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1. 发明授权

US08217198B2 Process for purifying removal of a chemical target compound from a suspension of crystals thereof in mother liquor 有权
标题翻译：从母液中的晶体悬浮液中净化化学靶化合物的方法
公开(公告)号：US08217198B2
公开(公告)日：2012-07-10
申请号：US12706367
申请日：2010-02-16
申请人： Joerg Heilek , Wolfgang Schneider , Wolfgang Gunkel , Volker Schliephake , Klaus Joachim Mueller-Engel
发明人： Joerg Heilek , Wolfgang Schneider , Wolfgang Gunkel , Volker Schliephake , Klaus Joachim Mueller-Engel
IPC分类号： C07C51/42
CPC分类号： B01D9/005 , B01D9/004 , B01D9/0045 , F16C19/30 , F16C19/38 , F16C19/545 , F16C19/56 , F16C23/086
摘要： A process for purifying removal of a chemical target compound from a suspension of crystals thereof in mother liquor in a wash column with forced transport of the crystal bed from the top downward, in which crystals are removed from the lower end of the crystal bed with a rotating removal device and melted, and a portion of the crystal melt is conducted back toward the crystal bed as wash melt, the removal device being secured with a drive shaft conducted into the wash column from the bottom through an inlet having a seal, said drive shaft being driven about its longitudinal axis by a drive unit for rotation and being mounted so as to be rotatable about its longitudinal axis in more than one bearing, such that the mounting in one of the bearings absorbs the downward force acting on the drive shaft, the mounting in two or more bearings absorbs forces acting radially outward from the drive shaft, and the mounting in one bearing is additionally capable of absorbing an upward force acting on the drive shaft.
摘要翻译：一种用于从其晶体悬浮液中清除化学目标化合物从洗涤塔母液中排出的方法，其中从顶部向下将晶体床强制输送，其中晶体从晶体床的下端被除去，旋转去除装置并熔化，并且一部分晶体熔体作为洗涤熔体被导回到晶体床，所述去除装置通过具有密封件的入口从底部传导到洗涤塔中的驱动轴固定，所述驱动轴通过用于旋转的驱动单元围绕其纵向轴线被驱动并且被安装成可以在多于一个轴承中围绕其纵向轴线旋转，使得其中一个轴承中的安装吸收作用在驱动轴上的向下的力，安装在两个或更多个轴承中吸收从驱动轴径向向外作用的力，并且在一个轴承中的安装另外能够吸收作用的向上的力在驱动轴上。

2. 发明授权

US08829134B2 Process for transporting in the tank of a tank truck or tanker ship a liquid monomer phase withdrawn from a storage vessel 有权
标题翻译：在罐车或油罐车的罐中运输的过程是从储存容器中取出的液体单体相
公开(公告)号：US08829134B2
公开(公告)日：2014-09-09
申请号：US12053158
申请日：2008-03-21
申请人： Joerg Heilek , Ulrich Hammon , Volker Schliephake , Klaus Joachim Mueller-Engel , Till Blum
发明人： Joerg Heilek , Ulrich Hammon , Volker Schliephake , Klaus Joachim Mueller-Engel , Till Blum
IPC分类号： C08F2/00 , B01D37/00 , C07C67/56 , C07C67/62 , C07C51/42 , C07C51/47 , C07C45/78 , C07C45/79 , C07C51/50
CPC分类号： C07C45/79 , C07C45/78 , C07C51/42 , C07C51/47 , C07C51/50 , C07C67/56 , C07C67/62 , C07C47/22 , C07C57/04 , C07C69/54
摘要： A process for transporting a liquid monomer phase which has been withdrawn from a storage vessel and comprises methacrylic monomers to an extent of ≧90% by weight, in a tank truck or in a tanker ship, in which the liquid monomer phase is subjected to a separating operation on the route from the storage vessel into the tank of a tank truck or of a tanker ship in order to separate polymer of the monomer present in dissolved form in the liquid monomer phase.
摘要翻译：一种运输液体单体相的方法，所述液体单体相已经从储存容器中取出并且包含甲基丙烯酸类单体至≥90重量％的程度，在油罐车或油罐船中，其中液体单体相经受在从储存容器进入罐车或油罐船的罐的路线上分离操作，以将以溶解形式存在的单体的聚合物分离在液体单体相中。

