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1. 发明授权

US5523484A Bis and tris N-(carbonyl, carbonimidoyl, carbonothioyl) sulfonamide charge control agents, toners and developers 失效
标题翻译：双和三-N-（羰基，亚氨基，碳酰硫基）磺酰胺电荷控制剂，调色剂和显影剂
公开(公告)号：US5523484A
公开(公告)日：1996-06-04
申请号：US316006
申请日：1994-09-30
申请人： John C. Wilson , Peter S. Alexandrovich
发明人： John C. Wilson , Peter S. Alexandrovich
IPC分类号： G03G9/097 , C07C311/51
CPC分类号： G03G9/09775 , G03G9/09783
摘要： An electrophotographic toner having polymeric binder and a charge control agent selected from the group consisting of sulfonamides having the general structure: ##STR1## Each R.sup.1 is independently O, S, N-H, N-R.sup.z, or N-L-R.sup.z ; where L is a linking group selected from: ##STR2## and R.sup.z is independently selected from the group consisting of alkyl having from 1 to 20 carbons, cycloalkyl having from 3 to 18 carbons, and aromatic and heteroaromatic ring systems having a solitary ring or 2 to 3 linked or fused rings. R.sup.a, R.sup.b, and R.sup.c are each independently a ring system of a single ring or 2 or 3 fused or linked rings, said ring system having from 3 to 34 carbons, including substituent carbons. d is an integer from 0 to 3. e is an integer from 0 to 3. The sum of d+e is 2 or 3.
摘要翻译：具有聚合物粘合剂和电荷控制剂的电子照相调色剂，其选自具有以下通式结构的磺酰胺：每个R 1独立地为O，S，N-H，N-Rz或N-L-Rz; 其中L是选自以下的连接基团：R IMA独立地选自具有1至20个碳的烷基，具有3至18个碳的环烷基，以及具有孤立环或2个碳原子的芳族和杂芳族环系统到3个连接或稠环。 R a，R b和R c各自独立地是单环或2或3个稠合或连接的环的环系，所述环系具有3至34个碳，包括取代基的碳。 d为0〜3的整数。e为0〜3的整数.d + e的和为2或3。

2. 发明授权

US5147749A Toners and developers containing n-substituted quinolinium salts as charge control agents 失效
标题翻译：含有取代的喹啉盐作为电荷控制剂的调色剂和显影剂
公开(公告)号：US5147749A
公开(公告)日：1992-09-15
申请号：US560695
申请日：1990-07-31
申请人： Peter S. Alexandrovich , John C. Wilson
发明人： Peter S. Alexandrovich , John C. Wilson
IPC分类号： G03G9/097
CPC分类号： G03G9/09758 , G03G9/0975
摘要： New electrostatographic toners and developers are provided containing new charge-control agents comprising N-substituted quinolinium salts having the structure: ##STR1## wherein R is a straight or branched chain alkyl group having from 1 to 5 carbon atoms, aralkyl in which the alkyl group has 1 to 20 carbon atoms and the aryl group has from 6 to 14 carbon atoms, R' and R", which are the same or different, represent hdyrogen or a straight or branched chain alkyl or alkoxy group having from 1 to 24 carbon atoms, aralkyl or alkaryl in which the alkyl group has 1 to 20 carbon atoms and the aryl group has from 6 to 14 carbon atoms, unsubstituted aryl having from 6 to 14 carbon atoms or aryl having from 6 to 14 carbon atoms substituted with one or more nitro, alkoxy or halo groups and X is hydrogen, chlorine, bromine, fluorine or iodine.
摘要翻译：提供了新的静电调色剂和显影剂，其含有新的电荷控制剂，其包含具有以下结构的N-取代的喹啉盐：其中R是具有1至5个碳原子的直链或支链烷基，其中烷基具有1至20个碳原子并且芳基具有6至14个碳原子，R'和R“相同或不同，表示氢原子或具有1至24个碳原子的直链或支链烷基或烷氧基原子，芳烷基或烷芳基，其中烷基具有1至20个碳原子，芳基具有6至14个碳原子，未取代的具有6至14个碳原子的芳基或具有6至14个碳原子的芳基被一个或多个更多的硝基，烷氧基或卤素基团，X是氢，氯，溴，氟或碘。

