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1. 发明授权

US5304424A High thermal conductivity diamond/non-diamond composite materials 失效
标题翻译：高导热性金刚石/非金刚石复合材料
公开(公告)号：US5304424A
公开(公告)日：1994-04-19
申请号：US954354
申请日：1992-09-30
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , B32B9/00
CPC分类号： C23C16/274 , C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C04B2235/427 , C04B2235/667 , Y10T428/249955 , Y10T428/249956 , Y10T428/249957 , Y10T428/249967 , Y10T428/24997 , Y10T428/24999 , Y10T428/2938 , Y10T428/2991 , Y10T428/30
摘要： A CVD diamond material, substantially free of voids, has an average crystallite size greater than about 15 microns, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm.sup.-1 greater than about 3, a Raman sp.sup.3 full width half maximum less than about 6 cm.sup.-1 and a diamond-to-graphite Raman ratio greater than about 25. The diamond material may also comprise carbon atoms with a C.sup.13 content less than 0.05 atomic %.
摘要翻译：基本上没有空隙的CVD金刚石材料具有大于约15微米的平均微晶尺寸，金刚石拉曼峰的最大强度（以/秒计）除以1270cm -1以上的光致发光强度大于约3，a 拉曼sp3全宽半最小小于约6cm -1，金刚石至石墨拉曼比大于约25.金刚石材料还可包含C13含量小于0.05原子％的碳原子。

2. 发明授权

US5270114A High thermal conductivity diamond/non-diamond composite materials 失效
标题翻译：高导热性金刚石/非金刚石复合材料
公开(公告)号：US5270114A
公开(公告)日：1993-12-14
申请号：US954671
申请日：1992-09-30
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/27 , B32B9/00
CPC分类号： C23C16/274 , C01B31/065 , C23C16/27 , Y10T428/249955 , Y10T428/249956 , Y10T428/249967 , Y10T428/2991 , Y10T428/30
摘要： The present invention comprises an article formed from a plurality of diamond particles and non-diamond particles compatible with diamond deposition preformed into a desired shape. Each of the particles has first surface regions in contact with immediately adjacent other ones of the particles, and second surface regions spaced apart from the immediately adjacent other ones of said particles to define boundaries of inter-particle voids between the immediately adjacent ones of the particles. The voids are infiltrated with high thermal conductivity CVD diamond material continuously coating the second surface regions of the particles and comprising merged growth fronts from the second surface regions of individual immediately adjacent ones of the particles into the inter-particle voids. The high thermal conductivity CVD diamond material has an average crystallite size greater than about 15 microns, an intensity ratio of diamond- Raman-peak-to-photoluminescence background intensity greater than about 20, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm.sup.-1 greater than about 3, a Raman sp.sup.3 full width half maximum less than about 6 cm.sup.-1 and a diamond-to-graphite Raman ratio greater than about 25. The thermal conductivity of the CVD diamond materials is in excess of 17 Wcm.sup.-1 K.sup.-1.
摘要翻译：本发明包括由多个金刚石颗粒和与金刚石沉积相容的非金刚石颗粒形成的制品，其预成形为所需形状。每个颗粒具有与直接相邻的其它颗粒接触的第一表面区域，以及与紧邻的另一个颗粒间隔开的第二表面区域，以限定紧邻的颗粒之间的颗粒间空隙的边界。空隙被高导热性CVD金刚石材料渗透，连续地涂覆颗粒的第二表面区域并且包括从单个紧邻的颗粒的第二表面区域到颗粒间空隙中的合并生长前沿。高导热性CVD金刚石材料具有大于约15微米的平均微晶尺寸，金刚石 - 拉曼峰 - 光致发光背景强度的强度比大于约20，金刚石拉曼峰的最大强度以计数/秒计除以大于约3的1270cm-1处的光致发光强度，小于约6cm -1的拉曼sp3全宽半最大值和大于约25的金刚石 - 石墨拉曼比。CVD的热导率金刚石材料超过17 Wcm-1K-1。

3. 发明授权

US5284709A Diamond materials with enhanced heat conductivity 失效
标题翻译：具有增强导热性的金刚石材料
公开(公告)号：US5284709A
公开(公告)日：1994-02-08
申请号：US789732
申请日：1991-11-08
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , C30B29/04
CPC分类号： C23C16/274 , C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C04B2235/427 , C04B2235/667 , Y10T428/249955 , Y10T428/249956 , Y10T428/249957 , Y10T428/249967 , Y10T428/24997 , Y10T428/24999 , Y10T428/2938 , Y10T428/2991 , Y10T428/30
摘要： A diamond film having an intensity ratio of diamond-Raman-peak-to-photoluminescence background intensity greater than about 20, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm greater than about 3, a Raman sp full width half maximum less than about 6 cm and a diamond-to-graphite Raman ratio greater than about 25. The diamond film has a thermal conductivity of at least 17 Wcm K.
摘要翻译：具有大于约20的金刚石 - 拉曼峰 - 光致发光背景强度的强度比的金刚石膜，以秒/秒除以金刚石拉曼峰的最大强度除以1270厘米以上的光致发光强度大于约3，拉曼sp全宽半最小值小于约6厘米，金刚石至石墨拉曼比大于约25.金刚石膜的热导率至少为17 Wcm。