3. 发明授权

US08299299B2 Process for separating acrylic acid present as a main constituent and glyoxal present as a by-product in a product gas mixture of a partial heterogeneously catalyzed gas phase oxidation of a C3 precursor compound of acrylic acid 有权
标题翻译：用于分离作为主要成分存在的丙烯酸和乙二醛作为副产物存在于丙烯酸的C3前体化合物的部分非均相催化气相氧化的产物气体混合物中
公开(公告)号：US08299299B2
公开(公告)日：2012-10-30
申请号：US12509078
申请日：2009-07-24
申请人： Till Blum , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jaeger , Volker Schliephake , Klaus Joachim Mueller-Engel , Ulrich Hammon , Joerg Heilek , Imke Britta Mueller
发明人： Till Blum , Peter Zurowski , Steffen Rissel , Sylke Haremza , Thorsten Friese , Ulrich Jaeger , Volker Schliephake , Klaus Joachim Mueller-Engel , Ulrich Hammon , Joerg Heilek , Imke Britta Mueller
IPC分类号： C07C51/42
CPC分类号： C07C51/252 , C07C51/43 , C07C57/04
摘要： A process for separating acrylic acid present as a main product and glyoxal present as a by-product in a product gas mixture of a partial gas phase oxidation of a C3 precursor compound, in which a liquid phase P is obtained, which consists of acrylic acid to an extent of at least 70% of its weight and, based on the molar amount of acrylic acid present therein, comprises at least 200 molar ppm of glyoxal, in which the glyoxal is separated from the acrylic acid in the liquid phase P by crystallization.
摘要翻译：将作为主要成分存在的丙烯酸和作为副产物存在的乙二醛的方法分离在得到液相P的C3前体化合物的部分气相氧化的产物气体混合物中，该混合物由丙烯酸至少其重量的70％的程度，并且基于其中存在的丙烯酸的摩尔量，包含至少200摩尔ppm的乙二醛，其中通过结晶将乙二醛与液相P中的丙烯酸分离。

4. 发明授权

US07732624B2 Process for operating a continuous removal of a target product X in the form of fine crystals 有权
标题翻译：用于以细晶体的形式连续移除靶产物X的方法
公开(公告)号：US07732624B2
公开(公告)日：2010-06-08
申请号：US12208737
申请日：2008-09-11
申请人： Joerg Heilek , Ulrich Hammon , Klaus Joachim Mueller-Engel , Volker Schliephake , Dieter Baumann
发明人： Joerg Heilek , Ulrich Hammon , Klaus Joachim Mueller-Engel , Volker Schliephake , Dieter Baumann
IPC分类号： C07D207/26 , C07C51/43 , C07C7/14
CPC分类号： B01D9/0013 , B01D9/004 , B01D9/005 , B01D9/0063 , C07C7/14 , C07C51/43 , C07C15/08 , C07C57/04
摘要： A process for continuously removing a target product X in the form of fine crystals from a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in an indirect heat transferer, in which the crystal suspension formed is conducted out of the heat transferer first into a mixed buffer tank and, from there, fed to an apparatus for separating the crystal suspension into crystals and liquid phase, and wherein external measures dissipade the oversaturation of the crystal suspension fed to the buffer vessel with target product X.
摘要翻译：通过在间接热转移体中冷却悬浮液结晶，从包含目标产物X和除了目标产物X的成分的液相P连续除去目标产物X的形式的方法，其中形成的晶体悬浮液为首先从热转移器中导出到混合缓冲罐中，从那里进料到用于将晶体悬浮液分离成晶体和液相的装置，并且其中外部措施消除了用目标物供给缓冲容器的晶体悬浮液的过饱和产品X.

5. 发明授权

US07319166B2 Method of purifying a raw melt of at least one monomer by crystallization 有权
标题翻译：通过结晶纯化至少一种单体的原料熔体的方法
公开(公告)号：US07319166B2
公开(公告)日：2008-01-15
申请号：US10476187
申请日：2002-05-02
申请人： Ulrich Hammon , Bernd Eck , Dieter Baumann , Joerg Heilek , Klaus Joachim Mueller-Engel
发明人： Ulrich Hammon , Bernd Eck , Dieter Baumann , Joerg Heilek , Klaus Joachim Mueller-Engel
IPC分类号： C07C51/43 , C07D207/00
CPC分类号： C07D207/267 , C07C51/43 , C07C57/04
摘要： The invention relates to a method for purifying a raw melt of at least one monomer by crystallization, wherein suspension crystallization is initially used and the resulting remaining melt or the suspension crystals that have been molten once again and separated are subjected to a mechanical separation operation before undergoing subsequent purification by crystallization.
摘要翻译：本发明涉及一种通过结晶纯化至少一种单体的原料熔体的方法，其中最初使用悬浮液结晶，并将所得剩余熔体或已经再次熔融并分离的悬浮液晶体进行机械分离操作，然后进行机械分离操作随后通过结晶进行纯化。