3. 发明授权

US5082883A Reduced viscosity polyblends of polyester and epoxy resins 失效
标题翻译：聚酯和环氧树脂的降粘粘度聚合物
公开(公告)号：US5082883A
公开(公告)日：1992-01-21
申请号：US491759
申请日：1990-03-12
申请人： Peter S. Alexandrovich , John E. Derimiggio , John C. Wilson
发明人： Peter S. Alexandrovich , John E. Derimiggio , John C. Wilson
IPC分类号： C08G59/16 , C08L63/00 , C08L67/00
CPC分类号： C08L63/00 , C08G59/1455 , C08L67/00
摘要： Polyblends are provided which display low melt viscosities. The polyblends comprise a polyester having a T.sub.g in the range of about 50.degree. to about 100.degree. C. and an epoxy polymer which is either an epoxy resin or an esterified epoxy resin.
摘要翻译：提供了显示低熔体粘度的聚合物。聚合物共混物包括Tg在约50℃至约100℃范围内的聚酯和环氧树脂或环氧树脂或酯化环氧树脂的环氧聚合物。

4. 发明授权

US5075190A Toners and developers containing N-substituted pyridinium salts as charge control agents 失效
标题翻译：含有N-取代吡啶鎓盐作为电荷控制剂的调色剂和显影剂
公开(公告)号：US5075190A
公开(公告)日：1991-12-24
申请号：US560644
申请日：1990-07-31
申请人： Peter S. Alexandrovich , Alexandra D. Bermel , Zona R. Pierce , John C. Wilson
发明人： Peter S. Alexandrovich , Alexandra D. Bermel , Zona R. Pierce , John C. Wilson
IPC分类号： C07D213/06 , C07D213/20 , C07F5/02 , G03G9/097
CPC分类号： C07D213/20 , C07F5/027 , G03G9/0975 , G03G9/09758
摘要： New electrostatographic toners and developers are provided containing new charge-control agents comprising N-substituted pyridinium salts having the ##STR1## wherein R is a straight or branched chain alkyl group having from 1 to 24 carbon atoms, aralkyl in which the alkyl group has 1 to 20 carbon atoms and the aryl group has from 6 to 14 carbon atoms, R.sup.1 is hydrogen or a straight or branched chain alkyl or alkoxy group having from 1 to 24 carbon atoms, aralkyl or alkaryl in which the alkyl group has 1 to 20 carbon atoms and the aryl group has from 6 to 14 carbon atoms, unsubstituted aryl having from 6 to 14 carbon atoms or aryl having from 6 to 14 carbon atoms substituted with one or more nitro, alkoxy or halo groups and X is hydrogen, chlorine, bromine, fluorine or iodine.
摘要翻译：提供了新的静电彩色调色剂和显影剂，其中含有新的电荷控制剂，其包含具有“IMAGE”的N-取代的吡啶鎓盐，其中R是具有1至24个碳原子的直链或支链烷基，其中烷基具有1 至20个碳原子，并且芳基具有6至14个碳原子，R 1是氢或具有1至24个碳原子的直链或支链烷基或烷氧基，其中烷基具有1至20个碳的芳烷基或烷芳基原子和芳基具有6至14个碳原子，未取代的具有6至14个碳原子的芳基或具有6至14个碳原子的芳基被一个或多个硝基，烷氧基或卤素基团取代，X是氢，氯，溴，氟或碘。