4. 发明授权

US5271971A Microwave plasma CVD method for coating a substrate with high thermal-conductivity diamond material 失效
标题翻译：用高导热性金刚石材料涂覆基材的微波等离子体CVD方法
公开(公告)号：US5271971A
公开(公告)日：1993-12-21
申请号：US954356
申请日：1992-09-30
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/27 , B05D3/06 , C23C16/26
CPC分类号： C23C16/274 , C01B31/065 , C23C16/27 , Y10T428/30
摘要： A two-stage microwave plasma CVD process is disclosed for making a CVD diamond material, substantially free of voids, which has an average crystallite size greater than about 15 microns, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm.sup.-1 greater than about 3, a Raman sp.sup.3 full width half maximum less than about 6 cm.sup.-1 and a diamond-to-graphite Raman ratio greater than about 25.
摘要翻译：公开了两级微波等离子体CVD方法，用于制造基本上没有空隙的CVD金刚石材料，其平均微晶尺寸大于约15微米，金刚石拉曼峰的最大强度（以计数/秒除以强度）在大于约3的1270cm -1处的光致发光，小于约6cm -1的拉曼sp3全宽半最大值和大于约25的金刚石 - 石墨拉曼比。

5. 发明授权

US5277975A High thermal-conductivity diamond-coated fiber articles 失效
标题翻译：高导热性金刚石涂层纤维制品
公开(公告)号：US5277975A
公开(公告)日：1994-01-11
申请号：US954358
申请日：1992-09-30
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , B32B9/00
CPC分类号： C23C16/274 , C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C04B2235/427 , C04B2235/667 , Y10T428/249955 , Y10T428/249956 , Y10T428/249957 , Y10T428/249967 , Y10T428/24997 , Y10T428/24999 , Y10T428/2938 , Y10T428/2991 , Y10T428/30
摘要： The present invention comprises an article formed for a plurality of diamond-coated fibers preformed into a desired shape. Each of the fibers has first surface regions in contact with immediately adjacent other ones of the fibers, and second surface regions spaced apart from the immediately adjacent other ones of said fibers to define boundaries of inter-fiber voids between the immediately adjacent ones of the fibers. The voids are infiltrated with high thermal conductivity CVD diamond material continuously coating the second surface regions of the fibers and comprising merged growth fronts from the second surface regions of individual immediately adjacent ones of the fibers into the inter-particle voids. The high thermal conductivity CVD diamond material has an average crystallite size greater than about 15 microns, an intensity ratio of diamond-Raman-peak-to-photoluminescence background intensity greater than about 20, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm.sup.-1 greater than about 3, a Raman sp.sup.3 full width half maximum less than about 6 cm.sup.-1 and a diamond-to-graphite Raman ratio greater than about 25. The thermal conductivity of the CVD diamond material is in excess of 17 Wcm.sup.-1 K.sup.-1.
摘要翻译：本发明包括形成用于预成形为所需形状的多个金刚石涂层纤维的制品。每个纤维具有与直接相邻的另一个纤维接触的第一表面区域和与紧邻的另一个纤维间隔开的第二表面区域，以限定紧邻的纤维之间的纤维间空隙的边界。空隙通过高导热性CVD金刚石材料渗透，连续地涂覆纤维的第二表面区域，并且包括从单独紧邻的纤维的第二表面区域到颗粒间空隙的合并生长前沿。高导热性CVD金刚石材料具有大于约15微米的平均微晶尺寸，金刚石 - 拉曼峰 - 光致发光背景强度的强度比大于约20，金刚石拉曼峰的最大强度（以计数/秒计）除了大于约3的1270cm-1处的光致发光强度，小于约6cm -1的拉曼sp3全宽半最大值和大于约25的金刚石 - 石墨拉曼比。CVD的热导率金刚石材料超过17 Wcm-1K-1。