6. 发明授权

US07795470B2 Method for the heterogeneously catalyzed partial direct oxidation of n-propane to acrylic acid 有权
标题翻译：将丙烷非均相催化部分直接氧化成丙烯酸的方法
公开(公告)号：US07795470B2
公开(公告)日：2010-09-14
申请号：US12142444
申请日：2008-06-19
申请人： Martin Dieterle , Joerg Heilek , Klaus Joachim Mueller-Engel
发明人： Martin Dieterle , Joerg Heilek , Klaus Joachim Mueller-Engel
IPC分类号： C07C51/16
CPC分类号： C07C51/215 , C07C57/04
摘要： A method for the heterogeneously catalyzed partial direct oxidation of propane to acrylic acid in the gas phase, in which the reaction gas inlet mixture comprises cyclopropane as an impurity and the acrylic acid, after it has been converted from the product gas mixture into the liquid phase, is operated from the other constituents of the liquid phase with the aid of a separation by crystallization.
摘要翻译：在气相中异丙烯催化部分直接氧化丙烷到丙烯酸的方法，其中反应气体入口混合物包含作为杂质的环丙烷和丙烯酸，在其从产物气体混合物转化成液相之后，借助于通过结晶分离，从液相的其它组分操作。

7. 发明授权

US07589236B2 Process for separating acrylic acid and benzoic acid present in a product gas mixture of a partial heterogeneously catalyzed gas phase oxidation of a C3 precursor compound of acrylic acid 有权
标题翻译：在丙烯酸C3前体化合物的部分非均相催化气相氧化的产物气体混合物中存在的丙烯酸和苯甲酸分离方法
公开(公告)号：US07589236B2
公开(公告)日：2009-09-15
申请号：US11873883
申请日：2007-10-17
申请人： Joerg Heilek , Klaus Joachim Mueller-Engel , Martin Dieterle , Armin Diefenbacher
发明人： Joerg Heilek , Klaus Joachim Mueller-Engel , Martin Dieterle , Armin Diefenbacher
IPC分类号： C07C51/42
CPC分类号： C07C51/42 , C07C51/235 , C07C51/43 , C07C51/44 , C07C57/04 , C07C63/06
摘要： A process for separating acrylic acid and benzoic acid present in the product gas mixture of a partial oxidation to acrylic acid, in which the acrylic acid and the benzoic acid are first converted to a liquid phase, constituents having a lower boiling point than benzoic acid and acrylic acid are removed therefrom by thermal separating processes, and the acrylic acid is removed by crystallization from the remaining liquid phase.
摘要翻译：将部分氧化的产物气体混合物中存在的丙烯酸和苯甲酸分离为丙烯酸的方法，其中丙烯酸和苯甲酸首先转化为液相，沸点低于苯甲酸的组分和通过热分离方法除去丙烯酸，通过从剩余液相中结晶除去丙烯酸。

8. 发明授权

US07129376B2 Method for the production of a purified melt of at least one monomer 有权
标题翻译：制备至少一种单体的纯化熔体的方法
公开(公告)号：US07129376B2
公开(公告)日：2006-10-31
申请号：US10476188
申请日：2002-05-02
申请人： Ulrich Hammon , Bernd Eck , Dieter Baumann , Joerg Heilek , Klaus Joachim Mueller-Engel
发明人： Ulrich Hammon , Bernd Eck , Dieter Baumann , Joerg Heilek , Klaus Joachim Mueller-Engel
IPC分类号： C07C51/42 , C07D207/24
CPC分类号： C07D207/267 , C07C51/43 , C07C51/47 , C07C51/48 , C07C57/04
摘要： The invention relates to a method for the production of a purified melt of a monomer melt obtained by condensation, absorption or extraction in a crystallizer, wherein the inlet to the crystallizer is subjected to a mechanical solid/liquid separation operation.
摘要翻译：本发明涉及通过在结晶器中冷凝，吸收或萃取获得的单体熔体的纯化熔体的制备方法，其中结晶器的入口进行机械固/液分离操作。