5. 发明授权

US5681680A Difunctional N-(2-cyanoethenyl) sulfonamides and toner compositions containing them 失效
标题翻译：二官能的N-（2-氰基乙烯基）磺酰胺和含有它们的调色剂组合物
公开(公告)号：US5681680A
公开(公告)日：1997-10-28
申请号：US644801
申请日：1996-05-10
申请人： John C. Wilson , Peter S. Alexandrovich
发明人： John C. Wilson , Peter S. Alexandrovich
IPC分类号： C07C311/19 , G03G9/097 , G03G9/087
CPC分类号： G03G9/09775 , C07C311/19 , C07C2102/08
摘要： There is provided a compound, useful in electrostatographic processes in the toner composition along with a polymeric binder, having the general structure: ##STR1## wherein R.sup.1 is selected from the group consisting of alkylene; arylene; arylenedialkylene; alkylenediarylene; oxydialkylene; and substituted or unsubstituted oxydiarylene; and R.sup.2 and R.sup.3, which can be the same or different, are independently selected from the group consisting of alkyl containing from 1 to 20 carbons; cycloalkyl containing from 3 to 18 carbons; unsubstituted aromatic ring systems; or aromatic ring systems substituted with one or more alkyl, hydroxy, alkoxy, carboxy, carboalkoxy, nitro, halo, cyano, amino, dialkylamino, acyl, trihalomethyl or alkylsulfonyl; heteroaromatic ring systems; said ring systems having a solitary ring or 2 to 3 linked or fused rings, and containing from 3 to 34 carbons; and R.sup.3 may also be ethenyl, unsubstituted or substituted with alkyl containing from 1 to 20 carbons or aryl containing from 5 to 10 carbons or aryl substituted with alkyl, hydroxy, carboxy, carboalkoxy, nitro, halo, cyano, amino, dialkylamino, acyl, trihalomethyl, or alkylsulfonyl. The described charge control agents are negative charge control agents and are essentially colorless making them particularly useful in toner compositions for color electrophotography. Thus, in another aspect of the invention, there is provided a toner composition including the charge control agent and a polymeric binder.
摘要翻译：提供了一种化合物，其可用于调色剂组合物中的静电印刷方法以及聚合物粘合剂，其具有以下一般结构：其中R 1选自亚烷基; 亚芳基亚芳基亚乙基; 亚烷基亚芳基; 氧化二烯和取代或未取代的氧代二亚芳基; 和可以相同或不同的R 2和R 3独立地选自含有1至20个碳的烷基; 含有3至18个碳原子的环烷基; 未取代的芳环体系; 被一个或多个烷基，羟基，烷氧基，羧基，烷氧羰基，硝基，卤素，氰基，氨基，二烷基氨基，酰基，三卤代甲基或烷基磺酰基取代的芳香环体系。杂芳环系统; 所述环体系具有单环或2至3个连接或稠环，并含有3至34个碳; 羟基，羧基，烷氧羰基，硝基，卤素，氰基，氨基，二烷基氨基，酰基，芳基，芳基，芳基，三卤代甲基或烷基磺酰基。所述的电荷控制剂是负电荷控制剂，并且基本上是无色的，使得它们在用于彩色电子照相术的调色剂组合物中特别有用。因此，在本发明的另一方面，提供了包含电荷控制剂和聚合物粘合剂的调色剂组合物。

6. 发明授权

US5385800A Bis and tris N-(carbonyl, carbonimidoyl, carbonothioyl)sulfonamide charge control agents, toners and developers 失效
标题翻译：双和三-N-（羰基，亚氨基，碳酰硫基）磺酰胺电荷控制剂，调色剂和显影剂
公开(公告)号：US5385800A
公开(公告)日：1995-01-31
申请号：US171784
申请日：1993-12-22
申请人： John C. Wilson , Peter S. Alexandrovich
发明人： John C. Wilson , Peter S. Alexandrovich
IPC分类号： G03G9/097 , G03G13/22
CPC分类号： G03G9/09775 , G03G9/09783
摘要： An electrophotographic toner having polymeric binder and a charge control agent selected from the group consisting of sulfonamides having the general structure: ##STR1## Each R.sup.1 is independently O, S, N--H, N--R.sup.z, or N--L--R.sup.z ; where L is a linking group selected from: ##STR2## and R.sup.z is independently selected from the group consisting of alkyl having from 1 to 20 carbons, cycloalkyl having from 3 to 18 carbons, and aromatic and heteroaromatic ring systems having a solitary ring or 2 to 3 linked or fused rings. R.sup.a, R.sup.b, and R.sup.c are each independently a ring system of a single ring or 2 or 3 fused or linked rings, said ring system having from 3 to 34 carbons, including substituent carbons. d is an integer from 0 to 3. e is an integer from 0 to 3. The sum of d+e is 2 or 3.
摘要翻译：具有聚合物粘合剂和电荷控制剂的电子照相调色剂，其选自具有以下通式结构的磺酰胺：每个R 1独立地为O，S，N-H，N-Rz或N-L-Rz; 其中L是选自以下的连接基团：R IMA独立地选自具有1至20个碳的烷基，具有3至18个碳的环烷基，以及具有孤立环或2个碳原子的芳族和杂芳族环系统到3个连接或稠环。 R a，R b和R c各自独立地是单环或2或3个稠合或连接的环的环系，所述环系具有3至34个碳，包括取代基的碳。 d为0〜3的整数。e为0〜3的整数.d + e的和为2或3。

