催化剂在液相中在氢过氧化物分解反应条件下搅拌，将叔丁基氢过氧化物转化成分解产物，主要是叔丁醇。

9. 发明授权

US08381717B2 System for solar heating water using a glass absorber 失效
标题翻译：使用玻璃吸收器的太阳能加热水系统
公开(公告)号：US08381717B2
公开(公告)日：2013-02-26
申请号：US12326995
申请日：2008-12-03
申请人： Mark A. Mueller
发明人： Mark A. Mueller
IPC分类号： F24J2/00
CPC分类号： F24S70/16 , F24S10/502 , F24S70/10 , F24S70/60 , F24S80/30 , F24S2080/05 , F24S2080/502 , Y02B10/20 , Y02E10/44 , Y10T29/49355
摘要： A system of passively heating water using solar energy and an absorber formed from two identical halves of molded darkened glass that are fused together. The absorber is essentially a plurality of black glass struts that are sandwiched between two black glass surfaces. The struts act as baffle plates and define cells. Water is carried through the system via the thermosiphoning effect.
摘要翻译：使用太阳能被动加热水的系统和由熔融在一起的两个相同的模制变黑玻璃的两半形成的吸收体。吸收器基本上是夹在两个黑色玻璃表面之间的多个黑色玻璃支柱。支柱作为挡板并定义细胞。水通过热虹吸效应进入系统。

10. 发明授权

US5436376A Production of tertiary butyl alcohol 失效
标题翻译：生产叔丁醇
公开(公告)号：US5436376A
公开(公告)日：1995-07-25
申请号：US288841
申请日：1994-08-11
申请人： Yu-Hwa E. Sheu , John R. Sanderson , Mark A. Mueller , William A. Smith
发明人： Yu-Hwa E. Sheu , John R. Sanderson , Mark A. Mueller , William A. Smith
IPC分类号： C07C27/12 , C07C29/132 , C07C29/50 , C07C29/88 , C07C31/12 , C07C41/09 , C07C29/48 , C07C29/80
CPC分类号： C07C29/50 , C07C29/132 , C07C29/88 , C07C31/12 , C07C41/09
摘要： A plural stage process for the production of tertiary butyl alcohol from isobutane wherein isobutane is reacted with oxygen in a first reactor to prepare a primary liquid reaction mixture comprising unreacted isobutane, tertiary butyl alcohol, tertiary butyl hydroperoxide and small amounts of oxygen-containing by-products, distilling the primary reaction product to provide a first lighter isobutane recycle distillation fraction and a first heavier liquid distillation fraction comprising the debutanized mixture of tertiary butyl hydroperoxide with tertiary butyl alcohol, diluting the first heavier liquid distillation fraction with an amount of tertiary butyl alcohol sufficient to provide a feed mixture comprising about 15 to 25 wt. % of tertiary butyl hydroperoxide, about 75 to 85 wt. % of tertiary butyl alcohol and minor amounts of oxygen-containing impurities, wherein the feed mixture is charged to a hydroperoxide decomposition reactor and contacted therein with a solid heterogeneous hydroperoxide decomposition catalyst to convert substantially all of the tertiary butyl hydroperoxide to tertiary butyl alcohol and a minor amount of oxygen-containing by-products to provide a final reaction mixture and wherein tertiary butyl alcohol is recovered from the final reaction mixture.
摘要翻译：用于从异丁烷生产叔丁醇的多级方法，其中异丁烷在第一反应器中与氧反应以制备包含未反应的异丁烷，叔丁醇，叔丁基过氧化氢和少量含氧副产物的初级液体反应混合物，产物，蒸馏初级反应产物以提供第一轻质异丁烷循环蒸馏馏分和第一较重液体蒸馏馏分，其包含叔丁基氢过氧化物与叔丁醇的经纯化的混合物，将第一较重液体蒸馏馏分用一定量的叔丁醇足以提供包含约15至25wt。叔丁基过氧化氢的百分比，约75至85wt。叔丁醇％和少量含氧杂质，其中将进料混合物加入到氢过氧化物分解反应器中，并与固体异相氢过氧化物分解催化剂接触，将基本上所有的叔丁基氢过氧化物转化成叔丁醇，少量的含氧副产物以提供最终的反应混合物，并且从最终反应混合物中回收叔丁醇。

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