6. 发明授权

US5273790A Method for consolidating diamond particles to form high thermal conductivity article 失效
标题翻译：用于固结金刚石颗粒以形成高导热性物品的方法
公开(公告)号：US5273790A
公开(公告)日：1993-12-28
申请号：US954673
申请日：1992-09-30
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/27 , B05D3/06
CPC分类号： C23C16/274 , C01B31/065 , C23C16/27 , Y10T156/10
摘要： Method for consolidating diamond material, substantially free of voids, has an average crystallite size greater than about 15 microns, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm.sup.-1 greater than about 3, a Raman sp.sup.3 full width half maximum less than about 6 cm.sup.-1 and a diamond-to-graphite Raman ratio greater than about 25. The diamond material may also comprise carbon atoms with a C.sup.13 content less than 0.05 atomic %.
摘要翻译：用于固结基本上没有空隙的金刚石材料的方法具有大于约15微米的平均微晶尺寸，以秒/秒计的金刚石拉曼峰的最大强度除以大于约3的1270cm -1处的光致发光强度，拉曼sp3全宽半最小值小于约6cm -1，金刚石至石墨拉曼比大于约25.金刚石材料还可包含C13含量小于0.05原子％的碳原子。

7. 发明授权

US5496596A Methods for producing diamond materials with enhanced heat conductivity 失效
标题翻译：生产具有增强导热性的金刚石材料的方法
公开(公告)号：US5496596A
公开(公告)日：1996-03-05
申请号：US188279
申请日：1994-01-28
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , B05D3/06 , C23C16/26
CPC分类号： C23C16/274 , C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C04B2235/427 , C04B2235/667 , Y10T428/249955 , Y10T428/249956 , Y10T428/249957 , Y10T428/249967 , Y10T428/24997 , Y10T428/24999 , Y10T428/2938 , Y10T428/2991 , Y10T428/30
摘要： A method for growing a diamond film, substantially free of voids, having an average crystallite size greater than about 15 microns, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm.sup.-1 greater than about 3, a Raman sp.sup.3 full width half maximum less than about 6 cm.sup.-1, and a diamond-to-graphite Raman ratio greater than about 25, includes the steps of preparing a substrate by abrasion with diamond particles; placing the substrate in a CVD reactor; depositing diamond during a first deposition stage by providing an atmosphere consisting essentially of a mixture of about 200 sccm H.sub.2 and 10 sccm CH.sub.4, at a pressure of about 90 Torr, providing between about 1,800 and 1,950 watts of microwave power at a frequency of about 2.45 GHz to ignite and sustain a plasma in the region of said substrate, and maintaining the substrate at a temperature of between about 625.degree. C. and 675.degree. C. for a period of time sufficient to form a diamond layer which is substantially continuous; depositing a diamond during a second deposition stage by providing an atmosphere consisting essentially of a mixture of about 200 sccm H.sub.2, 4.6 sccm CO, and 9 ccm of CH.sub.4 at a pressure of about 90 Torr, providing between about 1,800 and 1,950 watts of microwave power at a frequency of between about 2.45 GHz and maintaining said substrate material at a temperature of between about 625.degree. C. and 675.degree. C. for a period of time sufficient to form a diamond layer having a desired thickness; and removing the substrate material from said CVD reactor.
摘要翻译：用于生长基本上不含空隙的金刚石膜的方法，其平均微晶尺寸大于约15微米，金刚石拉曼峰的最大强度计数/秒除以1270cm -1以上的光致发光强度大于约如图3所示，拉曼峰3全宽半最小值小于约6cm -1，金刚石 - 石墨拉曼比大于约25，包括用金刚石颗粒磨损制备基底的步骤; 将衬底放置在CVD反应器中; 通过在大约90托的压力下提供基本上由大约200sccm H 2和10sccm CH 4的混合物组成的气氛，在第一沉积阶段沉积金刚石，以约2.45的频率提供约1,800至1950瓦的微波功率以在所述衬底的区域中点燃和维持等离子体，并将衬底保持在约625℃至675℃之间的温度下足以形成基本连续的金刚石层的时间; 在第二沉积阶段通过在约90托的压力下提供基本上由大约200sccm H 2，4.6sccm CO和9cm 3 CH 4的混合物组成的气氛来沉积金刚石，提供约1,800至1950瓦的微波功率以约2.45GHz的频率，并将所述衬底材料保持在约625℃至675℃之间的温度下足以形成具有所需厚度的金刚石层的时间; 以及从所述CVD反应器中去除衬底材料。