7. 发明授权

US4837393A Electrostatographic toner particle comprising a polyester containing a covalently bound quaternary phosphonium salt 失效
标题翻译：包含含有共价结合的季鏻盐的聚酯的静电色调调色剂颗粒
公开(公告)号：US4837393A
公开(公告)日：1989-06-06
申请号：US229045
申请日：1988-08-05
申请人： Peter S. Alexandrovich , Lawrence P. DeMejo , John C. Wilson
发明人： Peter S. Alexandrovich , Lawrence P. DeMejo , John C. Wilson
IPC分类号： C08K5/50 , G03G9/087 , G03G9/097
CPC分类号： G03G9/09741 , C08K5/50 , G03G9/08755 , G03G9/08791 , Y10S430/104 , Y10S430/105
摘要： New electrostatographic toners and developers are provided, containing dual function polyester binder/charge agents. The new toner particle has an average diameter in the range of 0.01 to 100 micrometers and comprises a binder polyester and a charge-control agent comprising a quaternary phosphonium salt, wherein the phosphonium salt has an anionic portion comprising a sulfonate group covalently bonded to a moiety containing at least one ester linkage to the binder polyester.
摘要翻译：提供新的静电调色剂和显影剂，包含双功能聚酯粘合剂/充电剂。新的调色剂颗粒的平均直径在0.01至100微米的范围内，并且包含粘合剂聚酯和包含季鏻盐的电荷控制剂，其中鏻盐具有阴离子部分，其包含共价键合到部分上的磺酸基含有至少一个与粘结剂聚酯的酯键。

8. 发明授权

US5714293A Toner compositions containing N-(2-cyanoethenyl)sulfonamides 失效
公开(公告)号：US5714293A
公开(公告)日：1998-02-03
申请号：US644805
申请日：1996-05-10
申请人： John C. Wilson , Peter S. Alexandrovich
发明人： John C. Wilson , Peter S. Alexandrovich
IPC分类号： G03G9/097
CPC分类号： G03G9/09775
摘要： There is provided a toner composition, useful in electrostatographic processes, comprising a polymeric binder and a charge-control agent having the general structure: ##STR1## wherein R.sup.1 is selected from the group consisting of hydrogen; alkyl containing from 1 to 20 carbons; cyano; cycloalkyl containing from 3 to 18 carbons; unsubstituted aromatic ring systems; aromatic ring systems substituted with one or more alkyl, halo, nitro, cyano, hydroxy, alkoxy, carboxy, carboalkoxy, amino, dialkylamino, acyl, trihalomethyl or alkysulfonyl; and heteroaromatic ring systems; said ring systems having a solitary ring or 2 to 3 linked or fused rings, and containing from 3 to 34 carbons; alkanoyl; alkoxycarbonyl; aminocarbonyl; alkylaminocarbonyl; aralkylaminocarbonyl; alkylsulfonyl; aroyl; aryloxycarbonyl; arylaminocarbonyl; arylsulfonyl; or aroyl, aryloxycarbonyl, arylaminocarbonyl, aralkylaminocarbonyl or arylsulfonyl substituted with one or more alkyl, hydroxy, alkoxy, carboxy, carboalkoxy, nitro, halo, cyano, amino, dialkylamino, acyl, trihalomethyl or alkylsulfonyl; and R.sup.2 and R.sup.3, which can be the same or different, are independently selected from the group consisting of alkyl containing from 1 to 20 carbons; cycloalkyl containing from 3 to 18 carbons; unsubstituted aromatic ring systems; or aromatic ring systems substituted with one or more alkyl, hydroxy, alkoxy, carboxy, carboalkoxy, nitro, halo, cyano, amino, dialkylamino, acyl, trihalomethyl or alkylsulfonyl; heteroaromatic ring systems; said ring systems having a solitary ring or 2 to 3 linked or fused rings, and containing from 3 to 34 carbons; and R.sup.3 may also be ethenyl, unsubstituted or substituted with alkyl containing from 1 to 20 carbons or aryl containing from 5 to 10 carbons or aryl substituted with alkyl, hydroxy, carboxy, carboalkoxy, nitro, halo, cyano, amino, dialkylamino, acyl, trihalomethyl, or alkylsulfonyl. The described charge control agents are negative charge control agents and are essentially colorless making them particularly useful in toner compositions for color electrophotography.