9. 发明申请

US20090076284A1 PROCESS FOR CONTINUOUSLY REMOVING A TARGET PRODUCT X IN THE FORM OF FINE CRYSTALS 有权
标题翻译：在精细晶体形式下连续去除目标产品X的方法
公开(公告)号：US20090076284A1
公开(公告)日：2009-03-19
申请号：US12209594
申请日：2008-09-12
申请人： Joerg Heilek , Peter Schlemmer , Ulrich Hammon , Klaus Joachim Mueller-Engel
发明人： Joerg Heilek , Peter Schlemmer , Ulrich Hammon , Klaus Joachim Mueller-Engel
IPC分类号： C07C51/43 , C07C7/14 , C07D207/04
CPC分类号： B01D9/0013 , B01D9/0045 , B01D9/0063 , C07C51/43 , C07C57/04
摘要： A process for continuously removing a target product X in the form of fine crystals from a liquid phase P comprising the target product X and constituents other than the target product X by cooling suspension crystallization in the secondary chamber, into which the liquid phase P flows continuously, of an indirect heat exchanger with simultaneous continuous flow of a coolant through the primary chamber of the indirect heat exchanger and continuous withdrawal of a crystal suspension S having a degree of crystallization Y from the secondary chamber, in which the degree of crystallization Y is adjusted on the basis of a heat balance conducted continuously with the aid of a process computer.
摘要翻译：从液相P连续除去来自包含目标产物X的液相P和除了目标产物X以外的成分的微晶形式的目标产物X的方法，通过冷却液相P连续流入的二次室中的悬浮液结晶的间接热交换器，其通过间接热交换器的主室同时连续流动冷却剂，并且从二级室连续取出具有结晶度Y的晶体悬浮液S，其中结晶度Y被调节基于在过程计算机的帮助下连续进行的热平衡。

10. 发明授权

US08461383B2 Process for starting up a separating process for purifying removal of acrylic acid crystals from a suspension S of crystals thereof in mother liquor 有权
标题翻译：用于启动分离过程的方法，用于从母液中的晶体的悬浮液S中纯化除去丙烯酸晶体
公开(公告)号：US08461383B2
公开(公告)日：2013-06-11
申请号：US12897199
申请日：2010-10-04
申请人： Joerg Heilek , Dirk Litters , Klaus Joachim Mueller-Engel
发明人： Joerg Heilek , Dirk Litters , Klaus Joachim Mueller-Engel
IPC分类号： C07C51/43
CPC分类号： C07C51/43 , C07C51/47 , C07C57/04
摘要： A process for starting up a separating process for purifying removal of acrylic acid crystals from a suspension S of crystals thereof in mother liquor with a hydraulic wash column which has a crystal melt circuit including crystal melt space, and a process space and a distributor space which are separated by an end with passages connecting the two spaces, in which the crystal bed is formed for the first time by first filling the crystal melt circuit and, at least partly, the process space with an acrylic acid-comprising startup liquid whose acrylic acid crystal formation temperature is less than or equal to the temperature of the suspension S increased by 15° C., and then continuing the filling of the wash column with the suspension S and optionally with control liquor until the difference between the pressure in the crystal melt space and the pressure in the distributor space falls suddenly, the arithmetic mean of the total waste liquor flow flowing through the filters of the filter tubes of the wash column until this time, based on the area of all filters, being not more than 80 m3/(m2·h).
摘要翻译：一种用于利用具有包括晶体熔融空间的晶体熔融回路的液压洗涤柱从母液中的晶体悬浮液S中纯化除去丙烯酸晶体的分离过程的工艺，以及工艺空间和分配器空间，通过连接两个空间的通道分开一端，其中通过首先填充晶体熔融回路并且至少部分地与包含丙烯酸的启动液体的工艺空间首次形成晶体床，其中丙烯酸晶体形成温度小于或等于悬浮液S的温度升高15℃，然后用悬浮液S和任选地与对照液体继续填充洗涤柱，直到晶体熔体中的压力差空间和分配器空间中的压力突然下降，流过滤器过滤器的总废液流的算术平均值根据所有过滤器的面积，直到此时为止，洗涤塔的管子不超过80立方米/（m2·h）。

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