8. 发明授权

US5316842A Diamond/non-diamond materials with enhanced thermal conductivity 失效
标题翻译：具有增强导热性的钻石/非金刚石材料
公开(公告)号：US5316842A
公开(公告)日：1994-05-31
申请号：US95314
申请日：1993-07-21
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/04 , C23C16/27 , B32B3/26
CPC分类号： C23C16/274 , C01B31/065 , C04B30/02 , C04B35/52 , C04B35/64 , C04B38/0038 , C23C16/045 , C23C16/27 , C04B2235/427 , C04B2235/667 , Y10T428/249955 , Y10T428/249956 , Y10T428/249957 , Y10T428/249967 , Y10T428/24997 , Y10T428/24999 , Y10T428/2938 , Y10T428/2991 , Y10T428/30
摘要： The present invention comprises an article formed from a plurality of non-diamond particles compatible with diamond deposition preformed into a desired shape. Each of the particles has first surface regions in contact with immediately adjacent other ones of the particles, and second surface regions spaced apart from the immediately adjacent other ones of said particles to define boundaries of inter-particle voids between the immediately adjacent ones of the particles. The voids are infiltrated with high thermal conductivity CVD diamond material continuously coating the second surface regions of the particles and comprising merged growth fronts from the second surface regions of individual immediately adjacent ones of the particles into the inter-particle voids. The high thermal conductivity CVD diamond material has an average crystallite size greater than about 15 microns, an intensity ratio of diamond- Raman-peak-to-photoluminescence background intensity greater than about 20, a maximum intensity of the diamond Raman peak in counts/sec divided by the intensity of photoluminescence at 1270 cm.sup.-1 greater than about 3, a Raman sp.sup.3 full width half maximum less than about 6 cm.sup.-1 and a diamond-to-graphite Raman ratio greater than about 25. The thermal conductivity of the CVD diamond material is in excess of 17 Wcm.sup.-1 K.sup.-1.
摘要翻译：本发明包括由与形成所需形状的金刚石沉积相容的多个非金刚石颗粒形成的制品。每个颗粒具有与直接相邻的其它颗粒接触的第一表面区域，以及与紧邻的另一个颗粒间隔开的第二表面区域，以限定紧邻的颗粒之间的颗粒间空隙的边界。空隙被高导热性CVD金刚石材料渗透，连续地涂覆颗粒的第二表面区域并且包括从单个紧邻的颗粒的第二表面区域到颗粒间空隙中的合并生长前沿。高导热性CVD金刚石材料具有大于约15微米的平均微晶尺寸，金刚石 - 拉曼峰 - 光致发光背景强度的强度比大于约20，金刚石拉曼峰的最大强度以计数/秒计除了大于约3的1270cm-1处的光致发光强度，小于约6cm -1的拉曼sp3全宽半最大值和大于约25的金刚石 - 石墨拉曼比。CVD的热导率金刚石材料超过17 Wcm-1K-1。

9. 发明授权

US5273825A Article comprising regions of high thermal conductivity diamond on substrates 失效
标题翻译：文章包括在基底上具有高导热性金刚石的区域
公开(公告)号：US5273825A
公开(公告)日：1993-12-28
申请号：US954353
申请日：1992-09-30
申请人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
发明人： John A. Herb , John M. Pinneo , Clayton F. Gardinier
IPC分类号： C01B31/06 , C23C16/27 , C30B29/04
CPC分类号： C23C16/274 , C01B31/065 , C23C16/27 , Y10T428/30 , Y10T428/31678
摘要： A diamond coated article, wherein the diamond has a thermal conductivity of at least 17 Wcm K.
摘要翻译：金刚石涂层制品，其中金刚石的导热率至少为17Wcm。

10. 发明授权

US5325384A Structure and method for mounting laser diode arrays 失效
标题翻译：安装激光二极管阵列的结构和方法
公开(公告)号：US5325384A
公开(公告)日：1994-06-28
申请号：US818286
申请日：1992-01-09
申请人： John A. Herb , John M. Pinneo
发明人： John A. Herb , John M. Pinneo
IPC分类号： H01L23/32 , H01S3/04 , H01S5/00 , H01S5/02 , H01S5/024 , H01S5/40 , H01S3/045
CPC分类号： H01S5/4025 , H01S5/02 , H01L2224/48091 , H01S5/02264 , H01S5/02272 , H01S5/02276 , H01S5/024 , H01S5/4031 , H01S5/405
摘要： A carrier for a laser diode bar comprises a generally rectangularly shaped block formed from a dielectric material having a high thermal conductivity. The block includes a stepped recess formed therein having a height essentially equal to one half the height of a laser diode bar to be mounted thereon. An assembly for mounting a laser diode bar comprises a pair of carriers in contact with one another and oriented such that their stepped recesses are in facing relationship to one another. A laser diode bar is positioned between the carriers in the space left by their combined stepped recesses. A plurality of assemblies may be placed in contact with or separated from one another.
摘要翻译：用于激光二极管棒的载体包括由具有高导热性的电介质材料形成的大致矩形的块。该块包括形成在其中的阶梯形凹部，其高度基本上等于要安装在其上的激光二极管条的高度的一半。用于安装激光二极管棒的组件包括彼此接触并定向成使得它们的台阶凹槽彼此面对关系的一对托架。激光二极管棒位于由它们组合的阶梯式凹槽留下的空间中的载体之间。多个组件可以彼此接触或分离放置。

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