9. 发明授权

US5405727A N-(carbonyl, carbonimidoyl, carbonothioyl) sulfonamide charge control agents and toners and developers 失效
标题翻译： N-（羰基，亚氨基，碳酰硫基）磺酰胺电荷控制剂和调色剂和显影剂
公开(公告)号：US5405727A
公开(公告)日：1995-04-11
申请号：US171783
申请日：1993-12-22
申请人： John C. Wilson , Peter S. Alexandrovich , Steven M. Bonser
发明人： John C. Wilson , Peter S. Alexandrovich , Steven M. Bonser
IPC分类号： C07C303/36 , C07C311/50 , G03G9/097
CPC分类号： G03G9/09766 , G03G9/09733 , G03G9/09775 , G03G9/09783
摘要： An electrophotographic toner having polymeric binder and a charge control agent selected from the group consisting of sulfonamides having the general structure: ##STR1## and metal salts thereof. T.sup.1 is independently selected from H, alkyl having from 1 to 20 carbons, cycloalkyl having from 3 to 18 carbons, and aromatic and heteroaromatic ring systems having a solitary ring or 2 to 3 linked or fused rings. R.sup.1 is O, S, N--H, N--R.sup.5, or N--L--R.sup.5 ; where L is a linking group selected from: ##STR2## and R.sup.5 is independently selected from alkyl having from 1 to 20 carbons, cycloalkyl having from 3 to 18 carbons, and aromatic and heteroaromatic ring systems having a solitary ring or 2 to 3 linked or fused rings. L.sup.1 and L.sup.2 are each independently a direct link or divalent alkyl or fluoroalkyl having from 1 to 20 carbons. R.sup.a and R.sup.b are each independently selected from the group consisting of H, F and ring systems having a solitary ring or from 2 to 3 fused or linked rings, said ring system having from 3 to 34 carbons, including carbons of substituent groups. If L.sup.1 is a direct link, R.sup.a is a ring system and if L.sup.2 is a direct link, R.sup.b is a ring system.
摘要翻译：具有聚合物粘合剂和电荷控制剂的电子照相调色剂，其选自具有以下通式结构的磺酰胺及其金属盐。 T 1独立地选自H，具有1至20个碳的烷基，具有3至18个碳的环烷基，以及具有孤立环或2至3个连接或稠环的芳族和杂芳族环系。 R1是O，S，N-H，N-R5或N-L-R5; 其中L是选自以下的连接基团：R 1和R 2独立地选自具有1至20个碳的烷基，具有3至18个碳原子的环烷基，以及具有单环或2至3个连接的或稠环。 L1和L2各自独立地为直接键或具有1至20个碳的二价烷基或氟代烷基。 R a和R b各自独立地选自H，F和具有孤立环的环系统或2至3个稠合或连接的环，所述环系具有3至34个碳，包括取代基的碳。如果L1是直接链路，则Ra是环系统，如果L2是直接链路，则Rb是环系统。

10. 发明授权

US5041625A Toners and developers containing N,N'-substituted-bis(pyridinium) salts as charge control agents 失效
标题翻译：含有N，N'-取代 - 双（吡啶鎓）盐作为电荷控制剂的调色剂和显影剂
公开(公告)号：US5041625A
公开(公告)日：1991-08-20
申请号：US560642
申请日：1990-07-31
申请人： John C. Wilson , Peter S. Alexandrovich
发明人： John C. Wilson , Peter S. Alexandrovich
IPC分类号： G03G9/097
CPC分类号： G03G9/0975 , G03G9/09758
摘要： New electrostatographic toners and developers are provided containing new charge-control agents comprising N,N'-substitutedbis(pyridinium) salts having the structure: ##STR1## wherein R is alkylene having from 1 to 20 carbon atoms or arylenedialkylene wherein each alkylene moiety has 1 to 6 carbon atoms and the arylene moiety has from 6 to 14 carbon atoms, R' and R", which are the same or different, represent hydrogen, a straight or branched chain alkyl or alkoxy group having from 1 to 24 carbon atoms, aralkyl or alkaryl in which the alkyl group has 1 to 20 carbon atoms and the aryl group has from 6 to 14 carbon atoms, aryl having 6 to 14 carbon atoms which is unsubstituted or aryl having 6 to 14 carbon atoms which is substituted with one or more nitro, alkoxy or halo groups and X and X', which are the same or different, are chlorine, bromine, fluorine or iodine.
摘要翻译：提供了新的静电色调调色剂和显影剂，其包含新的电荷控制剂，其包含具有以下结构的N，N'-取代双（吡啶鎓）盐：其中R是具有1至20个碳原子的亚烷基或芳基亚乙烯基，其中每个亚烷基部分具有1至6个碳原子，亚芳基部分具有6至14个碳原子，R'和R“可相同或不同，表示氢，具有1至24个碳原子的直链或支链烷基或烷氧基碳原子，芳烷基或烷芳基，其中烷基具有1至20个碳原子，芳基具有6至14个碳原子，具有6-14个碳原子的未被取代的芳基或具有6至14个碳原子的芳基被取代与一个或多个硝基，烷氧基或卤基，X和X'相同或不同，是氯，溴，氟或碘。

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